Within the air purification system of a nuclear power plant, specific radioactive isotopes are extracted from gases through adsorption onto activated carbon. To properly dispose of used activated carbon, it is essential to determine the concentration of radioactive nuclides within it. This study discusses the application of the pyrolysis method for analyzing the concentrations of 3H and 14C in spent activated carbon. The pyrolysis was conducted using Raddec’s Pyrolyser, with adjustments made to parameters such as temperature profiles, airflow rates, sample quantities, and trapping solution volumes. The evaluation method for the pyrolysis of activated carbon to analyze 3H and 14C involved adding 3H and 14C sources to the activated carbon before use and subsequently assessing the recovery rates of the added sources in comparison to the analysis results.

• Jieun Park(Korea Hydro and Nuclear Power (KHNP) Central Research Institute (KHNP-CRI))
• Kahee Jeong(Korea Hydro and Nuclear Power (KHNP) Central Research Institute (KHNP-CRI))
• Sooyeon Lim(Korea Hydro and Nuclear Power (KHNP) Central Research Institute (KHNP-CRI))
• Wook Sohn(Korea Hydro and Nuclear Power (KHNP) Central Research Institute (KHNP-CRI)) Corresponding author