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        검색결과 1

        1.
        2019.02 KCI 등재 SCOPUS 구독 인증기관 무료, 개인회원 유료
        A powder mixture of 70 wt% Al2O3 and 30 wt% hydroxyapatite (HA) is sintered at 1300 ℃ or 1350 ℃ for 2 h at normal pressure. An MgF2-added composition to make HA into fluorapatite (FA) is also prepared for comparison. The samples without MgF2 show α & β-tricalcium phosphates (TCPs) and Al2O3 phases with no HA at either of the sintering temperatures. In the case of 1,350 ℃, a CaAl4O7 phase is also found. Densification values are 69 and 78 %, and strengths are 156 and 104MPa for 1,300 and 1,350 ℃, respectively. Because the decomposition of HA produces a H2O vapor, fewer large pores of 5-6 μm form at 1,300 ℃. The MgF2-added samples show FA and Al2O3 phases with no TCP. Densification values are 79 and 87%, and strengths are 104 and 143 MPa for 1,300 and 1,350 ℃, respectively. No large pores are observed, and the grain size of FA (1-2 μm) is bigger than that of TCP (0.7 μm ≥) in the samples without MgF2. The resulting TCP/Al2O3 and FA/Al2O3 composites fabricated in situ exhibit strengths 6-10 times higher than monolithic TCP and HA.
        4,000원