Metal matrix composites(MMC) can obtain mechanical characteristics of application purposes that a single material is difficult to obtain. Al2 O3/AC8A composites were fabricated by low pressure infiltration process. The purpose is establishing the optimal casting conditions for composite preparation under low pressure. It is known the inorganic binder help infiltration. Therefore Al2O3 fiber preform's optimum sinter temperature is 1160℃, added inorganic binder is mixed binder(SiO2 sol:Al2O3 sol=5:2). And three fibers have been compared (Al2O3 80%/SiO2 20%, Al2O3 80%/SiO2 10% and Al2O3 97%/SiO2 3%). Al2O3/AC8A composites was made by each melting temperatures(650℃, 700℃, 750℃) and wear test was performed about effect of temperatures, kind of fiber, matrix and composites, aging time. Wear test is Ball on disk wear test. The resistance increased with the low melting temperature and Al2O3 80%/SiO2 20% fiber.
Ni and Ni-Cr reinforced Al alloy (AC8A) composites were fabricated by low pressure infiltration process. Porous Ni was applied as preform. Ni reinforced AC8A composites were fabricated under 0.3 MPa at 650, 700 and 750 degrees centigrade, respectively, while Ni-Cr reinforced AC8A composites were fabricated under low pressure limited to the maximum of 0.5 Mpa at 750, 800 and 850 degrees centigrade, respectively. Microstructure and phase composition of the composites were evaluated by optical microscope, X-Ray diffraction (XRD), electro-probe micro analyzer (EMPA). Intermetallic compounds Al3Ni and CrSi were observed in the composites. The results indicate that the grain size has been increasing with the increase of the infiltration temperatures. However, the wear resistance of Ni/AC8A and Ni-Cr AC8A peaked at 650 degree centigrade and 800 degrees centigrade, respectively. In addition, based on the wear characteristics and wear surfaces, Ni-Cr/AC8A composites have a better wear resistance than Ni/AC8A composites and AC8A.
The carbon brake discs were manufactured by densification the carbon fiber preform using PG-CVI technology with Propene as a carbon precursor gas and Nitrogen as a carrier gas. The densities of carbon brake discs were tested at different densification time. The results indicate that the densification rate is more rapid before 100 hrs than after 200 hrs. The CTscanning image and the SEM technology were used to observe the inner subtle structure. CT-images show the density distribution in the carbon brake disc clearly. The carbon brake disk made by PG-CVI is not very uniform. There is a density gradient in the bulk. The high-density part in the carbon brake is really located in the friction surface, especially in the part of inner circle. This density distribution is most suitable for the stator disc.
프로판(C3H8)을 반응가스로 사용하여 등온 저압화학기상침투법(low-pressure chemical vapor infiltration)으로 탄소/탄소 복합재료를 치밀화 할 때 반응온도, 반응가스농도, 가스유량, 반응압력 등의 제조공정변수들이 치밀화에 미치는 영향을 알아보기 위하여 실험계획법(Rdbust design method)에 의한 실험을 행하였다. 1회의 등온 저압화학기상침투 실험으로 탄소/탄소 복합재료의 부피 밀도와 표면과 내부의 부피 밀도의 차이를 특성치(characteristic value)로 한 실험계획법의 분산분석(analysis of variance)에 의하면 반응온도, 반응가스농도, 가스유량 등의 제고공정변수가 치밀화에 기여도가 높으며, 반응압력의 기여도와 제조공정변수들의 교호작용(interaction)에 의한 기여도는 낮은 것으로 나타났다. 반응온도가 1100˚C, 반응가스농도가 100% C3H8, 가스유량이 100 SCCM, 반응압력이 5torr인 조건에서 탄소/탄소 복합재료는 가장 높은 부피 밀도값을 나타내었으나 시편의 표면과 내부의 부피 밀도 차이값은 컸다.