In the present work, Al- composite powders were fabricated using a mechanical milling process and its milling behaviors and mechanical properties as functions of sizes ( , 500 nm and 50 nm) and concentrations (1, 3 and 10 wt.%) were investigated. For achieving it, composite powders and their compacts were fabricated using a planetary ball mill machine and magnetic pulse compaction technology. Al- composite powders represent the most uniform dispersion at a milling speed of 200 rpm and a milling time of 240 minutes. Also, the smaller particles were presented, the more excellent compositing characteristics are exhibited. In particular, in the case of the 50 nm added compact, it showed the highest values of compaction density and hardness compared with the conditions of and 500 nm additions, leading to the enhancement its mechanical properties.