손해배상액의 산정의 일환으로 합리적 실시료 를 산정하는 경우 합리적 실시료를 산정하는 여 러 방법들이 존재하며, 그 중에서도 하향식 접근 법을 통하여 합리적 실시료를 산정하는 케이스가 늘어나고 있다. 복합 기술이 주를 이루는 기술 분야에 한하여 서는 실시료 과적의 문제 해결의 이익이 경제적 타당성보다도 우선한다 할 것이며, 특히 표준 특 허의 분야에 있어서는 실시료 과적이 실재할 수 있다는 점을 고려해야 할 것이다. 따라서, 복합 기술이 주를 이루는 기술 분야와 표준 특허에 대 하여는 합리적 실시료 산정 시 하향식 접근법의 최대 누적 실시료의 결정으로 실시료의 상한을 결정하는 것이 타당할 것이다. 특허권의 가치가 변동성을 갖는 것으로 신뢰할 수 없다는 점을 고려할 때, 실시자가 실시한 기술에 집적된 전체 특허 각각에 대한 가치를 평가하 여 손해배상의 기초가 되는 특허의 기여도를 산 출하기에는무리가있을것으로판단되며, 특허권 자 사이에 형평성을 유지하면서도 공개된 데이터 에 의하여 기계적인 배분이 가능한 특허 카운팅 이 고려되어야 할 것으로 판단된다. 특허권 각각의 가치 평가를 진행하는 것은 가 치 변동 이슈와 현실적 어려움 등으로 배제되어 야 할 것으로 보이며, In re Innovatio의 판결이 나 로렌츠 커브와 같이 특허의 누적 분포에 따른 기술 내의 가치 비중에 관한 통계적 데이터의 객 관적 자료가 있다면, 이를 적극 활용하여 특허권 사이의 가치 비중을 고려하는 노력이 필요할 것 이다.
본 연구는 나이트록스 잠수와 공기 잠수를 비교하여 잠수작업에서의 안전성 및 경제성 평가를 시도하였다. 연구를 위해서 2010년 거가대교 침매터널 건설시 사용되었던 실제 잠수자료를 사용하였으며, 감압병 발생율, 작업시간, 감압시간 등 두 기체 다이빙의 특징을 분석하였다. 그 결과 잠수사가 호흡기체로 나이트록스를 사용하고 감압기체로 100% 산소를 사용한다면 감압병 발생확률을 최소화 할 수 있으며 감압기간 또한 크게 단축할 수 있음을 확인하였다. 그리고 실제 나이트록스를 사용한 공사기간과 공기 잠수를 하였을 경우의 가상의 공사기간을 비교해 본 결과 최대 3배의 공사기간 단축 효과를 가져왔음을 확인하였다. 결론적으로 시간적, 육체적으로 제한되어있는 환경에서 잠수 시 나이트록스 잠수가 공기 잠수보다 능률적이고 경제적임을 확인하였다.
The present work investigated the dispersion behavior of Y2O3 particles into AISI 316L SS manufactured using laser cladding technology. The starting particles were produced by high energy ball milling in 10 min for pre- alloying, which has a trapping effect and homogeneous dispersion of Y2O3 particles, followed by laser cladding using CO2 laser source. The phase and crystal structures of the cladded alloys were examined by XRD, and the cross section was characterized using SEM. The detailed microstructure was also studied through FE-TEM. The results clearly indi- cated that as the amount of Y2O3 increased, micro-sized defects consisted of coarse Y2O3 were increased. It was also revealed that homogeneously distributed spherical precipitates were amorphous silicon oxides containing yttrium. This study represents much to a new technology for the manufacture and maintenance of ODS alloys.
In the present work, 6061 Al-B4C sintered composites containing different B4C contents were fabricated and their characteristic were investigated as a function of sintering temperature. For this, composite powders and their compacts with B4C various contents from 0 to 40 wt.% were fabricated using a planetary ball milling equipment and cold isostatic pressing, respectively, and then they were sintered in the temperature ranges of 580 to 660o C. Above sin- tering temperature of 640o C, real density was decreased due to the occurrence of sweat phenomena. In addition, it was realized that sinterability of 6061Al-B4C composite material was lowered with increasing B4C content, resulting in the decrease in its real density and at the same time in the increment of porosity.
In the present work, Al- composite powders were fabricated using a mechanical milling process and its milling behaviors and mechanical properties as functions of sizes ( , 500 nm and 50 nm) and concentrations (1, 3 and 10 wt.%) were investigated. For achieving it, composite powders and their compacts were fabricated using a planetary ball mill machine and magnetic pulse compaction technology. Al- composite powders represent the most uniform dispersion at a milling speed of 200 rpm and a milling time of 240 minutes. Also, the smaller particles were presented, the more excellent compositing characteristics are exhibited. In particular, in the case of the 50 nm added compact, it showed the highest values of compaction density and hardness compared with the conditions of and 500 nm additions, leading to the enhancement its mechanical properties.
This study investigated refinement behaviors of TiC powders produced under different impact energy conditions using a mechanical milling process. The initial coarse TiC powders with an average diameter of 9.3 were milled for 5, 20, 60 and 120 mins through the conventional low energy mechanical milling (LEMM, 22G) and specially designed high energy mechanical milling (HEMM, 65G). TiC powders with angular shape became spherical one and their sizes decreased as the milling time increased, irrespective of milling energy. Based upon the FE-SEM and BET results of milled powders, it was found initial coarse TiC powders readily became much finer near 100 nm within 60 min under HEMM, while their sizes were over 200 nm under LEMM, despite the long milling time of up to 120 min. Particularly, ultra-fine TiC powders with an average diameter of 77 nm were fabricated within 60 min in the presence of toluene under HEMM.
In the present work, bismuth nanopowders with various particle size distributions were synthesized by controlling argon (Ar) gas flow rate and chamber pressure of a gas condensation (GC) apparatus. From the analyses of transmission electron microscopy (TEM) images and nitrogen gas adsorption results, it was found that as Ar gas flow rate increased, the specific surface area of bismuth increased and the average particles size decreased. On the other hand, as the chamber pressure increased, the specific surface area of bismuth decreased and the average particles size increased. The optimum gas flow rate and chamber pressure for the maximized electrochemical active surface area were determined to be 8 L/min and 50 torr, respectively. The bismuth nanopowders synthesized at the above condition exhibit 13.47 of specific surface area and 45.6 nm of average particles diameter.
In this paper, the electrochemical non-enzyme immunosensor has been developed for the determination of salmonella antigen, using inverse voltammetry. For the estimation of salmonella antigen concentration, the nanoparticles synthesized by microemulsion method were conjugated with salmonella antigen. Then, the immunocomplex between antibody immobilized on the transducer surface and antigen containing a magnetic nanoparticles was formed. From the linear relationship between the reduction peak current of Fe(III) and salmonella antigen concentration, it is suggested that the electrochemical non-enzyme biosensor is applicable to detect salmonella antigen in the concentration range of
Trace analysis of Cd and Pb at surface modified thick film graphite electrode with Bi nanopowder has been carried out using square-wave anodic stripping voltammetry (SWASV) technique. Bi nanopowder synthesized by gas condensation (GC) method showed the size of nm with BET surface area, . For a strong adhesion of the Bi nanopowder onto the screen printed carbon paste electrode, nafion solution was added into Bi-containing suspension. From the SWASV, it was found that the Bi nanopowder electrode exhibited a well-defined responses relating to the oxidations of Cd and Pb. The current peak intensity increased with increasing concentration of Cd and Pb. From the linear relationship between Cd/Pb concentrations and peak current, the sensitivity of the Bi nanopowder electrode was quantitatively estimated. The detection limit of the electrode was estimated to be and for Cd and Pb, respectively, on the basis of the signal-to-noise characteristics (S/N=3) of the response for the solution under a 10 min accumulation.
This article presents the successful consolidation of the mixed Co and Diamond powders for a drilling segment by the combined application of magnetic pulsed compaction (MPC) and subsequent sintering, and their properties were analyzed. Homogeneous hardness (Hv 220) and density (97%) of sintered bulks fabricated by MPC were obtained by the new technique, where higher pressure has been employed for short period of time than that of general process. A fine microstructure and homogeneous hardness in the consolidated bulk were observed without cracks. Relatively higher drilling speed of 9.61 cm/min and life time of 6.55 m were found to the MPCed specimens, whereas the value of the specimens fabricated by general process was 11.71 cm/min and 7.96 m, respectively. A substantial improvement of mechanical properties of segment was achieved through this study.
This article presents the challenges toward the successful consolidation of nanopowder using magnetic pulsed compaction (MPC). In this research the ultrafine-structured bulks have been fabricated by the combined application of magnetic pulsed compaction (MPC) and subsequent sintering, and their properties were investigated. The obtained density of bulk prepared by the combined processes was increased with increasing MPC pressure from 0.5 to 1.25 GPa. Relatively higher hardness and fracture toughness in the MPCed specimen at 1.25 GPa were attributed to the retention of the nanostructure in the consolidated bulk without cracks. The higher fracture toughness could be attributed to the crack deflection by homogeneous distribution and the retention of nanostructure, regardless of the presence of porosities. In addition, the as consolidated bulk using magnetic pulsed compaction showed enhanced breakdown voltage.
The electrophoretic deposition process of Ni nano-particles in organic suspension was employed for self-repairing of heat exchanger tubes. For this purpose, Ni nano-particles prepared by levitational gas condensation method were dispersed into the solution of ethanol with the addition of dispersant Hypermer KD2. For electrophoretic deposition of Ni nano-particles on the Ni alloy specimen, constant electric fields of 20 and 100 V were applied to the specimen in Ni-dispersed solution. It was found that as electrophoretic deposition proceeds, the size of the pit or crack remarkably decreased due to the agglomeration of Ni nano-particles at the pit or crack. This strongly suggests that the electrophoretic mobility of the charged particles is larger for the damaged part with a higher current value rather than outer surfaces with a lower current value.
In this work, the dispersion behavior of particles in binary aluminum (Al)-copper (Cu) cast alloy was investigated with respect to Cu contents of 20 (hypoeutertic), 33 (eutectic) and 40 (hypereutectic) wt.%. In cases of hypo and hypereutectic compositions, SEM images revealed that the primary Al and phases were grown up at the beginning, respectively, and thereafter the eutectic phase was solidified. In addition, it was found that some of particles can be dispersed into the primary Al phase, but none of them are is observed inside the primary 6 phase. This different dispersion behavior of particles is probably due to the difference in the val- ues of specific gravity between particles and primary phases. At eutectic composition, particles were well dispersed in the matrix since there is few primary phases acting as an impediment site for particle dispersion during solidification. Based on the experimental results, it is concluded that particles are mostly dispersed into the eutectic phase in binary Al-Cu alloy system.
The Ti-Ni alloy nanopowders were synthesized by a levitational gas condensation (LGC) by using a micron powder feeding system and their particulate properties were investigated by x-ray diffraction (XRD), transmission electron microscopy (TEM) and Brunauer-Emmett-Teller (BET) method. The starting Ti and Ni micron powders were incorporated into the micron powder feeding system. An ingot type of the Ti-Ni ahoy was used as a seed material for the levitation and evaporation reactions. The collected powders were finally passivated by oxidation. The x-ray diffraction experiments have shown that the synthesized powders were completely alloyed with Ti and Ni and comprised of two different cubic and monoclinic crystalline phases. The TEM results showed that the produced powders were very fine and uniform with a spherical particle size of 18 to 32nm. The typical thickness of a passivated oxide layer on the particle surface was about 2 to 3 nm. The specific surface area of the Ti-Ni alloy nanopowders was based on BET method.