간행물

한국분말야금학회지 KCI 등재 Journal of Korean Powder Metallurgy Institute

권호리스트/논문검색
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권호

Vol. 14 No. 2 (2007년 4월) 10

2.
2007.04 구독 인증기관 무료, 개인회원 유료
The magnetic alloys of Cu-Fe () were prepared by a mechanical alloying method and their structural and magnetic behaviors were examined by X-ray diffraction and Mossbauer spectra. The magnetization curves did not distinctly show the saturation at 70 kOe for the concentrated alloys of . The Mossbauer spectrum of at room temperature shows one Lorentzian line of the paramagnetic phase, whereas the Mossbauer spectrum of consists of sextet Lorentzian line at room temperature and a centered doublet line. The Mossbauer spectra of measured in the temperature ranges from 13 to 295 K, implies that to consists of two magnetic phases. One superimposed sextet corresponds to the ferromagnetic iron in Cu and the other one indicates the superparamagnetic iron rich phase.
3,000원
3.
2007.04 구독 인증기관 무료, 개인회원 유료
Ultrasonic-milling of metal oxide nanopowders for the preparation of tungsten heavy alloys was investigated. Milling time was selected as a major process variable. XRD results of metal oxide nanopowders ultrasonic-milled for 50 h and 100 h showed that agglomerate size reduced with increasing milling time and there was no evidence of contamination or change of composition by impurities. It was found that nanocomposite powders reduced at in a hydrogen atmosphere showed a chemical composition of 93.1W-4.9Ni-2.0Fe from EDS analysis. Hardness of sintered part using 50 h and 100 h powder samples was 399 Hv and 463 Hv, respectively, which is higher than the that of commercial products (330-340 Hv).
4,000원
4.
2007.04 구독 인증기관 무료, 개인회원 유료
Cu-Ni-P alloy nano powders were fabricated by the electrical explosion of electroless Ni plated Cu wires. The effect of applied voltage on the explosion was examined by applying pulse voltage of 6 and 28 kV, The estimated overheating factor, K, were 1.3 for 6 kV and 2.2 for 28 kV. The powders produced with pulse voltage of 6 kV were composed of Cu-rich solid solution, Ni-rich solid solution, and phase. While, those produced with 28 kV were complete Cu-Ni-P solid solution and small amount of phase. The initial P content of 6.5 at.% was reduced to 2-3 at.% during explosion due to its high vapour pressure.
4,000원
5.
2007.04 구독 인증기관 무료, 개인회원 유료
It is well known that thermal plasma process has lots of advantages such as high temperature and good quality for synthesis of nano particles. In this research, we attempt the synthesis of nano unitary and composite powder (Ag, Mg-Al, Zr-V-Fe) using transferred thermal plasma. Nano particles of metal alloy, ranging from 20 nm to 150 nm, have been synthesized by this process.
4,000원
6.
2007.04 구독 인증기관 무료, 개인회원 유료
In this work, the dispersion behavior of particles in binary aluminum (Al)-copper (Cu) cast alloy was investigated with respect to Cu contents of 20 (hypoeutertic), 33 (eutectic) and 40 (hypereutectic) wt.%. In cases of hypo and hypereutectic compositions, SEM images revealed that the primary Al and phases were grown up at the beginning, respectively, and thereafter the eutectic phase was solidified. In addition, it was found that some of particles can be dispersed into the primary Al phase, but none of them are is observed inside the primary 6 phase. This different dispersion behavior of particles is probably due to the difference in the val- ues of specific gravity between particles and primary phases. At eutectic composition, particles were well dispersed in the matrix since there is few primary phases acting as an impediment site for particle dispersion during solidification. Based on the experimental results, it is concluded that particles are mostly dispersed into the eutectic phase in binary Al-Cu alloy system.
3,000원
7.
2007.04 구독 인증기관 무료, 개인회원 유료
The alumina nano powders synthesized by levitational gas condensation (LGC) method were applied to catalyst in manufacturing process of Hanzsch reaction for Nitrendipine. The L-tartaric acid on the surface is carried out with participation of carbonyl fragments, O-H, C-H bonds which affects stereo selectivity, yield on the reagents positively. From the analysis of the IR-spectroscopy, the carbonyl fragments, O-H, and C-H bond were created by the catalytic reaction. From the analysis of the rR-spectroscopy, the carbonyl fragments, O-H, and C-H bond were created by the catalytic reaction. The newly created bonds made a chiral center on the final product.
4,000원
8.
2007.04 구독 인증기관 무료, 개인회원 유료
In the Ti(CN)-Co/Ni cermet, WC is an effective additive for increasing sinterability and mechanical properties such as toughness and hardness. In this work, WC, (WTi)C and (WTi)(CN) were used as the source of WC and their effects were investigated in the respect of microstructural evolution and mechanical properties. Regardless of the kinds of WC sources, the hard phase with dark core and bright rim structure was observed in the Ti(CN)-Co/Ni cermet under the incorporation of relatively small amount of WC. However, hard phases with bright core began to appear and their frequency increased with the increase of all kinds of WC source addition. The ratio of bright core to dark one in the (TiW)(CN)-Co/Ni cermet was greatest under the incorporation of (WTi)C compared at the same equivalent amount of WC. The mechanical properties were improved with the addition of WC irrespective of the kinds of sources, but the addition of (WTi)(CN) was less effective for the increase of fracture toughness.
4,000원
9.
2007.04 구독 인증기관 무료, 개인회원 유료
Using Spark Plasma Sintering process (SPS), consolidation behavior of gas atomized alloys were investigated via examining the microstructure and evaluating the mechanical properties. In the atomized ahoy powders, fine particles were homogeneously distributed in the matrix. The phase distribution was maintained even after SPS at 723 K, although particles were newly precipitated by consolidating at 748 K. The density of the consolidated bulk Mg-Zn-Y alloy was . The ultimate tensile strength (UTS) and elongation were varied with the consolidation temperature.
4,000원
10.
2007.04 구독 인증기관 무료, 개인회원 유료
Nanocrystalline transient aluminas (-alumina) were coated on core particles (-alumina) by a carbonate precipitation and thermal-assisted combustion, which is environmentally friend. The ammonium aluminum carbonate hydroxide (AACH) as a precursor for coating of transient aluminas was produced from precipitation reaction of ammonium aluminum sulfate and ammonium hydrogen carbonate. The crystalline size and morphology of the synthetic, AACH, were greatly dependent on pH and temperature. AACH with a size of 5 nm was coated on the core alumina particle at pH 9. whereas rod shape and large agglomerates were coated at pH 8 and 11, respectively. The AACH was tightly bonded coated on the core particle due to formation of surface complexes by the adsorption of carbonates, hydroxyl and ammonia groups on the surface of the core alumina powder. The synthetic precursor successfully converted to amorphous- and -alumina phase at low temperature through decomposition of surface complexes and thermal-assisted phase transformation.
4,000원