간행물

한국분말야금학회지 KCI 등재 Journal of Korean Powder Metallurgy Institute

권호리스트/논문검색
이 간행물 논문 검색

권호

Vol. 11 No. 4 (2004년 8월) 11

1.
2004.08 구독 인증기관 무료, 개인회원 유료
탄소재료는 결정구조에 따라 카본블랙(carbon black), 그라파이트(graphite), 탄소섬유(carbon fiber) 등 다양한 형태가 있으며 그 응용 또한 광범위하다. 이는 탄소재료가 화학적으로 매우 안정하고, 열 및 전기전도성이 우수하며, 기계적인 특성면에서도 고강도, 고탄성율을 가지고 있어서 구조적으로 안정하기 때문이다. 특히 (fullerene)와 탄소나노튜브(carbon naotube : CNT)등 근래 새로이 발견된 탄소물질들 은 그
4,000원
2.
2004.08 구독 인증기관 무료, 개인회원 유료
The application concept of using a fail safety filter on the filtering system is to prevent the particle leakage when the main filter element is broken at high temperature. In this study, the metal filters were fabricated by pressureless sintering method. The mixture of stainless steel powders and filler metal binder solved in the water solutions of 5% PVA was compacted to form the cylindrical filter without pressure. The compacted filter were sintered in the vacuum sintering furnace at 120 for 1 hour. The metal filter(produced with powder of 640-840 size) having more than above 50% porosity, 500 pore size, and permeability of 7.310m plugged within 2.5 minute to prevent the leakage of maximum slip particle size of less than 3.
4,000원
3.
2004.08 구독 인증기관 무료, 개인회원 유료
This study for preparation of aluminum nitride (AlN) with high purity was carried out by self-propagating high-temperature synthesis method in two different systems, Al-N and Al-N-AlN, with the change of nitrogen gas pressure and dilution factor. On the occasion of Al-N system, unreacted aluminum was detected in the product in spite of high nitrogen pressure, 10 MPa, This may be caused by obstructing nitrogen gas flow to inner part of molten and agglomerate of aluminum, formed in pre-heating zone. In Al-N-AlN system, AlN with a purity of 95% or ever can be prepared in the condition of f 0.5, PN2 1 MPa, and the purity can be elevated to 98% over in the condition of f = 0.7 and PN2 = 10 MPa
4,000원
4.
2004.08 구독 인증기관 무료, 개인회원 유료
Successful implementation of the powder forming process requires a detailed understanding of several interacting phenomena. The aim is to better control the process variables and to optimize the design parameters. A number of studies were carried out using various constitutive models that take the density change during powder forming into account. Most of them were developed for powders and sintered porous metals, but few of them can describe powder agglomerates, whose behaviour is different from that of uniformly arranged powders. The modification is needed to account for the effect of agglomeration on densification behaviour. Incorporating powder agglomeration into a constitutive model is of considerable importance, as it provides a possibility of relating the powder densification response to microstructural characteristics of powder particles, especially in case of nano powders. In this paper, we proposed a new powder agglomerate model in order to describe the unique densification behaviour of nano powders. The proposed model was applied to the densification of powder agglomerates during cold isostatic pressing.
4,000원
5.
2004.08 구독 인증기관 무료, 개인회원 유료
An experimental study on the combustion of superfine aluminum powders (average particle diameter, a: ∼0.1 ) in air is reported. The formation of aluminum nitride during the combustion of aluminum in air and the influence of the combustion scenario on the structures and compositions of the final products are in the focus of this study. The experiments were conducted in an air (pressure: 1 atm). Superfine aluminum powders were produced by the wire electrical explosion method. Such superfine aluminum powder is stable in air but once ignited it can burn in a self-sustaining way due to its low bulk: density (∼0.1 g/㎤) and a low thermal conductivity. During combustion, the temperature and radiation were measured and the actual burning process was recorded by a video camera. Scanning electron microscopy (SEM), X-ray diffraction (XRD) and chemical analysis were performed on the both initial powders and final products. It was found that the powders, ignited by local heating, burned in a two-stage self-propagating regime. The products of the first stage consisted of unreacted aluminum (-70 mass %) and amorphous oxides with traces of AlN. After the second stage the AlN content exceeded 50 mass % and the residual Al content decreased to ∼10 mass %. A qualitative discussion is given on the kinetic limitation for AlN oxidation due to rapid condensation and encapsulation of gaseous AlN.N.
4,000원
6.
2004.08 구독 인증기관 무료, 개인회원 유료
The elastic moduli of simulated dry process fuels with varying composition and density were measured in order to analyze the mechanical properties of a dry process fuel pellet. Resonant ultrasound spectroscopy(RUS) which can determine all elastic moduli with one set of measurements for a rectangular parallelepiped sample was used to measure the elastic moduli of UO and simulated dry process fuel. The simulated dry process fuel showed a higher value of Young's modulus than UO due to the presence of metallic precipitates and solid solution elements in the UO matrix. The correlation between Young's modulus and porosity(P) of simulated dry process fuel was found to be 231.4-651.8 P (GPa) at room temperature. Dry process fuel with a higher burnup showed higher Young's modulus because total content of fission product element was increased.
4,000원
7.
2004.08 구독 인증기관 무료, 개인회원 유료
Ultrafine titanium carbide particles were synthesized by the reaction of liquid-magnesium and vaporized TiCl+CCl(x = 1 and 2) solution. Fine titanium carbide particles with about 50 nm were successfully produced by combining Ti and C atoms released by chloride reduction of magnesium, and vacuum was then used to remove the residual phases of MgCl and excess Mg. Small amounts of impurities such as O, Fe, Mg and Cl were detected in the product, but such problem can be solved by more precise process control. The lattice parameter of the product was 0.43267 nm, near the standard value. With respect to the reaction kinetics, the activation energy for the reactions of TiCl+CCland Mg was found to 69 kJ/mole, which was about half value against the use of TiCl+CCl, and such higher reactivity of the former contributed to increase the stoichiometry until the level of TiC and decrease the free carbon content below 0.3 wt.%.
4,000원
8.
2004.08 구독 인증기관 무료, 개인회원 유료
Fe nanopowders were successfully synthesized by plasma arc discharge (PAD) process using Fe rod. The influence of chamber pressure on the microstructure was investigated by means of X-ray Diffraction (XRD), Field Emission Scanning Electron Microscope (FE-SEM), Transmission Electron Microscopy (TEM) and X-ray Photoelectron Spectroscopy (XPS). The prepared particles had nearly spherical shapes and consisted of metallic cores (a-Fe) and oxide shells (FeO), The powder size increased with increasing chamber pressure due to the higher dissolution and ejection rate of H and gas density in the molten metal.
4,000원
9.
2004.08 구독 인증기관 무료, 개인회원 유료
In this study, tantalum powder has been producted by MR-EMR combination process. MR-EMR combination process is a method that is able to improve demerits of MR(metallothermic reduction) and EMR(electronically mediated reaction) process. This study examined the characteristics of powder with the amount of reductant excess using TaF as feed materials, Na as a reductant and KCl/KF as a diluent. In addition, this study examined acid treatment that affect the high purification of powder. The impurities contained in powder was removed in various conditions of acid treatment. The total charge passed through external circuit and average particle size(FSSS) were increased with increasing amount of sodium excess. The proportion of fine particle(-325mesh) was decreased with increasing amount of sodium excess. The yield was improved from 70% to 76% with increasing amount of sodium excess. Considering the impurities, charge, morphology, particle size and yield, an amount of sodium excess of 10wt% were found to be optimum conditions for MR-EMR combination process.s.
4,000원
10.
2004.08 구독 인증기관 무료, 개인회원 유료
In the study, a hybrid constitutive model for densification of metallic powders was applied to cold isostatic pressing. The model is based on a pressure-dependent plasticity model for porous materials combined with a dislocation density-based viscoplastic constitutive model considering microstructural features such as grain size and inter-particle spacing. Comparison of experiment and calculated results of microscale and nanoscale Cu powders was made. This theoretical approach is useful for powder densification analysis of various powder sizes, deformation routes and powder processing methods.
4,000원
11.
2004.08 구독 인증기관 무료, 개인회원 유료
최근 들어 노트북, 통신장비 등 고성능 전자기기들은 산업수요의 특성상 소형화와 경량화 추세가 가속화되고 있으며, 컴퓨터, 냉장고, 에어컨 등 가전제품에 있어서도 안정한 전류공급 및 역률의 향상이 의무화되고 있다. 따라서 내부에 사용되는 부품의 고주파화, 고효율화, 손실감소를 위한 고성능 연자성코아 (그림 1. 참조) 개발의 필요성이 한층 증대되고있는 실정이다. (중략)
3,000원