간행물

한국분말야금학회지 KCI 등재 Journal of Korean Powder Metallurgy Institute

권호리스트/논문검색
이 간행물 논문 검색

권호

Vol. 20 No. 1 (2013년 2월) 11

1.
2013.02 구독 인증기관 무료, 개인회원 유료
The key concept of nanopowder agglomerate sintering (NAS) is to enhance material transport by controlling the powder interface volume of nanopowder agglomerates. Using this concept, we developed a new approach to full density processing for the fabrication of pure iron nanomaterial using Fe nanopowder agglomerates from oxide powders. Full density processing of pure iron nanopowders was introduced in which the powder interface volume is manipulated in order to control the densification process and its corresponding microstructures. The full density sintering behavior of Fe nanopowders optimally size-controlled by wet-milling treatment was discussed in terms of densification process and microstructures.
4,000원
2.
2013.02 구독 인증기관 무료, 개인회원 유료
The effect of particle size distribution on green and sintered properties of Fe-Cr-Mo prealloy powder was investigated in this study. For the study, prealloyed Fe-Cr-Mo powders with different particle sizes were mixed as various ratios and cold compacted at various pressure and sintered at for 30 min, atmosphere in the continuous sintering furnace. The results shows that the powders with large particle size distribution have high compressibility and low ejection force. However the green strength are much less than those with small particle size distribution. Tensile prperties of the sintered specimes with large particles size also have high strength and elongation.
4,000원
3.
2013.02 구독 인증기관 무료, 개인회원 유료
In the present study, we systematically investigated the effect of Mn addition on nitrogenation behavior and magnetic properties of Sm-Fe powders produced by reduction-diffusion process. Alloy powders with only single phase were successfully produced by the reduction-diffusion process. The coercivity of powder rapidly increased during nitrogenation and reached the maximum of 637 Oe after 16 hours. After further nitrogenation, it decreased. In contrast, the coercivity of powder gradually increased during nitrogenation for 24 hours. The coercivity of powder was higher than that of powder at the same condition of nitrogenation. It was considered that the Mn addition facilitates the nitrogenation of powder and enhances the coercivity.
4,000원
4.
2013.02 구독 인증기관 무료, 개인회원 유료
Ru films were successfully prepared by plasma-enhanced atomic layer deposition (PEALD) using and plasma. To optimize Ru PEALD process, the effect of growth temperature, plasma power and plasma time on the growth rate and preferred orientation of the deposited film was systemically investigated. At a growth temperature of and plasma power of 100W, the saturated growth rate of 0.038 nm/cycle was obtained on the flat /Si substrate when the and plasma time was 7 and 10 sec, respectively. When the growth temperature was decreased, however, an increased plasma time was required to obtain a saturated growth rate of 0.038 nm/cycle. Also, plasma power higher than 40 W was required to obtain a saturated growth rate of 0.038 nm/cycle even at a growth temperature of . However, (002) preferred orientation of Ru film was only observed at higher plasma power than 100W. Moreover, the saturation condition obtained on the flat /Si substrate resulted in poor step coverage of Ru on the trench pattern with an aspect ratio of 8:1, and longer plasma time improved the step coverage.
4,000원
5.
2013.02 구독 인증기관 무료, 개인회원 유료
The effect of carrier gases (He, ) on the properties of Ti coating layers were investigated to manufacture high-density Ti coating layers. Cold spray coating layers manufactured using He gas had denser and more homogenous structures than those using gas. The He gas coating layers showed porosity value of 0.02% and hardness value of Hv 229.1, indicating more excellent properties than the porosity and hardness of gas coating layers. Bond strengths were examined, and coating layers manufactured using He recorded a value of 74.3 MPa; those manufactured using gas had a value of 64.6 MPa. The aforementioned results were associated with the fact that, when coating layers were manufactured using He gas, the powder could be easily deposited because of its high particle impact velocity. When Ti coating layers were manufactured by the cold spray process, He carrier gas was more suitable than gas for manufacturing excellent coating layers.
4,000원
6.
2013.02 구독 인증기관 무료, 개인회원 유료
A bulk metallic glass-forming alloy, metallic glass powders was used for good commercial availability and good formability in supercooled liquid region. In this study, the Ni-based metallic glass was synthesized using by high pressure gas atomized metallic glass powders. In order to create a bulk metallic glass sample, the metallic glass powders with ball-milled Ni-based amorphous powder with 40%vol brass powder and Cu powder for 20 hours. The composite specimens were prepared by Spark Plasma Sintering for the precursor. The SPS was performed at supercooled liquid region of Ni-based metallic glass. The amorphous structure of the final sample was characterized by SEM, X-ray diffraction and DSC analysis.
3,000원
7.
2013.02 구독 인증기관 무료, 개인회원 유료
phosphor powders were synthesized using a seed (average particle size: 5 ) by the polymer solution route. PVA solution was added to the sol precursors consisting of the seed powder and metal nitrate salts for homogeneous mixing in atomic scale. All dried precursor gels were calcined at and then heated at in atmosphere. The final powders were characterized by using XRD, SEM, PSA, PL and PKG test. All synthesized powders were crystallized to YAG phase without intermediate phases of YAM or YAP. The phosphor properties and morphologies of the synthesized powders were strongly dependent on the PVA content. Finally, the synthesized phosphor powder heated at , which is prepared from 12:1 PVA content and has an average particle size of 15 , showed similar phosphor properties to a commercial phosphor powder.
4,000원
8.
2013.02 구독 인증기관 무료, 개인회원 유료
The extraction of metallic pure vanadium powder from raw oxide has been tried by Mg-reduction. In first stage, powders as initial raw material was reduced by hydrogen gas into phase. powder was reduced in next stage by magnesium gas at 1,073K for 24 hours. After reduction reaction, the MgO component mixed with reduced vanadium powder were dissolved and removed fully in 10% HCl solution for 5 hours at room temperature. The oxygen content and particle size of finally produced vanadium powders were 0.84 wt% and 1 , respectively
4,000원
9.
2013.02 구독 인증기관 무료, 개인회원 유료
A study of oxidation kinetic of Fe-36Ni alloy has been investigated using thermogravimetric apparatus (TGA) in an attempt to define the basic mechanism over a range of temperature of 400 to and finally to fabricate its powder. The oxidation rate was increased with increasing temperature and oxidation behavior of the alloy followed a parabolic rate law at elevated temperature. Temperature dependence of the reaction rate was determined with Arrhenius-type equation and activation energy was calculated to be 106.49 kJ/mol. Based on the kinetic data and micro-structure examination, oxidation mechanism was revealed that iron ions and electrons might migrate outward along grain boundaries and oxygen anion diffused inward through a spinel structure, .
4,000원
10.
2013.02 구독 인증기관 무료, 개인회원 유료
Fe-TiC composite powder was fabricated via two steps. The first step was a high-energy milling of FeO and carbon powders followed by heat treatment for reduction to obtain a (Fe+C) powder mixture. The optimal condition for high-energy milling was 500 rpm for 1h, which had been determined by a series of preliminary experiment. Reduction heat-treatment was carried out at for 1h in flowing argon gas atmosphere. Reduced powder mixture was investigated by X-ray Diffraction (XRD), Field Emission-Scanning Electron Microscopy (FE-SEM) and Laser Particle Size Analyser (LPSA). The second step was a high-energy milling of (Fe+C) powder mixture and additional powder, and subsequent in-situ synthesis of TiC particulate in Fe matrix through a reaction of carbon and Ti. High-energy milling was carried out at 500 rpm for 1 h. Heat treatment for reaction synthesis was carried out at for 1 h in flowing argon gas atmosphere. X-ray diffraction (XRD) results of the fabricated Fe-TiC composite powder showed that only TiC and Fe phases exist. Results from FE-SEM observation and Energy-Dispersive X-ray Spectros-copy (EDS) revealed that TiC phase exists uniformly dispersed in the Fe matrix in a form of particulate with a size of submicron.
4,000원