간행물
한국분말야금학회지 KCI 등재 Journal of Korean Powder Metallurgy Institute
- 발행기관 한국분말재료학회(구 한국분말야금학회)
- 자료유형 학술지
- 간기 격월간
- ISSN 1225-7591 (Print)2287-8173 (Online)
- 수록기간 1994 ~ 2024
- 주제분류 공학 > 금속공학 공학 분류의 다른 간행물
- 십진분류KDC 559DDC 629
권호리스트/논문검색
Vol. 10 No. 1 (2003년 2월) 12건
1.
2003.02
구독 인증기관 무료, 개인회원 유료
Nano-sized WC powders were synthesized by vapor phase reaction using the precusor of tungsten ethoxide under helium and hydrogen atmosphere. The phases of the powder were varied with reaction Bone and gas flow rate. The powder size was about 30nm in diameter, and the tungsten carbide powder was coated by carbon layer. The synthesis of nano-sized WC powders was promoted as the hydrogen gas flow rate became higher. Inversely, tungsten oxide was formed by increasing the flow rate of helium gas. The synthesized powders were analyzed by XRD, FE-SEM, carbon analyzer etc.
4,000원
2.
2003.02
구독 인증기관 무료, 개인회원 유료
The purpose of the present study is to investigate the method decreasing debinding time as well as lowering operation condition than pure supercritical debinding by using cosolvent or binary mixture of propane + . First method is to add cosolvent, such as n-hexane, DCM, methanol, 1-butanol, in supercritical . In case of adding cosolvent, we were found the addition of non-polar cosolvent (n-hexane) improves dramatically the binder removal rate (more than 2 times) compared with pure supercritical debinding, second method is to use mixture of supercritical propane + , as solvent. In case of using mixture of supercritical propane + , the rate of debinding speeded up with increasing of pressure and concentration of propane at 348.15 K. It was found that addition of cosolvent (e.g., n-hexane, DCM) and binary mixture propane + for supercritical solvent remarkably improved binder removal rate for the paraffin wax-based binder system, in comparison with using pure supercritical .
4,000원
3.
2003.02
구독 인증기관 무료, 개인회원 유료
Hybrid ceramic particle reinforced 6061 and 5083 Al composite powders were prepared by the combination of twin rolling and stone mill crushing process, followed by consolidating processes of cold compaction, degassing and hot extrusion. The composite bar consists of lamellar structure of ceramic particle rich area and matrix area, in which the hybrid was decomposed into each TiC of about and particles of about in diameter. It also found that fine precipitates of about 30 nm were embedded in the matrix, which have grains of about 3 . Higher UTS was measured at the 5083 composite bar compared to the conventionally fabricated composite, due to again refinement effect by the rapid solidification. No particle was shown to form in the interface between the matrix and reinforcement, whereas carbon was diffused into the matrix.
4,000원
4.
2003.02
구독 인증기관 무료, 개인회원 유료
The Sn - graphite composites were prepared by chemical encapsulation method for anode materials in Li-ion batteries. EDS and XRD analysis confirmed the presence of Sn in the graphite structure. Cyclic voltammometry (CV) measurement shows extra reduction and oxidation peaks, which might to be related to the formations of alloy compounds. Graphite-tin composite electrodes demonstrated higher Lithium storage capacities than graphite electrodes. Due to the nature of fine Sn particles on graphite surface, the graphite-tin composite electrodes have shown a good cycle properties.
4,000원
5.
2003.02
구독 인증기관 무료, 개인회원 유료
Al-l4wt.%Ni-l4wt.% Mm(Mm=misch metal) alloy powders rapidly solidified by the gas atomization method were subjected to mechanical milling(MM). The morphology, microstructure and hardness of the powders were investigated as a function of milling time using scanning electron microscopy(SEM), transmission electron microscopy(TEM) and Vickers microhardness tester. Microstructural evolution in gas-atomized Al-l4wt.%Ni-l4wt.% Mm(Mm=misch metal) alloy powders was studied during mechanical milling. It was noted that the as-solidified particle size of decreases during the first 48 hours and then increases up to 72 hours of milling due to cold bonding and subsequently there was continuous refinement to on milling to 200 hours. Two microstructurally different zones, Zone A, which is fine microstructure area and Zone B, which has the structure of the as-solidified powder, were observed. The average thickness of the Zone A layer increased from about 10 to in the powder milled for 24 hours. Increasing the milling time to 72 hours resulted in the formation of a thicker and more uniform Zone A layer, whose thickness increased to about . The TEM micrograph of ball milled powder for 200 hours shows formation of nano-particles, less than 20 nm in size, embedded in an Al matrix.
4,000원
6.
2003.02
구독 인증기관 무료, 개인회원 유료
Porous TiNi bodies were produced by Self-propagating High-temperature Synthesis (SHS) method from a powder mixture of Ti and Ni. Porosity, pore size and structure, mechanical property, and transformation temperature of TiNi product were investigated. The average porosity and pore size of produced porous TiNi body are 63% and , respectively. XRD analysis showed that the major phase of produced TiNi body is B2 phase. Its average fracture strength and elastic modulus measured under dry condition were MPa and GPa, respectively. It could be strained up to 7.3 %. The transformation temperatures determined by DSC showed the temperature of and temperature of .
4,000원
7.
2003.02
구독 인증기관 무료, 개인회원 유료
Sintering behavior of 2xxx series Al alloy was investigated to obtain full densification and sound microstructure. The commercial 2xxx series Al alloy powder. AMB2712, was used as a starting powder. The mixing powder was characterized by using particle size analyzer, SEM and XRD. The optimum compacting pressure was 200 MPa, which was the starting point of the "homogeneous deformation" stage. The powder compacts were sintered at after burn-off process at . Swelling phenomenon caused by transient liquid phase sintering was observed below of sintering temperature. At , sintering density was increased by effect of remained liquid phase. Further densification was not observed above . Therefore, it was determined that the optimum sintering temperature of AMB2712 powder was .C.
4,000원
8.
2003.02
구독 인증기관 무료, 개인회원 유료
Lee et al. reported that a mixture of Cu and Ta, the combination of which is characterized by a positive heat of mixing, of +2 kJ/㏖, can be amorphized by mechanical alloying(MA). It is our aim to investigate to what extent the MA is capable of producing a non-equilibrium phase with increasing the heat of mixing. The system chosen is the binary with =+19 kJ/㏖. The mechanical alloying was carried out using a Fritsch P-5 planetary mill under Ar gas atmosphere. The vial and balls are made of Cu containing 1.8-2.0 wt.%Be to avoid contaminations arising mainly from Fe when steel balls and vial are used. The MA powders were characterized by the X-ray diffraction, EXAFS and thermal analysis. We conclude that two phase mixture of nanocrystalline fcc-Cu and bcc-Mo with grain size of 10 nm is formed by the ball-milling for a 3:7 mixture of pure Cu and Mo, the evidence for which has been deduced from the thermodynamic and structural analysis based on the DSC, X-ray diffraction and EXAFS spectra.
4,000원
9.
2003.02
구독 인증기관 무료, 개인회원 유료
Effect of the Process Parameters on the Fe Nano Powder Formation in the Plasma Arc Discharge Process
To investigate the effect of the parameters of the plasma arc discharge process on the particle formation and particle characteristics of the iron nano powder, the chamber pressure, input current and the hydrogen volume fraction in the powder synthesis atmosphere were changed. The particle size and phase structure of the synthesized iron powder were studied using the FE-SEM, FE-TEM and XRD. The synthesized iron powder particle had a core-shell structure composed of the crystalline -Fe in the core and the crystalline in the shell. The powder generation rate and particle size mainly depended on the hydrogen volume fraction in the powder synthesis atmosphere. The particle size increased simultaneously with increasing the hydrogen volume fraction from 10% to 50%, and it ranged from about 45nm to 130 nm.
4,000원
10.
2003.02
구독 인증기관 무료, 개인회원 유료
The effect of bedding on the microstructure of added with ultra-fine SiC was investigated. The bedding and the addition of ultra-fine SiC effectively inhibited grain growth of matrix grain. The microstructures of the specimens sintered with bedding powder consisted of fine-grains as compared with the specimens sintered without bedding powder. In addition, the grain size and the difference of grain size between the specimens sintered with bedding and without bedding was reduced with increasing SiC content. Some ultra-fine SiC particles were trapped in the grains growed. The number of SiC particles trapped in the grains increased with increasing the grain growth. When ultra-fine SiC particles were added in the ceramics, the strength was improved but the toughness was decreased, which was considered to be resulted from the decrease of the grain size
4,000원
11.
2003.02
구독 인증기관 무료, 개인회원 유료
3,000원
12.
2003.02
구독 인증기관 무료, 개인회원 유료
3,000원
