In this study, QA/QC (quality control/quality assurance) data of reduced sulfur compounds from several institutes were obtained and compared based on the Korean standard method for off-odor. From the results, attempts were made to optimize the analytical conditions and improve the measurement reliability of reduced sulfur compounds analyses from detailed CF/TD and GC/PFPD information. Analysis results (minimum detection limit, precision, recovery rate) of reduced sulfur compounds based on the each analytical condition corresponded with the Korean standard methods for off-odor. Therefore, we expect that we could execute the exact analysis if we use the analytical condition of CF/TD and GC/PFPD in this study