In order to investigate functional groups on the surface of Multi-walled Carbon Nanotubes (MWCNTs) induced by oxyfluorination, XPS (X-ray photoelectron spectroscopy) analysis was carried out. All core level spectra of MWCNTs were deconvoluted to several Pseudo-Voigt functions (sum of Gaussian-Lorentzian functions). Both O1s and F1s binding energy of oxyfluorinated MWCNTs shifted high value as increment of fluorine mixing ratio. The carbon-fluorine covalent bonding concentration increased as increment of fluorine mixing ratio. The shape and intensity of OF10-MWCNTs are similar with those of as-received MWCNTs. However, the intensity and binding energies of main peak position of OF20-MWCNTs and OF30-MWCNTs were dramatically increased by oxyfluorination.
The purpose of this experimental study is to investigate the application of materials of construction with MWNT and TiO2. high performance nano MWNT-TiO2 carrier was fabricated by sol-gel method and performance analyzed by XRD and SEM. As a result, high performance nano MWNT-TiO2 carrier was no significant differences in coating state, crystallinity and microstructure.
The purpose of this experimental study is to investigate the application of materials of construction with MWNT and TiO2. high performance nano MWNT-TiO2 carrier was fabricated by sol-gel method and performance analyzed by XRD and SEM. As a result, high performance nano MWNT-TiO2 carrier was no significant differences in coating state, crystallinity and microstructure.