The malodor as the sense pollutions is rising to surface with a new environmental matter. Especially, malodor"s appeal is increasing steadily from a residential area of the industrial complex. The odor characteristic and odor active compounds of industries should be identified to solve this problem. The dye company was selected as a sample among the industries. Air samples of the dye company were sampled with polyester aluminum bag and it was analyzed by GC/FID/O and GC/MS. The feature of the complex odor was ironing, sour and burnt smell. The odor active compounds of individual odor which contribute these smell were mainly 2-ethyl-hexanal, octanal, 2-ethyl-1-hexanol and nonanal. This study will help odor problem of industries to solve effectively.