This study examines the role of the nano- and micro-particle ratio in dispersion stability and mechanical properties of composite resins for SLA(stereolithography) 3D printing technology. VTES(vinyltriethoxysilane)-coated ZrO2 ceramic particles with different nano- and micro-particle ratios are prepared by a hydrolysis and condensation reaction and then dispersed in commercial photopolymer (High-temp) based on interpenetrating networks(IPNs). The coating characteristics of VTES-coated ZrO2 particles are observed by FE-TEM and FT-IR. The rheological properties of VTEScoated ZrO2/High-temp composite solution with different particle ratios are investigated by rheometer, and the dispersion properties of the composite solution are confirmed by relaxation NMR and Turbiscan. The mechanical properties of 3Dprinted objects are measured by a tensile test and nanoindenter. To investigate the aggregation and dispersion properties of VTES-coated ZrO2 ceramic particles with different particle ratios, we observe the cross-sectional images of 3D printed objects using FE-SEM. The 3D printed objects of the composite solution with nano-particles of 80 % demonstrate improved mechanical characteristics.

Many investments and works being continued to preserve green ocean in each countries of the world. Especial1y, the researches on the prevention of marine oil pollution being strengthened. It is not easy to disclose sludge oils that were produced necessarily in the ships operation, so that they are transferred to shore treating facility after collected inside the ship＇s sludge tank mostly. However, this shore transferring method is not only costly and time consuming but also entails risk of oil pollution. In this regard, it will be the best way to manage the sludge oils inside ship itself. The purpose of this study is to device an ultrasonic breaking systems which recycle the sludge oil from ships into usable oil to be burnt. In this paper, the first place, matrix structures of sludge fuel oil(SFO) and sludge lubricating oil(SLO) with the irradiation time for ultrasonic vibrator were interpreted. And, erosion damage for vibrator horn tip which is one of important part of ultrasonic breaking systems was examined under such an environment of the sludge oils. The material for horn tip is being made of SS41 steel and its erosion phase was investigated with variation of the vibration amplitude of 50μm and 24μm as well as the change of temperature in the oil environments. It is suggested that the experimental results can be helpful to the development of sludge oil disposing systems for the vessel.

Ni기 초합금인 B1914로 다결정, 방향성 및 단결정을 제조하여, 상온과 고온에서 이들 결정종류에 따른 변형을 관찰하였다. 이들 결정을 제작하기 위하여 진공 주조로에서 냉각속도와 온도구배를 제어하였으며, 제작된 봉상 시편들은 2단계의 진공열처리를 하고 아르곤가스로 급냉하였다. 동일한 모합금인 B1914로 제조된 결정들은 결정종류에 따라서 뚜렷한 변형(stress-strain)을 나타내었다. 즉, 항복강도와 인장강도는 다결정, 방향성 및 단결정 순으로 뚜렷이 증가하였다. 또한 600˚C에서 모든 결정들은 γ'의 강화효과로 인해서 가장 높은 741-816MPa의 항복강도를 나타내었으며, 인장강도는 1005-1139MPa이었다.