본 연구는 꼬막 패각 잔골재와 PP 폐어망 섬유를 혼입한 자원순환 콘크리트의 역학적 성능과 계면 변화 영역에서의 미세구조 특성 을 분석하였다. 패각 잔골재와 폐어망 섬유를 적절한 방법으로 전처리하고 자원화를 고려하여 3D 프린팅 콘크리트 배합을 선정해 콘 크리트 시편을 제작하였다. 제작된 시편은 KS L ISO 679 규정에 따라 압축강도와 휨강도를 측정하였고, BSE 모드를 이용한 SEM 이 미지 촬영을 통해 미세구조를 분석하였다. SEM 이미지는 히스토그램 및 형상 기반 상 분리 방법, 그리고 계면 변화 영역의 픽셀값 차 이를 활용하여 이미지를 분리하고 미세구조를 분석하였다. 역학적 성능을 확인하기 위해 PP 섬유를 0.0%, 0.5%, 1.0vol.% 혼입한 시 편의 압축강도와 휨강도를 측정한 결과, PP 섬유 0.5vol.% 혼입 시 섬유 브릿징 효과로 인해 가장 높은 압축 및 휨강도가 나타났다. SEM 이미지 분석 결과, 일반 잔골재와 바인더 계면보다 패각 잔골재와 바인더 계면에서 더 큰 직경의 공극이 관찰되었으며, PP 섬유 와 바인더 계면에서는 상대적으로 작은 공극이 형성됨을 확인하였다. 이를 바탕으로 미세구조 분석 결과와 역학적 성능 간의 상관관 계를 규명하였다.

Copper-coated carbon fibers have excellent conductivity and mechanical properties, making them a promising new lightweight functional material. One of the main challenges to their development is the poor affinity between carbon fiber and metals. This paper selects different carbon fibers for copper electroplating experiments to study the effect of carbon fiber properties on the interface bonding performance between the copper plating layer and carbon fibers. It has been found that the interfacial bonding performance between copper and carbon fiber is related to the degree of graphitization of carbon fiber. The lower the degree of graphitization of carbon fiber, the smaller the proportion of carbon atoms with sp2 hybrid structure in carbon fiber, the stronger the interfacial bonding ability between carbon fiber and copper coating. Therefore, carbon fiber with lower graphitization degree is conducive to reducing the falling off rate of copper coating and improving the quality of copper coating, and the conductivity of copper-plated carbon fibers increases with the decrease of graphitization degree of carbon fibers. The conductivity of copper-plated carbon fibers increases by more than six times when the graphitization degree of carbon fibers decreases by 23.9%. This work provides some benchmark importance for the preparation of highquality copper-plated carbon fibers.

In this work, the trend in the performance of carbon fiber (CF) and its composite during self-polymerization of polydopamine (PDA) at carbon fiber surface was investigated by varying the self-polymerization time of dopamine in an aqueous solution. Research has shown that the PDA coating elevated the surface roughness and polarity of the inert fiber. The tensile strength of single carbon fiber was significantly improved, especially after 9 h of polydopamine self-polymerization, increasing by 18.64% compared with that of desized carbon fiber. Moreover, the interlaminar shear strength (ILSS) of CF-PDA9-based composites was 35.06% higher than that of desized CF-based composites. This research will provide a deep insight into the thickness and activated ingredients of dopamine oxidation and self-polymerization on interfacial compatibility of carbon fiber/epoxy resin composites.

This study investigated the growth behavior and characteristics of compounds formed at the interface between a liquid Al-Si-Cu alloy and solid cast iron. Through microstructural analyses, it was observed that various AlFe and AlFeSi phases are formed at the interface, and the relative proportion of each phase changes when small amounts of strontium are added to the Al alloy. The results of the microstructural analysis indicate that the primary phases of the interfacial compounds in the Al-Si-Cu base alloy are Al8Fe2Si and Al4.5FeSi. However, in the Sr-added alloys, significant amounts of binary AlFe intermetallic compounds such as Al5Fe2 and Al13Fe4 formed, in addition to the AlFeSi phases. The inclusion of Sr has a slight diminishing effect on the rate at which the interfacial compounds layer thickens during the time the liquid Al alloy is in contact with the cast iron. The study also discusses the nano-indentation hardness and micro-hardness of the interfacial phases.