In this study, the surface characteristics—including roughness, oxide layer thickness, and composition—of the electropolished layer on STS316L steel tubes subjected to double melting via the VIM/VAR process were investigated after exposure to Cl2 gas. The tubes were exposed to Cl2 gas for 1 to 13 d to simulate semiconductor conditions. Surface roughness increased with Cl2 exposure time, showing values of 0.01, 0.04, 0.04 and 0.03 μm after 0, 1, 5 and 9 d, respectively. At the same time, the oxide layer thickness on EPed STS316L, which was initially 8.2 nm, decreased to 3.18, 2.58 after 1, 5 d of Cl2 exposure, approaching the initial thickness of 2.38 nm observed on non-EPed STS316L. After 9 d, the thickness further decreased to 0.51 nm, with no significant change was observed thereafter. Before Cl2 exposure, the CrO/FeO ratio was 2.26. After 1, 5, and 9 d of exposure, the ratio decreased to 2.06, 1.75, and 1.27, respectively. In addition, the penetration depth of Cl into the oxide layer increased with longer exposure time. These results suggest that the formation of chromium chlorides led to the breakdown of the stable Cr2O3 layer.

As a safety device, a rupture disc are used to control pressure to minimize the explosion risk once the internal pressure of high pressure equipment exceeds a critical level. In this paper, optimization method was developed to secure optimal design of domed Rupture disks. The parameter analysis was performed through design of experiment to parameter of Rupture disk made of AISI 316.The Diameter, Thickness and Hight of Rupture disk were selected as design parameters for design parameter analysis. The results of parameter analysis revealed that the Diameter, thickness and hight were burst pressure-sensitive design parameters. Based on the valid performance factors, a regression equation to predict its performance was deducted and using the equation, an optimal design. And a sample model was fabricated, followed by burst pressure testing, after optimal design and analytical verification. In this research, it is verified that the optimal design method and the credibility of the analysis of this study is deemed very high. Furthermore, utilizing this mechanism would inspect the effect of the design parameter performance and increase the credibility and efficiency of a design.

This study investigates the directional recrystallization behavior of Ni based oxide dispersion strengthened (ODS) alloy according to the zone annealing velocity. The zone annealing temperature is set as 1390oC, while the zone velocities are set as 2.5, 4, 6, and 10 cm/h, respectively. The initial microstructure observation of the as-extruded sample shows equiaxed grains of random orientation, with an average grain size of 530 nm. On the other hand, the zone annealed samples show a large deviation in grain size depending on the zone velocities. In particular, grains with a size of several millimeters are observed at 2.5-cm/h zone velocity. It is also found that the preferred orientation varies with the zone annealing velocity. On the basis of these results, this study discusses the role of zone velocities in the directional recrystallization of Ni base ODS alloy.

This study investigates the oxidation properties of Fe-14Cr ferritic oxide-dispersion-strengthened (ODS) steel at various high temperatures (900, 1000, and 1100°C for 24 h). The initial microstructure shows that no clear structural change occurs even under high-temperature heat treatment, and the average measured grain size is 0.4 and 1.1 μm for the as-fabricated and heat-treated specimens, respectively. Y–Ti–O nanoclusters 10–50 nm in size are observed. High-temperature oxidation results show that the weight increases by 0.27 and 0.29 mg/cm2 for the asfabricated and heat-treated (900°C) specimens, and by 0.47 and 0.50 mg/cm2 for the as-fabricated and heat-treated (1000°C) specimens, respectively. Further, after 24 h oxidation tests, the weight increases by 56.50 and 100.60 mg/cm2 for the as-fabricated and heat-treated (1100°C) specimens, respectively; the latter increase is approximately 100 times higher than that at 1000°C. Observation of the surface after the oxidation test shows that Cr2O3 is the main oxide on a specimen tested at 1000°C, whereas Fe2O3 and Fe3O4 phases also form on a specimen tested at 1100°C, where the weight increases rapidly. The high-temperature oxidation behavior of Fe-14Cr ODS steel is confirmed to be dominated by changes in the Cr2O3 layer and generation of Fe-based oxides through evaporation.