Metal-additive manufacturing techniques, such as selective laser sintering (SLS), are increasingly utilized for new biomaterials, such as cobalt-chrome (Co-Cr). In this study, Co-Cr gas-atomized powders are used as charge materials for the SLS process. The aim is to understand the consolidation of Co-Cr alloy powder and characterization of samples sintered using SLS under various conditions. The results clearly suggest that besides the matrix phase, the second phase, which is attributed to pores and oxidation particles, is observed in the sintered specimens. The as-built samples exhibit completely different microstructural features compared with the casting or wrought products reported in the literature. The microstructure reveals melt pools, which represent the characteristics of the scanning direction, in particular, or of the SLS conditions, in general. It also exposes extremely fine grain sizes inside the melt pools, resulting in an enhancement in the hardness of the as-built products. Thus, the hardness values of the samples prepared by SLS under all parameter conditions used in this study are evidently higher than those of the casting products.
A connection between pulse-periodical laser radiation power and stability of liquid-metal contacts between powder particles during selective laser sintering (SLS) is determined based on analysis solving the problem of stability of liquid column in the gravity and capillary forces field. On the grounds of obtained relationships the optimization of pulse-periodical laser radiation power and SLS-process duration is realized, that allows to produce voluminous powder porous materials with pre-determined physical and mechanical properties and surface geometry. Results of metallographic investigations of powder porous materials of titanium powder produced with technological regimes calculated by means of obtained relationships are given in the work
This paper investigates the characteristic of single-layered and multi-layered compacts made by selective laser sintering using titanium powder (TILOP45 and TILOP150, Sumitomo Titanium Corp.) There were few defects in smooth surface of laser sintered specimen in vacuum as compared to the laser sintered specimen in argon. Maximum tensile strength of singlelayered compact was about 200MPa. Multi-layered compacts show the density of around 75% and the adhesive bonding was not observed between layers, resulted in 70MPa of maximum bending strength and 50MPa of maximum tensile strength.
To investigate the effect of process parameters on selective laser sintering of Cu/polyamide mixed powder, Cu/polyamide mixed powder was sintered by selective laser with changing laser power and scanning speed. The properties of sintered body were evaluated by measuring the density and tensile strength, and analysis of XRD, FT-Raman and microstructure. With an increase in the laser power, the density and ultimate tensile strength of sintered Cu/polyamide body increase and then decrease. The maximum values of the density and ultimate tensile strength were decreased with increasing laser scanning speed. These changes were concerned with the difference of irradiation energy of laser into the powder layer. It was considered that the change of the mechanical property of the sintered body with irradiation energy of laser is due to the changes of amount of copper particle and property of polyamide.
A new low melting inorganic binder, monoclinic , has been developed for Selective Laser Sintering (SLS) of alumina powder by dehydration process of boron oxide powder in a vacuum oven at . It led to better green SLS parts and higher bend strength far green and fired parts compared to other inorganic binders such as aluminum and ammmonium phosphate. This appeared to be due to its low viscosity and better wettability of the alumina particle surface. A low density single phase ceramic, aluminum borate (), and multiphase ceramic composites, , were successfully developed by laser processing of alumina-monoclinic powder blends followed by post-thermal processing; both and have whisker-like grains. The physical and mechanical properties of these SLS-processed ceramic parts were correlated to the materials and processing parameters. Further densification of the ceramic composites was carried out by infiltration of colloidal silica, and chromic acid into these porous SLS parts followed by heat-treatment at high temperature (). The densities obtained after infiltration and subsequent firing were between 75 and 80% of the theoretical densities. The bend strengths are between 15 and 33 MPa.
단사정 HBO2 분막을 무기접착제로 이용하여 선택적 레이저 소결 기술을 적용시켜 알루미나-글래스 복합재료를 제조하였다. 만들어진 green SLS 시험편을 여러 온도에서 열처리하여 글래스-세라믹 복합재료를 얻었다. 글래스의 양이 많을수록 복합재료는 높은 밀도와 높은 굽힘강도를 보여주었다. 열처리 온도 900˚C에서 복합재료는 최대 밀도와 최대 강도를 나타낸다. 이것은 글래스의 낮은 점도로 인한 좋은 유동성 때문에 글래스의 재분배가 이루어졌기에 가능하다고 생각되어진다. 그리고 기공이 많은 열처리한 SLS 시험편에 콜로이드 실리카를 주입시켜 치밀화시켰다.
저용융점을 가진 새로운 무기 접착제인 단사정 HBO2가 알루미나 분말의 선택적 레이저 소결을 하기 위한 접착제로서 개발되었다. 이것을 이용하여 만들어진 green body는 현재까지 알루미나 분말의 선택적 레이저 소결을 위하여 개발된 다른 무기 접착제들인 알루미늄(Ai)과 Ammonium Phosphate(NH4H2PO4)을 이용하여 제조된 것에 비교하여 훨씬 높은 굽힘 강도를 가지고 있고 또 정밀도가 우수하였다. Green Body는 후속의 열처리를 받음으로써 저밀도 단상 세라믹 AI18B4O33과 다상 세라믹 복합재료 AI2O3-AI4B2O9으로 된다. AI18B4O33과 AI4B2O9의 결정립의 모양은 휘스커 구조와 유사하였다. 재료인자와 가공변수가 이 세라믹의 기계적 및 물리적 성질에 미치는 영향이 조사되었다.