We report the structural, morphological and magnetic properties of the Ni70Mn30 alloy prepared by Planetary Ball Mill method. Keeping the milling time constant for 30 h, the effect of different ball milling speeds on the synthesis and magnetic properties of the samples was thoroughly investigated. A remarkable variation in the morphology and average particle size was observed with the increase in milling speed. For the samples ball milled at 200 and 300 rpm, the average particle size and hence magnetization were decreased due to the increased lattice strain, distortion and surface effects which became prominent due to the increase in the thickness of the outer magnetically dead layer. For the samples ball milled at 400, 500 and 600 rpm however, the average particle size and hence magnetization were increased. This increased magnetization was attributed to the reduced surface area to volume ratio that ultimately led to the enhanced ferromagnetic interactions. The maximum saturation magnetization (75 emu/g at 1 T applied field) observed for the sample ball milled at 600 rpm and the low value of coercivity makes this material useful as soft magnetic material.

Fe-TiC composite powders are fabricated by planetary ball mill processing. Two kinds of powder mixtures are prepared from the starting materials of (a) (Fe, TiC) powders and (b) (Fe, TiH2, Carbon) powders. Milling speed (300, 500 and 700 rpm) and time (1, 2, and 3 h) are varied. For (Fe, TiH2, Carbon) powders, an in situ reaction synthesis of TiC after the planetary ball mill processing is added to obtain a homogeneous distribution of ultrafine TiC particulates in Fe matrix. Powder characteristics such as particle size, size distribution, shape, and mixing homogeneity are investigated. In case of (Fe, TiC) powder many coarse TiC particulates with size of several μm are unevenly distributed in Fe-matrix. The composite powder prepared from (Fe, TiH2, C) powder mixture showed a homogeneous dispersion of ulatrafine TiC particulates.

The study of grinding behavior characteristics on aluminum powders and carbon nano tubes (CNTs) has recently gained scientific interest due to their useful effect in enhancing advanced nano materials and components, which significantly improves the property of new mechatronics integrated materials and components. We performed a series of dry grinding experiments using a planetary ball mill to systematically investigate the grinding behavior during Al/CNTs nano composite fabrication. This study focused on a comparative study of the various experimental conditions at several variations of rotation speeds, grinding time and with and without CNTs. The results were monitored for the particle size distribution, median diameter, crystal structure from XRD pattern and particle morphology at a given grinding time. It was observed that pure aluminum powders agglomerated with low rotation speed and completely enhanced powder agglomeration. However, Al/CNTs composites were achieved at maximum experiment conditions (350 rpm, 60 min.) of this study by a mechanical alloy process for Al/CNTs mixed powders because the grinding behavior of Al/CNTs composite powder was affected by addition of CNTs. Indeed, the powder morphology and crystal size of the composite powders changed more by an increase of grinding time and rotation speed.

유성밀로써 사문석과 활석을 분쇄시 X-ray 회절분석, FT-IR, DSC-TG, 입도분석 그리고 SEM관찰 등을 이용하여 결정조직과 물리적 특성변화를 조사하였다. 분쇄기간이 증가함에 따라 사문석과 활석 원시료의 결정피크가 점처 감소하여 120분 이상 분쇄시 비정질상으로 변하였으며 이와 같은 변화는 마그네슘 결정 조직의 무질서에 기인한다. 분쇄된 시료에서 나타나는 흡열반응의 피크는 원시료보다 낮은 온도에서 관찰되었다. 또한 불규칙한 모양의 원시료는 분쇄처리를 실시함에 따라 구형의 응집체로 변하였다.