간행물

한국재료학회지 KCI 등재 SCOPUS Korean Journal of Materials Research

권호리스트/논문검색
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권호

제28권 제10호 (2018년 10월) 10

1.
2018.10 구독 인증기관 무료, 개인회원 유료
We report the structural, morphological and magnetic properties of the Ni70Mn30 alloy prepared by Planetary Ball Mill method. Keeping the milling time constant for 30 h, the effect of different ball milling speeds on the synthesis and magnetic properties of the samples was thoroughly investigated. A remarkable variation in the morphology and average particle size was observed with the increase in milling speed. For the samples ball milled at 200 and 300 rpm, the average particle size and hence magnetization were decreased due to the increased lattice strain, distortion and surface effects which became prominent due to the increase in the thickness of the outer magnetically dead layer. For the samples ball milled at 400, 500 and 600 rpm however, the average particle size and hence magnetization were increased. This increased magnetization was attributed to the reduced surface area to volume ratio that ultimately led to the enhanced ferromagnetic interactions. The maximum saturation magnetization (75 emu/g at 1 T applied field) observed for the sample ball milled at 600 rpm and the low value of coercivity makes this material useful as soft magnetic material.
4,000원
2.
2018.10 구독 인증기관 무료, 개인회원 유료
The passivation of AZ91D Mg alloys by plasma anodization requires deliberate choice of process parameters due to the presence of large amounts of structural defects. We study the dependence of pore formation, surface roughness and corrosion resistance on voltage by comparing the direct current (DC) mode and the pulse wave (pulse) mode in which anodization is performed. In the DC plasma anodization mode, the thickness of the electrolytic oxide film of the AZ91D alloy is uneven. In the pulse mode, the thickness is relatively uniform and the formed thin film has a three-layer structure. The pulse mode creates less roughness, uniform thickness and improved corrosion resistance. Thus, the change of power mode from DC to pulse at 150 V decreases the surface roughness (Ra) from 0.9 μm to 0.1 μm and increases the corrosion resistance in rating number (RN) from 5 to 9.5. Our study shows that an optimal oxide film can be obtained with a pulse voltage of 150 V, which produces an excellent coating on the AZ91D casting alloy.
4,000원
3.
2018.10 구독 인증기관 무료, 개인회원 유료
Visible and IR windows require a combination of high optical transparency and superior thermal and mechanical properties. Materials, fabrication and characterization of transparent ceramics for visible/IR windows are discussed in this review. The transparent polycrystalline Y2O3, Y2O3-MgO nanocomposites and MgAl2O4 spinel ceramics are fabricated by advanced ceramic processing and the use of special sintering technologies. Ceramic processing conditions for achieveing fully densified transparent ceramics are strongly dependent on the initial powder characteristics. In addition, appropriate use of sintering technologies, including vacuum sintering, hot-pressing and spark plasama sintering methods, results in outstanding thermal and mechanical properties as well as high optical transparency of the final products. Specifically, the elimination of light scattering factors, including residual pores, second phases and grain boundaries, is a key technique for improving the characteristics of the transparent ceramics. This paper discusses the current research issues related to synthesis methods and sintering processes for yttria-based transparent ceramics and MgAl2O4 spinel.
4,500원
4.
2018.10 구독 인증기관 무료, 개인회원 유료
Cu2ZnSn(S,Se)4 (CZTSSe) films were prepared on Mo coated soda lime glass substrates by sulfo-selenization of sputtered stacked Zn-Sn-Cu(CZT) precursor films. The precursor was dried in a capped state with aqueous NaOH solution. The CZT precursor films were sulfo-selenized in the S + Se vapor atmosphere. Sodium was doped during the sulfo-selenization treatment. The effect of sodium doping on the structural and electrical properties of the CZTSSe thin films were studied using FE-SEM(field-emission scanning electron microscopy), XRD(X-ray diffraction), XRF(X-ray fluorescence spectroscopy), dark current, SIMS(secondary ion mass spectrometry), conversion efficiency. The XRD, XRF, FE-SEM, Dark current, SIMS and cell efficiency results indicated that the properties of sulfo-selenized CZTSSe thin films were strongly related to the sodium doping. Further detailed analysis and discussion for effect of sodium doping on the properties CZTSSe thin films will be discussed.
4,000원
5.
2018.10 구독 인증기관 무료, 개인회원 유료
This study examines the effect of microstructural factors on the strength and deformability of ferrite-pearlite steels. Six kinds of ferrite-pearlite steel specimens are fabricated with the addition of different amounst of Mn and V and with varying the isothermal transformation temperature. The Mn steel specimen with a highest Mn content has the highest pearlite volume fraction because Mn addition inhibits the formation of ferrite. The V steel specimen with a highest V content has the finest ferrite grain size and lowest pearlite volume fraction because a large amount of ferrite forms in fine austenite grain boundaries that are generated by the pinning effect of many VC precipitates. On the other hand, the room-temperature tensile test results show that the V steel specimen has a longer yield point elongation than other specimens due to the highest ferrite volume fraction. The V specimen has the highest yield strength because of a larger amount of VC precipitates and grain refinement strengthening, while the Mn specimen has the highest tensile strength because the highest pearlite volume fraction largely enhances work hardening. Furthermore, the tensile strength increases with a higher transformation temperature because increasing the precipitate fraction with a higher transformation temperature improves work hardening. The results reveal that an increasing transformation temperature decreases the yield ratio. Meanwhile, the yield ratio decreases with an increasing ferrite grain size because ferrite grain size refinement largely increases the yield strength. However, the uniform elongation shows no significant changes of the microstructural factors.
4,000원
6.
2018.10 구독 인증기관 무료, 개인회원 유료
ZnO crystals with different morphologies are synthesized through thermal evaporation of the mixture of Zn and Cu powder in air at atmospheric pressure. ZnO crystals with wire shape are synthesized when the process is performed at 1,000 oC, while tetrapod-shaped ZnO crystals begin to form at 1,100 oC. The wire-shaped ZnO crystals form even at 1,000 oC, indicating that Cu acts as a reducing agent. As the temperature increases to 1,200 oC, a large quantity of tetrapod-shaped ZnO crystals form and their size also increases. In addition to the tetrapods, rod-shaped ZnO crystals are observed. The atomic ratio of Zn and O in the ZnO crystals is approximately 1:1 with an increasing process temperature from 1,000 oC to 1,200 oC. For the ZnO crystals synthesized at 1,000 oC, no luminescence spectrum is observed. A weak visible luminescence is detected for the ZnO crystals prepared at 1,100 oC. Ultraviolet and visible luminescence peaks with strong intensities are observed in the luminescence spectrum of the ZnO crystals formed at 1,200 oC.
4,000원
7.
2018.10 구독 인증기관 무료, 개인회원 유료
This study investigates the effect of fatigue stress on the damping capacity in a damaged Fe-22Mn-12Cr-3Ni-2Si- 4Co damping alloy under fatigue stress. α’ and ε-martensite forms by fatigue stress in the damaged Fe-22Mn-12Cr-3Ni-2Si- 4Co damping alloy under fatigue stress. The α’ and ε-martensite forms with the specific direction and surface relief, or they cross each other. With an increasing fatigue stress, the volume fraction of α’-martensite and ε-martensite increases. With an increasing fatigue stress, the damping capacity increases with an increase in the volume fraction of ε-martensite. The increase in the damping capacity in the damaged Fe-22Mn-12Cr-3Ni-2Si-4Co alloy under fatigue stress strongly affects the increase of ε-martensite formed by fatigue stress, but the damping capacity of the damaged Fe-22Mn-12Cr-3Ni-2Si-4Co damping alloy under fatigue stress is strongly controlled by a large amount of α’-martensite.
4,000원
8.
2018.10 구독 인증기관 무료, 개인회원 유료
ZnO micro/nanocrystals are formed by a vapor transport method. Mixtures of ZnO and TiO powders are used as the source materials. The TiO powder acts as a reducing agent to reduce the ZnO to Zn and plays an important role in the formation of ZnO micro/nanocrystals. The vapor transport process is carried out in air at atmospheric pressure. When the weight ratios of TiO to ZnO in the source material are lower than 1:2, no ZnO micro/nanocrystals are formed. However, when the ratios of TiO to ZnO in the source material are greater than 1:1, the ZnO crystals with one-dimensional wire morphology are formed. In the room temperature cathodoluminescence spectra of all the products, a strong ultraviolet emission centered at 380 nm is observed. As the ratio of TiO to ZnO in the source material increases from 1:2 to 1:1, the intensity ratio of ultraviolet to visible emission increases, suggesting that the crystallinity of the ZnO crystals is improved. Only the ultraviolet emission is observed for the ZnO crystals prepared using the source material with a TiO/ZnO ratio of 2:1.
4,000원
9.
2018.10 구독 인증기관 무료, 개인회원 유료
This study investigates the microstructural properties of CoCrFeMnNi high entropy alloy (HEA) oxynitride thin film. The HEA oxynitride thin film is grown by the magnetron sputtering method using nitrogen and oxygen gases. The grown CoCrFeMnNi HEA film shows a microstructure with nanocrystalline regions of 5~20 nm in the amorphous region, which is confirmed by high-resolution transmission electron microscopy (HR-TEM). From the TEM electron diffraction pattern analysis crystal structure is determined to be a face centered cubic (FCC) structure with a lattice constant of 0.491 nm, which is larger than that of CoCrFeMnNi HEA. The HEA oxynitride film shows a single phase in which constituting elements are distributed homogeneously as confirmed by element mapping using a Cs-corrected scanning TEM (STEM). Mechanical properties of the CoCrFeMnNi HEA oxynitride thin film are addressed by a nano indentation method, and a hardness of 8.13 GPa and a Young’s modulus of 157.3 GPa are obtained. The observed high hardness value is thought to be the result of hardening due to the nanocrystalline microstructure.
4,000원
10.
2018.10 구독 인증기관 무료, 개인회원 유료
To study the effects of graphite shape and the composite fabricating method on the mechanical properties of graphite/copper (Gr/Cu) composites, a copper composite using graphite flakes or graphite granules as reinforcing phases is fabricated using mechanical mixing or electroless plating method. The mechanical properties of the Gr/Cu composites are evaluated by compression tests, and the compressive strength and elongation of the Gr/Cu composites using graphite granules as a reinforcing phase are compared with those of Cu composites with graphite flakes as a reinforcing phase. The compressive yield strength or maximum strength of the Gr/Cu composites with graphite granules as a reinforcing phase is higher than that of the composites using graphite flakes as a reinforcing phase regardless of the alignment of graphite. The strength of the composite produced by the electroless plating method is higher than that of the composite material produced by the conventional mechanical mixing method regardless of the shape of the graphite. Using graphite granules as a reinforcing phase instead of graphite flakes improves the strength and elongation of the Gr/Cu composites in all directions, and reduces the difference in strength or elongation according to the direction.
4,000원