버즈풋 트레포일(Lotus corniculatus L.) 및 이탈리안 라이그라스(Lolium multiflotrum L.) 의 치사온도를 결정하기 위하여, 각각 "Au Dewey"와 국내 육성품종인 "화산 101호" 품종을시험재료조 하여 종자를 Petri dish에서 발아시켜 작은 화분에 10 개체씩 이식, 생장실에서 4주간 재배하였다. 45, 50 및에서 처리한 경우에는 60분간 처리했을 때에도 거의 식물체손상이 없었다. 분 처리에서는 잎이 약간 시든

Calcium phosphate powders were successfully synthesized by using re-cycled eggshell and phosphoric acid. The crystallization behavior and powder morphologies of the synthesized powders were dependent on the starting condition of the eggshell, the mixing ratio and method of the eggshell and phosphoric acid, and calcination temperature. In general, -tricalcium phosphate was stably synthesized at about 90 for 1h at each proper mixing ratio. And, the synthesized powders showed the similar microstructures to the morphology of original eggshell with uniform particle sizes. In this study, the calcium phosphate powders were synthesized with eggshell in various processing method. And their unique microstructures obtained from the eggshell were also. observed. The crystalline developments and microstructures of the synthesized powders were examined by X-ray diffractometer and scanning electron microscopy

Two-component ceramic (alumina-zirconia) composites were fabricated by a soft-solution process in which polyethylene glycol (PEG) was used as a polymeric carrier. Metal salts and PEG were dissolved in ethyl alcohol without any precipitation in 1:1 volume ratio of alumina and zirconia. In the non-aqueous system, the flammable solvent made explosive, exothermic reaction during drying process. The reaction resulted in formation of volume expanded, porous precursor powders by a vigorous decomposition of organic components in the precursor sol. The PEG content affected the grain size of sintered composites as well as the morphology of precursor powders. The difference of microstructure in sintered composite was attribute to the solubility and homogeneity of metal cations in precursor sol. At the optimum amount of the PEG polymer, the metal ions were dispersed effectively in solution and a homogeneous polymeric network was formed. It made less agglomerated particles in the precursor sol and affected on uniform grain size in sintered composite.

Mechanical alloying (MA) by high energy ball mill of Pure chromium Powders was carried out under the nitrogen gas atmosphere. Cr-N amorphous alloy powders have been produced through the solid-gas reaction subjected to MA. The atomic structure during amorphization process was observed by X-ray and neutron diffractions. An advantage of the neutron diffraction technique allows us to observe the local atomic structure surrounding a nitrogen atom. The coordination number of metal atoms around a N atom turns out to be 5.5 atoms. This implies that a nitrogen atom is located at both of centers of the tetrahedron and octahedron formed by metal atoms to stabilize an amorphous Cr-N structure. Also, we have revealed that a Cr-N amorphous alloy may produced from a mixture of pure Cr and Cr nitrides powders by solid-solid reaction during mechanical alloying.

In the present study, imbedded copper matrix powders have been successfully prepared from the () composite salt solution. The composite powders were formed by drying the solution at 200~40 in the hydrogen atmosphere. Photocatalytic characteristics was evaluated by detecting TOC (total organic carbon) amount with TOC analyzer (model 5000A Shimadzu Co). Phase analysis of composite powders was carried out by XRD, DSC and powder size was measured with TEM. The mean particle size of composite powders was about 100 nm and a few zinc and copper oxide phases was included. The reduction ratio of TOC amount was 60% by the composite powders under the UV irradiation for 8 hours

본 연구를 통하여 다하중 경우를 가지는 평면구조물의 위상을 도출하기 위한 최적화 프로그램을 개발하였다. 계산시간을 줄이고 실용적인 위상최적화를 수행하기 위하여 사절점 저차 유한요소를 이용하였다. 저차 유한요소를 사용하여 도출되는 위상에 나타나는 체크무늬현상을 제거하기 위해 여과절차를 도입하였다. 위상최적화를 수행하기 위하여 가등질화된 물질로 구조재를 표현하였고 물질을 재분배하기 위하여 최적정기준을 바탕으로 유도한 크기조절 알고리듬을 도입하였다. 개발된 프로그램을 이용하여 단하중 경우와 다하중 경우에 대한 평면 구조물의 위상을 도출하고 이를 비교분석하였다. 본 연구를 통하여 구조물의 실제적인 위상을 도출하기 위해서는 다하중 경우가 반드시 고려되어야 하는 것으로 나타났다.

Lee et al. reported that a mixture of Cu and Ta, the combination of which is characterized by a positive heat of mixing, of +2 kJ/㏖, can be amorphized by mechanical alloying(MA). It is our aim to investigate to what extent the MA is capable of producing a non-equilibrium phase with increasing the heat of mixing. The system chosen is the binary with =+19 kJ/㏖. The mechanical alloying was carried out using a Fritsch P-5 planetary mill under Ar gas atmosphere. The vial and balls are made of Cu containing 1.8-2.0 wt.%Be to avoid contaminations arising mainly from Fe when steel balls and vial are used. The MA powders were characterized by the X-ray diffraction, EXAFS and thermal analysis. We conclude that two phase mixture of nanocrystalline fcc-Cu and bcc-Mo with grain size of 10 nm is formed by the ball-milling for a 3:7 mixture of pure Cu and Mo, the evidence for which has been deduced from the thermodynamic and structural analysis based on the DSC, X-ray diffraction and EXAFS spectra.

본 논문은 8절점 고체요소를 이용하여 항공기 충돌에 의한 원전 격납건물의 동적 거동을 분석하고 그 결과를 기술하였다. 콘크리트의 재료적 특성을 표현하기 위하여 Drucker-Prager항복기준을 바탕으로 항복면과 파괴면을 형성하였다. 이때 항복면과 파괴면은 콘크리트의 소성변형이 누적되면 가변하는 것으로 가정하였다. 철근의 재료특성은 변형도에 의존적인 탄성/점소성모델을 이용하여 표현하였다. 표준고체요소의 성능저하를 방지하기 위하여 Hughes가 제시한 B bar법을 바탕으로 변형도-변위관계 행렬을 형성하였다. 동적 시간이력해석을 수행하기 위하여 안정적인 수렴성을 가지는 암시적인 Newmark법을 도입하였다. 마지막으로 시간이력해석을 통하여 콘크리트 균열변형도의 수준과 충돌하는 항공기의 종류에 따른 격납건물의 동적거동변화를 조사하고 이를 정량적으로 기술하였다.

본 연구는 체외에서 소 난포란유래의 배반포 생산에 있어서 배지 내에 첨가하는 외인성 고정질소 원으로써 아미노산과 FBS의 첨가효과를 검토하였다. 소 난포란의 체외성숙은 TCM-l99용액, 체외 수정은 Fer-TALP용액으로 행하였으며, 체외수정후 24시간째(day 1)의 수정난자를 체외배양에 제공하였다. 체외배양용 기초배지는 YS용액, 기초 배양법은 25개 난자/10 배지의 단순.미소적배양법을 이용하였다. 본 연구의 결과를 요약하면 다음과 같다. 1.

Pure and fine, two-component titanate powders (barium titanate, calcium titanate etc.) were synthesized by an ethylene glycol method. Titanium isopropoxide and other metal ionic salts were dissolved in liquid-type ethylene glycol without any precipitation. In non-aqueous system, the amount of ethylene glycol affected the solubility and homogeneity of metal cation sources in the solution. At the optimum amount of the polymer, the metal ions were dispersed effectively in solution and a homogeneous polymeric network was formed. Most of the synthesized powders had sub-micron or nano-size primary particles after calcination and the agglomerated calcined powders were easily ground by ball milling process. All synthesized titanate powders had stable crystallization behavior at low temperature and high specific surface area after ball milling. The crystallization behavior and the microstructures of the calcined powders were affected on the ethylene glycol content.