우리나라는 1983년에 절충교역 제도를 도입하여 국방 전력증강의 효율적 수단으로 활용하여 왔다. 그런데 절충교역은 계약체결이 획득기술에 대한 가치평가 결과를 근거로 이루어지기 때문에 국외업체와의 협상 등 업무과정상 지연될 가능성이 존재한다. 절충교역 계약체결이 지연되면 무기체계 구매사업이 늦어져 국방 전력증강에 심각한 악영향을 주게 된다. 따라서 본 연구에서는 절충교역 계약 과정, 특히 계약 소요기간에 영향을 미치는 요인들을 통계적으로 분석하여 소요기간을 결정하는 요인을 규명하고자 하였다. 영향 요인으로는 국외업체국적, 사업진행 형태 (경쟁/단독 입찰), 사업 특성 (최초/계속 사업), 최초 제안기술의 수, 국내무기체계 분야별 국방과학기술수준, 기본사업 규모 등 6개를 고려하였다. 가설 검증은 절충교역 계약이 체결된 25개 사업을 대상으로, 상관분석 및 다중회귀분석을 통하여 이루어졌다. 상관분석 결과에 의하면, 기본사업 규모, 최초 제안기술의 수, 사업 특성 등이 종속변수인 절충교역 계약 기간과 양의 상관관계를 갖고 있음을 알 수 있었다. 다중회귀분석 결과에서는 기본사업 규모와 사업진행 형태가 절충교역 계약 소요기간에 유의한 영향을 미치는 것으로 나타났다.

The reduction mechanism of the composite powders mixed with and CuO has been studied by using thermogravimetry (TG), X-ray diffraction, and microstructure analyses. The composite powders were made by simple Turbula mixing, spray drying, and ball-milling in a stainless steel jar with the ball to powder ratio of 32 to 1 at 80 rpm for 1 h without process controlling agents. It is observed that all the oxide composite powders are converted to W-coated Cu composite powder after reducing treatment under hydrogen atmosphere. For the formation mechanism of W-coated Cu composite powder, the sequential reduction steps are proposed as follows: CuO contained in the ball-milled composite powder is initially reduced to Cu at the temperature range from 20 to 30. Then, powder is reduced to W via W and W at higher temperature region. Finally, the gaseous phase of formed by reaction of with water vapour migrates to previously reduced Cu and deposits on it as W reduced by hydrogen. The proposed mechanism has been proved through the model experiment which was performed by using Cu plate and powder.der.

본 연구에서는 산화텅스텐() 분말을 이용하여 여러 금속 기판에 텅스텐 박막을 코팅하는 방법에 관한 연구를 수행하였다. 본 연구에서 언급되는 W 코팅은 Lee 등이 보고한 W, Cu 산화물을 이용하여 W-Cu 복합분말을 제조하는 것으로부터 아이디어가 출발되었으며, 본 연구의 결과는 기존의 6불화 텅스텐 가스() 를 열 분해하여 증착시키는 화학증착법(CVD: chemical vapor deposition)과 순수 텅스텐 target을 sputtering하여

The microstructure of the 1020 mild steel target in the region ahead of craters, made by colliding against Cu and W-Cu shaped-charge jets. has been investigated in the present work. The region ahead of the crater impacted by the Cu shaped-charge jet reveals grain refinement implying the formation of sub-grains, while that of W-Cu one leads to martensitic transformation indicating that the region was heated up to an austenitic region which was followed by rapid cooling. The pressure of W-Cu shaped-charge jet impacting against the target when calculated is higher than that of Cu one. The microhardness of the region ahead of the crater impacted by the W-Cu shaped-charge jet is also higher than that of the Cu one. The microstructure of W-Cu slug that remains inside of the crater depicts the occurrence of the remarkable elongation of W particles during the liner collapse. The microstructural evolution of the region ahead of the crater is discussed on the basis of the pressure dependency of the ferrite/austenite transformation in the steel.

The microstructure of the reagion of carters, created by Cu and W-Cu shaped charge jets, in a 1020 mild steel target has been intestiaged. The region ahead of the crater created by the Cu shaped charge jet, reveals dramatic grain refinement implying the occurrence of a dynamic recrystallization, while that of W-Cu one dose a martensitic transformation indicative of heating up to an austenitic region followed by rapid cooling.The impacting pressure calculated when the W-Cu shaped charge jet encounters the target is higher than that of the Cu one. The micro-hardness of the region ahead of the crater created by the W-Cu shaped charge jet is also higher than that of the Cu one. The microstructure of W-Cu slug remained in the inside of the craters depicts the occurrence of the remarkable elongation of W particles during the liner collaphse. From these results, the microstructural variation of the region ahead of the crater with Cu and W-Cu shaped charge jets is discussed in trems of the pressure dependency of the transformation region of ferrite and austenite phases.

Liquid phase sintering of 90W-6Ni-4Mn alloy has been investigated as functions of sintering atmosphere, heating rate, and reduction temperature. The present work accounts for the thermodynamic oxidatiodreduction reactions of constituent powders of W, Ni and Mn. By discounting these reactions, the previous investigations would obtain only the alloy with large pores and the lowered relative sintered density, by the liquid phase sintering under a dry hydrogen atmosphere. the sintering cycle consisted of a rapid heating to reduction temperatures under high purity nitrogen atmosphere, and holding for 4 hours and sintering at for 1 hour under a dry hydrogen gas. The relative density of the sintered alloy increased with increasing heating rate. As the reduction temperature increased, the relative density increased to the lm theotical density at the duction temture above . The mimsturcatre of sintered alloys has been analysed by a scanning election microscope. The sintered density was compared with those obtained from the other investigators. It was found that the reduction results in the lowered densification of 90W-6Ni-4Mn alloy. This is caused by the fact that reducing reactions of W and Ni oxides contained in W an Ni powders concomitantly leads to oxidizing reaction of Mn powder the oxidized Mn is hardly reduced at sintering temperature and thereby remains large pores in the alloy. It is concluded that the W-Ni-Mn alloy with full density can be obtained by the precise control of atmosphere, heating rate, and sintering temperature.