Y-type barium ferrite was prepared by the glass-ceramic method. Glasses with composition of were prepared, and the precipitation behavior of Y-type ferrite from the glass matrix was investigated by heating glass specimens at various temperature. which is a precursor of M-type ferrite was precipitated at about 813 K and an unknown compound, phase X, was precipitated at about 850 K. M-type ferrite and Y-type ferrite started to form at about 923 K and 1103 K, respectively. The formation of Y-type ferrite was int erpreted as the result of the reaction of M-type ferrite with a melt of phase X.
Y-type barium ferrite ( Me=Zn, Co, Cu) expected as an electromagnetic wave absorber were prepared by the glass-ceramic method. The glasses with composition of were prepared. Single-phase powders of Y type barium ferrite were obtained with the composition . The shape of Y-type crystals depended strongly on the heating temperature and changed from a plate-like hexagon to a complex polyhedron with increasing heating temperature. Correlation was recognized between saturation magnetization and crystal shape. Electromagnetic wave absorption characteristics was affected by the saturation magnetization and crystal shape.
WC-TiC-TaC binderless cemented carbide was oxidized under low partial pressure of oxygen (50ppm) at 873K for 1 to 20 h. Surface roughness was measured using atomic force microscope, and effect of TiC amount on oxidation behavior of the carbide was investigated. WC phase was oxidized more easily than WC-TiC-TaC solid solution phase. With an increase in TiC amount, WC-TiC-TaC phase increased and the oxidation resistance of the carbide increased.
The effect of TiC content on oxidation behavior of the sintered WC-TiC-TaC alloys with 2 mass% TaC and different TiC amounts of 3-45 mass% was investigated through oxidation tests in air at 973K. As a result of the tests, it was revealed that with increasing TiC content in the alloys, mass changes caused by oxidation and thickness of the scale decreased. Thus, it is considered that the main component of the scales changed gradually from to with increasing TiC content in the alloys, and oxygen diffusion through the scale to the alloys was inhibited gradually.
Images created by stack imaging spectral amplitudes based on the impact-echo (SIBIE) method are largely one-dimensional because a single frequency domain spectrum for waves reflected below a single point of impact is used to create them. The method has limitations for representing defects in a cross section of a concrete structural element using two-dimensional coordinates. This study focused on defect detection and visualization in a concrete structural element using multiple impacts and accumulated SIBIE. An impactor was used to induce energy at multiple points positioned at prescribed intervals along the structural element. A modified SIBIE method was applied to the collected data for each point and the modified SIBIE images were accumulated to generate one image (an accumulated SIBIE image). As a result, the defect positions could be represented in the cross section of the structural element using a two-dimensional coordinate system. And the method appears to improve upon existing methods to detect voids or other defects in concrete.