Fatigue crack growth rate tests were conducted as a function of temperature, dissolved hydrogen (DH) level, and frequency in a simulated PWR environment. Fatigue crack growth rates increased slightly with increasing temperature in air. However, the fatigue crack growth rate did not change with increasing temperature in PWR water conditions. The DH levels did not affect the measured crack growth rate under the given test conditions. At 316 oC, oxides were observed on the fatigue crack surface, where the size of the oxide particles was about 0.2 μm at 5 ppb. Fatigue crack growth rate increased slightly with decreasing frequency within the frequency range of 0.1 Hz and 10 Hz in PWR water conditions; however, crack growth rate increased considerably at 0.01 Hz. The decrease of the fatigue crack growth rate in PWR water condition is attributed to crack closure resulting from the formation of oxides near the crack tips at a rather fast loading frequency of 10 Hz.
The effect of retained and reversed austenite on the damping capacity in high manganese stainless steel with two phases of martensite and austenite was studied. The two phase structure of martensite and retained austenite was obtained by deformation for various degrees of deformation, and a two phase structure of martensite and reverse austenite was obtained by reverse annealing treatment for various temperatures after 70 % cold rolling. With the increase in the degree of deformation, the retained austenite and damping capacity rapidly decreased, with an increase in the reverse annealing temperature, the reversed austenite and damping capacity rapidly increased. With the volume fraction of the retained and reverse austenite, the damping capacity increased rapidly. At same volume of retained and reversed austenite, the damping capacity of the reversed austenite was higher than the retained austenite. Thus, the damping capacity was affected greatly by the reversed austenite.
Cubic boron nitride (c-BN) is a promising material for use in many potential applications because of its outstanding physical properties such as high thermal stability, high abrasive wear resistance, and super hardness. Even though 316L austenitic stainless steel (STS) has poor wear resistance causing it to be toxic in the body due to wear and material chips, 316L STS has been used for implant biomaterials in orthopedics due to its good corrosion resistance and mechanical properties. Therefore, in the present study, c-BN films with a B4C layer were applied to a 316L STS specimen in order to improve its wear resistance. The deposition of the c-BN films was performed using an r.f. (13.56 MHz) magnetron sputtering system with a B4C target. The coating layers were characterized using XPS and SEM, and the mechanical properties were investigated using a nanoindenter. The friction coefficient of the c-BN coated 316L STS steel was obtained using a pin-on-disk according to the ASTM G163-99. The thickness of the obtained c-BN and B4C were about 220 nm and 630 nm, respectively. The high resolution XPS spectra analysis of B1s and N1s revealed that the c-BN film was mainly composed of sp3 BN bonds. The hardness and elastic modulus of the c-BN measured by the nanoindenter were 46.8 GPa and 345.7 GPa, respectively. The friction coefficient of the c-BN coated 316L STS was decreased from 3.5 to 1.6. The wear property of the c-BN coated 316L STS was enhanced by a factor of two.
Austenite precipitation behavior was studied with solidification rates and alloying contents, N and Cr, in duplex stainless steels by directional solidification. Directional solidification experiments were carried out with solidification rates, 1~100mm/s, and N and Cr contents, 0~0.27wt.%, 25~28wt.% respectively, in a duplex stainless steel, CD4MCU. As the solidification rate increases, the dendrite spacing reduced and the austenite phase in the ferrite matrix became finer. The volume fraction of austenite phase increased and its shape went to be round with increasing nitrogen contents in duplex stainless alloys. The Cr alloying element, even though it is a ferrite former, showed to enhance the nitrogen solubility in the alloy and caused the austenite round and finer. Also, Cr was supposed to decrease the austenite volume fraction, but it increased the austenite slightly due to increasing nitrogen solubility during solidification.
본 연구에서는 오스테나이트계 스테인리스 강재(STS 304)에 대해 NaCl 환경 중에서 틈부식 특성을 연구하기 위해, 정전압 분극장치에 의해 분극특성시험을 실시하여 NaCl 용액의 농도에 따른 STS 304 강재의 틈부식에 의한 분극 거동에 대해 연구한 결과는 다음과 같은 결론을 얻었다. 1) 틈부위는 심하게 부식되고 틈의 인접한 외부 표면은 부동태화된다. 2) 오스테나이트계 스테인리스강재인 STS 304 강재는 분극거동에 있어서 부식 전위는 3.5% NaCl까지 농도가 증가할수록 귀전위화되다가 농도가 3.5%이상으로 증가할수록 오히려 비전위화된다. 3) 부식 전위하에 전류밀도는 NaCl 농도가 3.5%까지 증가할수록 더 많이 배류되다가 3.5% 이상으로 증가할수록 오히려 더 적게 배류된다.(이 논문의 결론(요약) 부분임)
Concept of primary solidification mode control was adopted to obtain optimal solidification crack resistance, hot ductility, corrosion resistance and toughness for austenitic stainless steel. By controlling primary solidification phase as primary δ and containing no ferrite at room temperature, optimal solidification crack resistance, hot ductility, corrosion resistance and cryogenic toughness could be obtained. The optimum chemical composition of austenitic stainless steel ranges 1.46~1.55(Creq/Nieq ratio) calculated by Schaeffler's equation.
스테인리스강은 최근에 다양한 구조 부재와 산업분야에서 스테인리스강의 상용이 증가하고 있다. 그러나 스테인리스강은 건축구조기준에 구조재료로 포함되어 있지 않고 해당 설계기준은 규정되어 있지 않다. 본 논문에서는 오스테나이트계 스테인리스강 STS304로 제작된 이면전단 볼트접합부에 대한 실험적을 수행되었다. 주요 변수는 볼트배열과 하중방향 연단거리로 설정하였다. 실험 결과, 순단면파단과 블록전단파단이 발생하였고, 블록전단파단 접합부의 경우연단거리가 증가함에 따라 내력이 증가하였다. 또한, 현행 기준식에 의한 예측내력과 실험 내력을 비교하였다.
Recently, since stainless steels have important properties such as superior durability, fire resistance and corrosion resistance, they are widely used as non-structural element as well as structural element in building construction. In this study, experimental studies have been performed to investigate the structural behaviors such as ultimate strength and fracture mode of double shear two-bolted connection and four-bolted connection with austenitic stainless steel(STS304) and varied end distance. In case of two-bolted connection, all of specimens showed block shear fracture. And four-bolted connection failed by block shear fracture or net section fracture at test end.
This study focused on the ultimate behaviors(ultimate strength and fracture mode ) of single shear bolted connection with austenitic sainless steel(STS201) and curling effect on the ultimate strength using finite element analysis based on test results. Main variables are end distance in the parallel direction to loading and edge distance in the perpendicular direction to loading. The validation of finite element analysis procedures was verified through the comparisons of ultimate strength, fracture mode and curling(out-of-plane deformation) occurrence between test results and numerical predictions. Curling was observed in both test and analysis results and it reduced the ultimate strength of single- shear bolted connections with relatively long end distances. Strength reduction ratios caused by curling were estimated quantitatively by maximum 19%, 32%, respectively for specimens with edge distance, 48 mm and 60 mm compared with strengths of uncurled connections with restrained out-of-plane deformation. Finally, analysis strengths were compared with current design strengths and it is found that design block shear equations did not provide the accurate predictions for bolted connections with strength reduction by curling.
This study focused on the ultimate strength and curling effect on the strength of single shear bolted connection with austenitic sainless steel (STS201) using finite element analysis. The validation of finite element analysis was verified through the comparisons of ultimate strength and fracture mode between existing test results and numerical predictions. Curling (out-of-plane deformation) was observed in both test and analysis and it reduced the ultimate strength of single shear bolted connections with relatively long end distances. Strength reduction ratio caused by curling was estimated quantitatively by maximum 19%, 32%, respectively for specimens with edge distance, 48mm and 60mm compared with strengths of uncurled connections with restrained out-of-plane deformation.
This paper is to investigate the stress-strain curves for STS 201 austenitic stainless steel over the full strain range. Ramberg-Osgood expression can be used to predict the stress-strain curve up to the 0.2% proof stress. Rasmussen and Shin have developed the approach for stress-strain curve of stainless steels beyond 0.2% proof stress based on the Ramberg-Osgood concept. However, for STS201 stainless steel, two existing concepts were not available for predicting the curves and therefore modified method was discussed in this paper.