Microstructural analysis of a (α+β) Ti alloy was investigated to consider phase transformation in each step of thethermo-mechanical process using by SEM and TEM EDS. The TAF (Ti-6Al-4Fe) alloy was thermo-mechanically treated withsolid solution at 880oC, rolling at 880oC and annealing at 800oC. In the STQ state, the TAF microstructure was composedof a normal hcp α and metastable β phase. In a rolled state, it was composed of fine B2 precipitates in an α phase, whichhad high Fe segregation and a coherent relationship with the β matrix. Finally, in the annealing state, the fine B2 precipitateshad disappeared in the α phase and had gone to the boundary of the α and β phase. On the other hand, in a lower rollingtemperature of 704oC, the B2 precipitates were more coarse in both the α and the boundary of α and β phase. We concludedthat microstructural change affects the mechanical properties of formability including rolling defects and cracks.
Metastable phase characteristics of beta Ti alloys were investigated to consider the relationship of the microstructureand diffraction pattern in TEM. TEM analysis showed that the microstructure was mottled as a modulated structure, and thediffraction pattern was composed of spot streaks between the main spots of a stable beta phase with a specific latticerelationship. The modulated structure may be induced by short distance slip or atom movement during a very short intervalof solution treated and quenched (STQ) materials. The athermal ω phase, which could be precipitated at low temperature aging,is also analysed by the metastable phase. The metastable phases including athermal ω phase had a common characteristic ofhardened and brittle behavior because the dislocation slip was restricted by a super lattice effect due to short distance atommovement at the metastable state.
This study was performed to fabricate the porous titanium foam by space holder method using NaCl powder, and to evaluate the effect of NaCl volume fractions (33.3~66.6 vol.%) on the porosities, compressive strength, Young's modulus and permeability. For controlling pore size, CP titanium and NaCl particles were sieved to different size range of 70~150 and 300~425 respectively. NaCl of green Ti compact was removed in water followed by sintered at for 2 hours. Total porosities of titanium foam were in the range of 38-70%. Pore shape was a regular hexahedron similar that of NaCl shape. Porous Ti body showed that Young's modulus and compressive strength were in the range of 0.6-6 GPa and 8-127 MPa respectively. It showed that pore size and mechanical properties of Ti foams was controllable by NaCl size and volume fractions.
Ti scaffolds with a three-dimensional porous structure were successfully fabricated using powder metallurgy and modified rapid prototyping (RP) process. The fabricated Ti scaffolds showed a highly porous structure with interconnected pores. The porosity and pore size of the scaffolds were in the range of 66~72% and 300~400 μm, respectively. The sintering of the fabricated scaffolds under the vacuum caused the Ti particles to bond to each other. The strength of the scaffolds depended on the layering patterns. The compressive strength of the scaffolds ranged from 15 MPa to 52 MPa according to the scaffolds' architecture. The alkali treatment of the fabricated scaffolds in an aqueous NaOH solution was shown to be effective in improving the bioactivity. The surface of the alkali-treated Ti scaffolds had a nano-sized fibre-like structure. The modified surface showed a good apatite forming ability. The apatite was formed on the surface of the alkali treated Ti scaffolds within 1 day. The thickness of the apatite increased when the soaking time in a simulated body fluid (SBF) solution increased. It is expected that the surface modification of Ti scaffolds by alkali treatment could be effective in forming apatites in vivo and can subsequently enhance bone formation.
본 논문에서는 Ti-48.5at%Al-0.96at%Mo 조성을 갖는 γ-TiAl 합금은 항온 단조 및 후속 조직제어 열처리 시 발달하는 집합조직의 변화에 관해 연구하였다. 특히, 동적 재결정 후 조직제어 열처리 온도와 시간의 증가에 따라 발생하는 lamellar volume fraction 과 집합조직 변화에 주목하여 관찰하였다. 동적 재결정 후 집합조직은 ND⊥(302) 선분과, TD⊥(100) 및 이에 비해 상대적으로 다소 약한(111) 성분들이 발달하였으며, 열처리 온도와 시간이 증가함에 따라 lameller volume fraction 은 증가했고 동일한 성분의 집합조직도 점차 강하게 발달함을 알 수 있었다. 하지만 상온인장시험 결과는 lameller volume fraction이 증가할수록 낮은 상온 연신을 보였는데, 이는 준 층상조직을 갖는 γ-TiAl합금의 상온인장특성이 집합조직의 영향보다는 lameller volume fractio과 같은 미세조직 특성에 더욱 강하게 영향을 받기 때문인 것으로 판단된다.
본 논문은 모바일 RPG게임 내 인앱 결제 서비스 이용자들에 대한 사용성 평가를 통해 향후 국내 모바일 RPG게임 개발자 및 기획자들에게 업데이트 및 개발에 필요한 자료를 모색하고 제안하는 데 그 목적을 두었다. 모바일 게임 '리니지M'의 인 앱 결제 서비스를 주로 이용하는 이용자들을 대상으로 정량적 평가를 위한 사용성 평가를 실시했다. 사용성 평가를 위한 도구로는 피터모빌(Peter Morville)이 정의한 'The User Experience Honeycomb'를 기준으로 설계한 설문지를 통해 설문조사를 하였다. 이러한 통계결과를 접근성, 가치성, 신뢰성, 매력성, 사용성 총 5가지 측면으로 나누어 분석하였고, 이를 통하여 새로운 모바일 RPG게임 개발에 도움을 줄 것으로 기대한다.