The correct computer simulation of the powder compaction stage requires the determination of the elastoplastic parameters which characterize its mechanical behavour. Instrumented dies are frequently used to monitor the longitudinal and radial stress occurring during powder compaction. When strain gages are employed a previous calibration is needed. Many sources of error exist that can lead to the incorrect calibration of the instrumented die. By means of a FEM simulation some of these problems are analysed. The effect of die wall thickness, compression length, and strain location are studied.
The influence of doping on the structural and morphological properties of the phosphor system, obtained ultrasonically via Spray Pyrolysis from common gadolinium and europium nitrate solutions, was studied. The particle morphology, crystalline and chemical structure were studied by XRD, SEM and EDS. TEM was applied in order to identify the structure and growth of "primary nanoparticles" and determine the presence of domains locally affected by "Moires Frames" and "Crystallite Size". The SADP allows determining the presence of a polycrystalline material with two phases in the "as-prepared" samples, and only an Ia3 phase along the thermal treatment.
This paper presents a study of large grains by transmission electron microscopy in two WC-Co alloys, one W rich and one C rich. In the W rich alloy, some large grains are found in contact with the phase. The C content influences the morphology of large grains: they are flatter in the C rich alloy with smoother interfaces. Whatever the C content, they contain few dislocations compared to matrix grains except often in a small area. Small WC grains are often found inside the large grains. They have likely been engulfed during the growth of the large grains owing to the low boundary energy.
Based on the comparison of structures and properties of the HS6-5-2 high speed steels made with the powder injection moulding method, pressureless forming, compacting and sintering, and commercial steels made with the ASEA-STORA method, fine carbides spread evenly in the steel matrix were found in the structure of all tested high-speed steels in the sintered state. The steels made with the pressureless forming method are characteristic of the lowest sintering temperature and the highest density, resulting from the high carbon concentration coming from the binding agent degradation.
Processing of W-Cu graded materials from attritor-milled W-CuO mixtures is described. The powder reduction steps are investigated by TG and XRD analyses and by microstructural observations (SEM, TEM). Sintering of reduced powder with different compositions is analysed by dilatometry. Sintering behaviour of the graded component processed by co-compaction of a 10/20/30wt%Cu multi-layer material is briefly discussed. Liquid Cu migration is observed and smooths the composition gradient. Perspectives to control this migration are discussed.
The present study examined the possibility of cryopreservation of the D-shaped and umbo larvae of arkshell (Scapharca broughtonii), in terms of the survival rates after freezing and thawing. D-shaped and umbo larvae of arkshells were obtained from a shellfish farming on Yosu city. The average shell lengths were m and , respectively. Five cryoprotectants (CPAs), dimethyl sulfoxide (DMSO), glycerol, ethylene glycol (EG), propylene glycol (PG), and methanol, were tested at the concentrations of 1.5, 2.0 and 2.5 M. After larvae suspended in CPAs, cryoprotectants were loaded in 0.5 ml straws at a larval density of 50-100 larvae per straw, and epuilibrated for 10 and 20 minute at room temperature (), repectively. Straws were cooled at a rate of /min from to , held for 5 min at , and then cooled at /min to and equilibrated for 5 min followed by plunging in liquid nitrogen. After storage in liquid nitrogen for 1 day, straws were thawed in a water. As soon as straws were observed to melt, larvae were diluted with an equal volume of ASW and then washed twice with a large volume of ASW at an interval of 2 min to unload the CPAs. The results showed that after equilibration for 10 and 20 minute at room temperature, no larvae survived using methanol as CPAs, and it was observed that larval shells all open slightly, and larval flesh broke down and slopped over the shells. The highest survival rates (D-shaped larvae: 77.6%, umbo larvae: 59.3%) were obtained with 2M DMSO, and 1.5M glycerol yielded survival rates of 53.8% for D-shaped larvae and 37.5% for umbo larvae. The surviving D-shaped larvae showed active rotary motion and perfect membrane integrity and cytoplasmic normality, and the vigorous movement of veliger cilia was observed inside the closed shells. The breakdown of tissue occurred in the abnormal larvae, and the isolated cell often run out of shells.
상시 이용가능한 전천후, 범세계적인 정확한 항법을 개발하는 것이 항해자들의 숙원이었다. 이제 시스템의 보완의 문제가 국제적인 규모에 초점이 맞추어 진다면 현시점의 기술로도 이 숙원이 앞으로 10년 내에 이루어 질 가능성이 엿보인다. 범세계적인 전파항법은 그 정의상 수신지점이 아무리 멀리 떨어지고 고립되어 있다 하더라도 육·해·공 어디서나 아무런 전파간섭 없이 수신될 수 있는 것이어야 한다. 범세계적인 항법방식을 채택하는 데 있어서 중요하게 고려되는 사항은 간섭이 없는 주파수 스펙트럼의 이용과 전파항법의 송신사양의 발천이다. 국가안보를 위한 항해와 민간의 목적을 위한 항해 사이의 갈등과 국가간의 요구의 상이는 국가적 결정과 국제적 협력을 위한 의미있는 도전을 나타낸다. 송신국이 육지에 있는 장거리항법방식 2가지, 즉 Loran-C와 Omega는 현재 시행되고 있으며, 인공위성항법방식이 앞으로 실현될 가능성이 있는데, 지금이 바로 행동을 취할 때라고 제안한다. 본 논문은 Loran-C와 Omega 방식의 기술사양서 발행의 절실한 필요성과 이러한 범세계적인 전파항법의 송신에 요구되는 주파수, 스펙트럼의 정의의 필요성을 기술한다. 그리고 국제 전기통신협회의 후원하에 1979년 Genova에서 열린 World Administrative Radio Conference에 앞서서 주의를 요하는 특별한 기술적인 분야에 대해서 기술한다.