Spherical fine powders of tungsten oxide powders were prepared by the emulsion evaporation method. The characteristics of the powders prepared were examined by means of TGA, X-ray diffraction, SEM and image analysis. The emulsions were prepared by fast mixing of aqueous phase containing tugsten and the organic phase which composed of kerosene, surfactant, and paraffin oil. Precursors were made by evaporating the emulsionin the kerosene bath at , and then calcined at in order to produce tungsten oxide powders. The average particle size of the tungsten oxide powders was and their shapes were spherical at the both case of w/o and o/w type emulsions. As the HLB value of the surfactant increased and the concentration of tungsten ions decreased the mean particle siqe of tungsten oxide powders decreased whereas agglomerationsize increased. The optimum concentration of Span 80 was 8 percent by volume, and the optimum stirring speed in the emulsion formation was 5000 rpm in order to obtain fine and well dispersed powders.

We present the results of one-dimensional numerical simulations of SNR evolution in the in­homogeneous medium considering the effects of the evaporation of the cloud and the thermal conduction. We have included the effects of changing evaporation rate as a function of cloud size and the ambient temperature so that the clouds could be evaporated completely before they reach the center of the SNR. The heat conduction markedly changes the density distribution in the remnant interior. To explain the observed morphologies of the centrally peaked X-ray SNRs(for example W44), the maximal thermal conduction is required. However, this is unlikely due to the magnetic field and the turbulent motion. The effects of the evaporation of the cloud and the thermal conduction described here may explain the class of remnants observed to have centrally peaked X-ray emmision.

In this study, organic electroluminescent devices(OELD) with a structure of a glass substrate/ITO/TPD/Tb(ACAC)3(Phen-Cl)/Alq3/Al was fabricated by vacuum evaporation method, where Tb complex was known to have green light emitting property. Electroluminescent(EL) and I-V characteristics of this structure were investigated. This triple-layer structure shows the green EL spectrum at the wavelwngth of 546nm, which is almost the same as the PL spectrum of Pb(ACAC)3(PhenCl). It was found in current-voltage(I-V) characteristics of the devices that the operating voltage was about 12V.

열증착법에 의해서 온도 85˚C인 glass기판 위에 CdS 박막을 제작하였다. 두께가 200nm정도로 측정된 CdS박막은 공기 중에서 온도 250˚C-550˚C범위에서 각각 30분간 열처리 되었으며 이들 시료에 대하여 4-point probe, XRD, SEM, UV-Spectrophotometer 및 광발광 측정으로 전기적 광학적 특성을 조사하였다. 이들의 일련의 실험값은 열처리 온도 370˚C 근처에서 구조의 변화를 보여주었는데, 열처리 온도에 대한 비저항아니 XRD, SEM 의 측정은 cubic로부터 hexagonal구조로의 변환을 나타내었다. 특히 상온에서 측정한 광발광에서 green edge emission(GEE)피이크가 2.42eV를 나타내었는데 이 때의 발광 중심은 열처리할 때 생긴 S-vacancy에 보상된 산소로 이루어진 'CdO'의 악셉터준위에 기인하는 것으로 해석되며 그 이온화 에너지는 약 0.16eV이었다.

페르브스카이트 구조를 갖는 CaTiO3-La(Zn12/Ti12)O3계에서 소결 온도와 소결 시간의 증가에 따른 ZnO의 휘발과 이에 따른 고주파 유전 특성에 대하여 조사하였다. 시편 내부를 WDS 분석한 결과 위치에 따른 ZnO의 농도차를 관찰할 수 있었고, 시편의 두께를 달리하여 QxfO 값을 조사한 결과 ZnO가 많이 휘발된 가장자리에서 더 높은 QxfO 값을 얻을 수 있었다. 0.535CaTiO3-0. 465La(Zn12/Ti12/)O3몰비로 1550˚C, 2시간동안 합성한 결과 소결 밀도 5.31g/㎤, 유전율 50, Qxf034,000, 온도계수 +8ppm/˚C의 고주파 유전 특성을 갖는 소결체를 얻을 수 있었다.

증착법을 이용해 증착시 기판의 온도를 변화시키면서 MnSbPt 합금 박막을 만들고 이를 열처리 한 후 나타나는 자기 및 자기광학적 성질을 조사하였다. Mn45Sb45Pt10조성의 박막에서 0.85˚의 높은 Kerr Rotation Angle값을 나타내고, 또한 광원의 입사파장이 단파장으로 이동하여도 우수한 Kerr Rotation Angle 값을 유지함으로써 자기광 재료로서의 기록밀도 향상가능성이 기대된다. 이 재료가 갖고 있는 열악한 자기적성질도 열처리를 통하여 포화자화값과 보자력의 향상 효과를 얻었지만, 자기광 재료가 갖추어야할 수직자화를 얻기에는 미흡하여 이에 대한 보완이 필요하다.

Recently, many researchers make a great effort to develop high efficient marine diesel engines using low grade heavy oil, and also study substitution fuel oil for engines and boilers. In case of Fisheries Vessels, we need to know that fish oil can be substituted for fuel oil. Therefore, it is studied that evaporation, ignition and combustion phenomena of the single droplet of fish oils (i.e., Sardine fish oil, File fish oil and Alaska pollac oil) on heated plane surface to evaluate appropriateness as substitution oil. Methanol and light oil are tested simultaneously to help the evaluation on these Fish oils. The results are summarized as follows: 1. The type of evaporation and combustion is spherical evaporation in case of methanol and light oil. And fish oil blended with light oil was finished after spherical evaporation happen when high temperature. 2. Ignition of Pure fish oil was shorter than that of fish oil blended with light oil. 3. Heat transferred to droplet could make qualitative comparison by contact diameter of droplet with hot surface as time changes. Life time of droplet according to the change of heated surface temperature was greatly influenced by droplet contact condition on the heated surface. 4. As far as combustion phenomena was concerned, apparent diameter of the fish oil droplet increased after ignition and decreased suddenly by internal boiling of droplet. 5. Three fish oils had similar phenomena on the evaporation, ignition and combustion. 6. Evaporation and combustion feature of fish oil could not be shown by coefficient of evaporation velocity of droplet and coefficient of combustion velocity of droplet.

In this paper, to percuss whether fish oil can substitute for marine fuel oil, the characteristics on the evaporation and ignition of 3 fish oils, Sardine oil, File fish oil and Alaska pollac oil, were investigated experimentally by suspending single fish oil droplel in hot atmosphere, and experiments on methanol and light oil were also carried out to compare the characteristics. The results abtained are summarized as follow; 1) Evaporation and ignition phenomena on the methanol and light oil by the present experimental method agreeded with the results of the earlier investigation. 2) The characteristic on evaporation and ignition of all 3 fish oils took the same pattern; in late stage of evaporation at atmospheric Temperature 550℃ droplet rapidly expanded and contracted, and then remained solid corbide, but in case of 650℃ rapidly expanded and ignitied, and then completly burned non-remained solid carbide. 3) As fish oil mixed with light oil (50% weight), in beginning stage of evaporation droplet depended on the characteristics of light oil, but in end stage depended on fish oil. 4) Ignition temperature of fish oil droplets was about 470℃, higher than about 250℃ of light oil, but atmospheric temperature to ignite droplet was about 650℃, lower than about 750℃ of light oil.

An evaporation disk model is proposed_to figure out shapes of molecular disks with density distributions of ρ_d∝r^(-n)(n$gt;1.8) using the energy and pressure equilibrium conditions as well as to explain the collimation mechanism of optical and radio jets with an openning angle of about 10 inside bipolar molecular outflows. Numerical hydrodynamic calculation of the jet inside shows that the jet velocity increases with a dependence on z^(1-5) and the Mach number of the jet converges to √3 . Mechanical energy of the jet heats the jet material, increasing the jet temperature with a distance. Calculated Ha flux in shock condition and radio continuum intensity at 5GHz are surely comparable to the observed ones. These results strongly support the evaporation disk model in collimating jet.

본 연구에서는 우리나라 56개 연구지역에 대해서 증발량 산정방법 중에 하나인 공기동력학적 방법의 적용성을 검토하였다. 이를 위해 과거 연구 자들에 의해서 제안된 공기동력학적 증발량 산정식들을 7가지 형식으로 구분하고 일반화하여 증발량 산정모델을 유도하였다. 또한, 공기동력학적 방법 적용에 필요한 기상요소자료들(풍속, 포화미흡량, 기온, 대기압)을 이용하여 4가지의 다변량 선형회귀모델을 유도하고 그 적용성을 검토하였다. 기상자료들의 자기상관의 영향을 고려하기 위해 변수들을 차분시켜 회귀분석을 실시하고 자기상관을 고려하지 않은 경우와 비교한 결과 결정 계수 값에 큰 차이가 없음을 확인하였다. 연구결과에 의하면 공기동력학적 모델이나 다변량 선형회귀모델 모두에서 산정된 월 증발량과 관측된 월 증발량 사이에 매우 높은 상관성이 있는 것으로 나타났다. 하지만 대부분의 증발량 산정모델에서 8, 9, 10, 11, 12월에 증발량을 과다 산정하고 있는 것으로 나타났다. 다변량 선형회귀모델들에 사용된 기상요소자료들은 모두 증발량 산정에 유의한 영향력이 있는 것으로 나타났으며, 특히 포화 미흡량이 가장 중요한 기상요소이며, 두 번째로는 기온, 세 번째로는 풍속, 그리고 마지막으로 대기압인 것으로 나타났다.

The effect of mixed oil on the drying characteristics of sewage sludge in oil vacuum evaporation systems was studied. The experimental results showed that the drying rate with cooking oil was faster than that with refined oil due to the difference of thermal conductivity and composition of mixed oil. However, the heating value of all dried sludge was enhanced and the moisture content was below 1% due to penetration of oil into the microbial cells in sludge during the drying procedure. TGA analysis of sludge mixed with the refined oil, which had a higher volatility, showed the slope of the primary falling period was sharply declined. The result of DTA analysis also showed that the first peak was higher than the second peak and corresponded with the phenomena observed in the TGA analysis. In the DTA analysis, the temperature of the primary peak and the secondary peak of dried sludge were comparatively lower than those of raw sludge. Therefore, mixed oil could decrease the self-ignition temperature in an oil-sludge mixing system. In case of waste cooking oil, the TGA and DTA results showed similar results to those of raw sludge, but the DTA results showed that the secondary peaks of dried sludge were narrower and sharper than those of raw sludge. Overall, mixing oil could be a principal factor in controlling the drying efficiency and thermal properties of sludge-derived fuel in oil vacuum evaporation systems.

증발접시 증발량의 경우 저수지 증발량을 산정하는 간접적인 방법으로 유용하게 적용되고 있다. 따라서 본 연구에서는 이용할 수 있는 기상자료 가 제한적인 경우에 기온자료만을 이용하여 증발접시 증발량을 산정하는 식을 제안하였다. 이를 위해서 전국 12개 지역에서 관측된 증발접시 증발 량과 비교를 통해 제안식을 유도하였다. 또한 전국 44개 지역에 대해서 본 연구에서 제안된 증발접시 증발량 산정식을 다른 기온자료에 기초한 식 들뿐만 아니라, 여러 종류의 기상자료(기온, 풍속, 습도, 일조시간)를 필요로 하는 식들과 비교하여 적용성을 파악하였다. 연구결과에 의하면 본 연 구에서 제안된 증발량 산정식들은 다른 기온자료에 기초한 식들과 비교하여 전반적으로 양호한 증발접시 증발량 산정결과를 보였다. 본 연구에서 제안된 증발량 산정식의 경우 우리나라 56개 연구지역 대부분에서 전반적으로 양호한 증발접시 증발량 산정결과를 보였다. 따라서 본 연구에서 수 정 제안된 기온자료만을 이용한 증발접시 증발량 산정식들은 우리나라에서 이용할 수 있는 기상자료가 제한적인 경우에 특히 적용성이 있는 것으 로 판단된다. 추후에는 저수지에서 관측된 기온 및 증발접시 증발량 자료를 바탕으로 저수지 증발량 산정을 위한 제안식들의 적용성 검토연구가 필 요하다.

In construction sites there are many cases that concrete is cured in a dry condition, without being moistured, after form have been removed. Consequently such curing condition causes cracks on concrete. In this study is to observe when applied ERCO(Emulsified Refined Cooking Oil) coating on concrete surfaces after removal of form, affects water evaporation and Shrinkage of high-strength mortar.