Because of depletion of fossil fuel from the earth curst and increase of environmental concerns, in search of an efficient alternative to the traditional carbon black (CB), a biochar known as rice husk carbon (RHC) has been examined here as a filler material to develop the EPDM composite. In this regard, the ball milled RHC was further treated with ultrasonic wave and used with or without its surface treatment by the silane coupling agent [i.e., 3-mercaptopropyl triethoxysilane (3-MPTMS)]. Among the RHC, ultrasonic treated RHC (UHC) and silane treated UHC (USHC), the EPDM composite of USHC showed nearly similar tensile strength to that of the CB (e.g., CB: 33.88 kgf/cm2, USHC: 31.38 kgf/cm2 at 20 wt% filler loading) with an enhanced elongation at break (e.g., CB: 206%, USHC: 342% at 20 wt% filler loading) and surprisingly much less compression set value (CB: 40.87%, USHC: 18.95% even after 40 wt% of filler loading). Compared to RHC, the UHC also showed its better performance next to the USHC. In addition to presence of both the carbon and silica in RHC and additional silica within the flexible aliphatic chain in USHC, the disintegration of RHC by ultrasonic treatment towards its narrow particle distribution, smaller particle size, and increased surface area is considered very much effective to develop the corresponding high performance EPDM composites. Thus, the use of waste material, i.e., rice husk through the ultrasonication of RHC followed by its surface treatment can be used as a potential filler material to prepare the environment friendly and cost effective high performing composites to be used in different efficient end products, and motivated further for industrial upscaling.

In this study, Ti-Mo-EB composites are prepared by ball milling and spark plasma sintering (SPS) to obtain a low elastic modulus and high strength and to evaluate the microstructure and mechanical properties as a function of the process conditions. As the milling time and sintering temperature increased, Mo, as a β-Ti stabilizing element, diffused, and the microstructure of β-Ti increased. In addition, the size of the observed phase was small, so the modulus and hardness of α-Ti and β-Ti were measured using nanoindentation equipment. In both phases, as the milling time and sintering temperature increased, the modulus of elasticity decreased, and the hardness increased. After 12 h of milling, the specimen sintered at 1000oC showed the lowest values of modulus of elasticity of 117.52 and 101.46 GPa for α-Ti and β-Ti, respectively, confirming that the values are lower compared to the that in previously reported studies.

Oxide dispersion-strengthened (ODS) steel has excellent high-temperature properties, corrosion resistance, and oxidation resistance, and is expected to be applicable in various fields. Recently, various studies on mechanical alloying (MA) have been conducted for the dispersion of oxide particles in ODS steel with a high number density. In this study, ODS steel is manufactured by introducing a complex milling process in which planetary ball milling, cryogenic ball milling, and drum ball milling are sequentially performed, and the microstructure and high-temperature mechanical properties of the ODS steel are investigated. The microstructure observation revealed that the structure is stretched in the extrusion direction, even after the heat treatment. In addition, transmission electron microscopy (TEM) analysis confirmed the presence of oxide particles in the range of 5 to 10 nm. As a result of the room-temperature and high-temperature compression tests, the yield strengths were measured as 1430, 1388, 418, and 163 MPa at 25, 500, 700, and 900oC, respectively. Based on these results, the correlation between the microstructure and mechanical properties of ODS steel manufactured using the composite milling process is also discussed.

In this study, we investigate the effect of the duration of mechanical alloying on the microstructures and mechanical properties of ODS ferritic/martensitic steel. The Fe(bal.)-10Cr-1Mo pre-alloyed powder and Y2O3 powder are mechanically alloyed for the different mechanical alloying duration (0 to 40 h) and then constantly fabricated using a uniaxial hot pressing process. Upon increasing the mechanical alloying time, the average powder diameter and crystallite size increased dramatically. In the initial stages within 5 h of mechanical alloying, inhomogeneous grain morphology is observed along with coarsened carbide and oxide distributions; thus, precipitate phases are temporarily observed between the two powders because of insufficient collision energy to get fragmented. After 40 h of the MA process, however, fine martensitic grains and uniformly distributed oxide particles are observed. This led to a favorable tensile strength and elongation at room temperature and 650oC.

최근 대규모 토목 및 건축 구조물 증가 추세로 건설 부재의 고강도 및 경량화에 대한 수요가 높아지고 있다. 기존 시멘트 경량 복합체의 경우 단위 체적 중량이 낮아 강도 저하 문제가 발생할 수 있다. 보통 경량화를 위해서 시멘트 복합체를 배합할 때 일반 경량골재와 고무재질의 경량골재, 플라스틱 펠릿 등 다양한 인공 경량골재를 적용한 시멘트 복합체로 경량화를 확보할 수 있다. 이 중에서도 시멘트 복합체의 인공 경량골재로 플라스틱을 사용하면 상대적으로 골재 자체의 강도를 확보하면서 경량화를 꾀할 수 있지만 재료의 매끄러운 표면 특성으로 인해 시멘트 페이스트와 부착하는 데 불리한 부분이 있고 이는 콘크리트 골재 또는 시멘트 복합체 골재로서의 사용에 있어 단점이 된다. 띠라서 이번 연구에서는 기존 연구에서 플라스틱 골재 로 가장 적합한 유형으로 확인된 PP, PE 두가지 유형의 플라스틱 골재와 강섬유, 양생방법을 변수로 하여 실험을 진행하였고 실험 결과 플라스틱의 비중이나 표면 재질뿐만 아니라 강섬유의 혼입유무, 양생방법에 의해서 시멘트 복합체의 물리적 특성이 변화된다는 것을 확인하였다.

In recent, fiber-reinforced composites have been widely used in many fields because of their excellent performance. In order to manufacture lightweight, high-performance, and inexpensive composites various laminated structures were designed. Six types of hybrid composites were fabricated with glass/basalt/aramid fibers by VARTM process. The effect of the laminated structure on the mechanical properties of composites was investigated through impact energy, tensile and bending strength. Compared to other conditions more higher impact energy was obtained when the aramid fibers were in the center position and more higher bending strength was obtained when the fibers are laminated in the order of increasing bending performance from top to bottom. The laminate structure did not affect tensile strength which mainly depends on the property of fibers.

This study was conducted for the purpose of suggesting a standard that can be used under ambient temperature by improving the low mechanical and thermal properties of ABS. PC was used as a filler, and post-curing conditions of the ABS/PC blend injection material were investigated. It was found that the ABS/PC blend injection material having a PC content of 20 wt.% or more showed little change in tensile properties at a temperature of 50°C, and a decrease in tensile properties of less than 10% at 80°C.

In this study, a nanocrystalline FeNiCrMoMnSiC alloy was fabricated, and its austenite stability, microstructure, and mechanical properties were investigated. A sintered FeNiCrMoMnSiC alloy sample with nanosized crystal was obtained by high-energy ball milling and spark plasma sintering. The sintering behavior was investigated by measuring the displacement according to the temperature of the sintered body. Through microstructural analysis, it was confirmed that a compact sintered body with few pores was produced, and cementite was formed. The stability of the austenite phase in the sintered samples was evaluated by X-ray diffraction analysis and electron backscatter diffraction. Results revealed a measured value of 51.6% and that the alloy had seven times more austenite stability than AISI 4340 wrought steel. The hardness of the sintered alloy was 60.4 HRC, which was up to 2.4 times higher than that of wrought steel.

The effects of different spray angles (90°, 85°, 80°) on the microstructure and mechanical properties of a Y2O3 coating layer prepared using the atmospheric plasma spray (APS) process were studied. The powders employed in this study had a spherical shape and included a cubic Y2O3 phase. The APS coating layer exhibited the same phase as the powders. Thickness values of the coating layers were 90°: 203.7 ± 8.5 μm, 85°: 196.4 ± 9.6 μm, and 80°: 208.8 ± 10.2 μm, and it was confirmed that the effect of the spray angle on the thickness was insignificant. The porosities were measured as 90°: 3.9 ± 0.85%, 85°: 11.4 ± 2.3%, and 80°: 12.7 ± 0.5%, and the surface roughness values were 90°: 5.9 ± 0.3 μm, 85°: 8.5 ± 1.1 μm, and 80°: 8.5 ± 0.4 μm. As the spray angle decreased, the porosity increased, but the surface roughness did not show a significant difference. Vickers hardness measurements revealed values of 90°: 369.2 ± 22.3, 85°: 315.8 ± 31.4, and 80°: 267.1 ± 45.1 HV. It was found that under the condition of a 90° angle with the lowest porosity exhibited the best hardness value. Based on the aforementioned results, an improved method for the APS Y2O3 coating layer was also discussed.

The behaviour of semiconducting graphene quantum dots (GQDs), as good candidates for various biological carrier applications and optical sensing, are necessary to be studied under various conditions. In this study, GQD models were generated according to the geometrical and chemical specifications of synthesized GQDs to achieve the most realistic models. The GQDs’ bandgap and distribution of their electric surface charges were obtained using computational chemistry method. Finite element analysis was conducted on pristine and defective GQDs to study Young and shear modulus. Buckling load and resonant frequency modes of GQDs were calculated analytically and demonstrated under various boundary conditions. The dimension of GQDs has an average of 3.5 ± 0.4 nm, with an interlayer spacing of 0.36–0.40 nm. Computational chemistry studies revealed the characteristic zero-band-gap nature of graphene. Finite element studies showed that the by introducing the inevitable dislocation, mono atom vacancy and Stone–Wales defects to GQD models, their mechanical properties reduces to approach data from experimental investigations, whereas an increase in the number of layers does not influence the obtained results significantly.

Because of the International Maritime Organization(IMO)'s regulation to regulate emissions of ships, a change is taking place to replace ship fuels from Heavy Fule Oil(HFO) to Liquefied Natural Gas(LNG). In the case of LNG, it is a material obtained by liquefying Natural Gas(NG), and it is -163 degrees below zero, and the volume is reduced to 1/600 level. The material of the tank that can store LNG must be a material that can safely store LNG in a cryogenic environment, and the materials of the tank that can store LNG are limited in the International Code of the Construction and Equipment of Ships Carrying Liquefied Gases in Bulk(IGC Code). Among the materials listed in the IGC Code, 9% nickel steel is used as a material for LNG fuel propulsion tanks that are recently ordered because of relatively high mechanical properties under cryogenic environments. In this study, the mechanical properties of butt welds were measured following the weld reliability evaluation of Flux Cored Arc Welding(FCAW) butt welds made of 9% nickel steel by PARTI. The measured mechanical properties are tensile strength, bending strength, hardness, and cryogenic impact test required by the classification for Welding Procedure Specification(WPS) approval.

When performing finite element analysis using materials with porosity the porosity shows different mechanical properties from the existing mechanical properties of the existing base materials. In this study the equivalent properties were calculated and verified by applying the representative volume element (RVE) method and assuming that the material with porosity is a 2D orthotropic material. In case of finite element analysis using porous material or composite material, it is inefficient to perform the analysis through material modeling. Based on the element volume and element stress values ​​derived using the finite element analysis program, the representative stress values ​​and elastic modulus matrix were calculated using Python. In addition, equivalent properties were derived using the calculated elastic modulus matrix. The pores were simulated by etching a thin plate specimen made of STS304 material in a certain pattern, and the elastic modulus and Poisson's ratio were measured through a UTM and compared with simulation results. It was confirmed that an error of 7.028% for elastic modulus and 10% for Poisson's ratio occurred, and through this, the validity of this simulation was verified.

The demand for materials with porosity is steadily increasing and the need for porous materials is increasing in fields such as chemical engineering and energy storage. In order to minimize trial and error, verifying design validity through finite element method at the design stage has the advantage to verify design validity with low cost. However there are limitations in finite element analysis using porous materials. In this study calculating the equivalent mechanical properties reflecting the porosity was carried out, and the first step was the isotropic elasticity in plane stress condition. The equivalent elastic modulus and the equivalent Poisson's ratio were derived through simulation. Assuming that the voids exist in a two-dimensional symmetrical shape and a constant distribution, the unit cell was defined and the equivalent mechanical properties were calculated. The specimen with same condition were measured through a universal test machine (UTM), the elastic modulus and Poisson's ratio were measured. The similarity between the value obtained through the simulation and the value measured through the experiment was under 5%, so the validity of this simulation was verified. With this result, FEM with porous materials will be used for design.

The effect of sintering conditions on the austenite stability and strain-induced martensitic transformation of nanocrystalline FeCrC alloy is investigated. Nanocrystalline FeCrC alloys are successfully fabricated by spark plasma sintering with an extremely short densification time to obtain the theoretical density value and prevent grain growth. The nanocrystallite size in the sintered alloys contributes to increased austenite stability. The phase fraction of the FeCrC sintered alloy before and after deformation according to the sintering holding time is measured using X-ray diffraction and electron backscatter diffraction analysis. During compressive deformation, the volume fraction of strain-induced martensite resulting from austenite decomposition is increased. The transformation kinetics of the strain-induced martensite is evaluated using an empirical equation considering the austenite stability factor. The hardness of the S0W and S10W samples increase to 62.4-67.5 and 58.9-63.4 HRC before and after deformation. The hardness results confirmed that the mechanical properties are improved owing to the effects of grain refinement and strain-induced martensitic transformation in the nanocrystalline FeCrC alloy.

본 연구의 목적은 생체 신호 측정 압력 및 인장 직물 센서의 전극을 자수 공정을 이용하여 제작할 때 전도사의 필요 물성을 파악하는 것이다. 스마트 웨어러블 제품의 전극을 전도사를 이용한 자수 공정을 통해 전극 및 회로 등을 제작하면 불필요한 재료 손실이 없고 복잡한 전극 모양이나 회로 디자인을 컴퓨터 자수기를 이용하여 추가 공정 없이 제작할 수 있다. 하지만 보통의 전도사는 자수 공정 내의 부하를 못 이기고 사절 현상이 발생하기에 본 연구에서는 silver coated multifilament yarn 3종류의 기계적 물성인 S-S curve, 두께, 꼬임 구조 등을 분석하고 동시에 자수기의 실의 부하를 측정하여 자수 공정 내 전도사의 필요 물성을 분석하였다. 실제 샘플 제작에서 S-S curve의 측정 결과가 가장 낮은 silver coated polyamide/polyester가 아닌 silver coated multifilament의 사절이 발생하였으며 그 차이는 실의 꼬임 구조와 사절이 일어난 부분을 관찰한 결과 수직으로 반복적인 부하가 일어나는 자수 공정에서 꼬임이 풀리면서 사절이 일어나는 것을 알 수 있었다. 추가적으로 압저항 압력/인장 센서를 제작하여 생체 신호 측정용 지표인 gauge factor를 측정하였으며 스마트 웨어러블 제품의 대량 생산화에 중요한 부분인 자수 전극 제작으로의 적용 가능성을 확인하였다.

Wire arc additive manufacturing (WAAM) is being considered as a technology to replace the conventional manufacturing process of titanium alloys. However, coarse β grains, which can extend through several deposited materials, result in strong textures and anisotropy. As a solution, we study the plastic deformation effects of ultrasonic needle peening (UNP) on the microstructure. UNP treated materials deform plastically and the dislocation density increases. Fine α+α' grains with low aspect ratio are observed in the UNP treated specimens. UNP treated WAAM Ti-6Al-4V alloys have higher strength and lower elongation than those characteristics of WAAM Ti-6Al-4V alloys. Due to UNP treatment, the z-axis directional specimens exhibit a greater effect of reducing elongation than do the x-axis directional specimens. The UNP treatment produces fine grains in proportion to the number of times UNP is performed, thereby increasing strength. UNP processes produce a large number of dislocations in the WAAM Ti-6Al-4V alloys, with the most dislocations being formed at the surface.

Compared to carbon nanotubes (CNTs), graphene possesses high strength due to wrinkled surface texture caused by a high density of surface defects which benefits more contact with the polymer material than a rolled-up CNT. In the present review, we have discussed and compared the various properties of CNTs (1-D) and graphene (2-D) obtained in experimental results. The effects of covalent and non-covalent functionalization of CNTs and graphene on the properties of its composites have also been reviewed and compared. A comparative analysis has been carried out between CNTs and graphene-reinforced polymer composites. Furthermore, the synergetic effects of CNTs and graphene hybrid nanofiller on the mechanical properties of polymer composites have also been briefly discussed. Finally, this review concludes with the potential application and future challenges are discussed with regards to filler and their polymer composites.

Additive manufacturing technology, 3D printing, has been applied to various industrial fields. This production method is a production method with less material, cost and time savings, and less restrictions in shape, and is also making a leap forward in the field of eco-friendly product production. In particular, FDM (fused depositon modeling) method of extrusion lamination manufacturing is widely applied in products and medical fields. And as an alternative to mold manufacturing, it is widely used in manufacturing plastic products and parts. Therefore, this paper quantitatively and qualitatively analyzes the mechanical properties according to the processing factors of the specimen through the processing of the ABS tensile specimen printed by the FDM type 3D printer and derives the optimum value.

알루미늄합금 6061-T6 판재에 대하여 마찰교반용접과 텅스텐 이너트 가스 용접의 교차 용접부의 미세조직과 기계적 특성에 있어서 용접 순서의 영향을 분석하기 위한 시험편을 성공적으로 제작하였다. FSW-ED 시험편이 다른 조합들보다 가장 좋은 기계적 특성을 나타내었다. 흥미롭게도, TIG-FSW ED 시험편이 FSW-TIG ED 시험편보다 높은 인장강도를 나타내었다. 용접부 경도의 경우, FSW 시편이 TIG-FSW 및 FSW-TIG 시험편보다 높은 값을 나타내었고, TIG-FSW 시험편이 FSW-TIG 시험편보다 높은 값을 나타내었다. FE-SEM을 이용한 인장 파면에 대한 관찰을 통하여, 모든 시험편에서 연성파괴를 나타내는 다양한 크기의 딤플들이 관찰되었다. FSW-TIG 시험편의 파면에서는 용융지(熔融池) 표면 영역에서 기공들이 관찰되는 반면, TIG-FSW 시험편에서는 기공의 형성은 관찰되지 않았다. 경도와 미세조직의 결과를 통해 TIG-FSW 공정이 FSW-TIG 공정보다 높은 인장강도를 확보할 수 있는 공정임을 확인하였다.

In this study, AlSi10Mg powders with average diameters of 44 μm are additively manufactured into bulk samples using a selective laser melting (SLM) process. Post-heat treatment to reduce residual stress in the as-synthesized sample is performed at different temperatures. From the results of a tensile test, as the heat-treatment temperature increases from 270 to 320oC, strength decreases while elongation significantly increases up to 13% at 320oC. The microstructures and tensile properties of the two heat-treated samples at 290 and 320oC, respectively, are characterized and compared to those of the as-synthesized samples. Interestingly, the Si-rich phases that network in the as-synthesized state are discontinuously separated, and the size of the particle-shaped Si phases becomes large and spherical as the heat-treatment temperature increases. Due to these morphological changes of Si-rich phases, the reduction in tensile strengths and increase in elongations, respectively, can be obtained by the post-heat treatment process. These results provide fundamental information for the practical applications of AlSi10Mg parts fabricated by SLM.