The analytical method for 16 organophosphorus pesticides was developed in this study. The 16 organophosphorus pesticides were analyzed by liquid chromatography-tandem mass spectrometry (LC/MS/MS) using on-line solid phase extraction (on-line SPE) with PLRP- S cartridge. Analysis of all analytes in the MS/MS was processed in the electrospray ioni-zation (ESI) positive mode. They are Azinphos ethyl, Chlorfenvinphos, Ethion, Famphur, Phosmet, Phosphamidon, Terbufos, Aspon, Chlorpyrifos-methyl, Crotoxyphos, Dichlofenthi-on, Dicrotophos, Fonofos, Thionazin, Dimethoate and Iprobenfos. Limits of detection (LODs) and Limits of quantification(LOQs) were obtained as 0.8~2.0 ng/L and 2.6~6.4 ng/L, respectively. All compounds were not detected at the 8 sampling points of the raw water and clean water.
In this study, a new idea for developing a space scale for measuring mass in a microgravity environment was proposed by using the inertial force properties of an object to measure its mass. The space scale detected the momentum change of the specimen and reference masses by using a load-cell sensor as the force transducer based on Newton’s laws of motion. In addition, the space scale calculated the specimen mass by comparing the inertial forces of the specimen and reference masses in the same acceleration field. By using this concept, a space scale with a capacity of 3 kg based on the law of momentum conservation was implemented and demonstrated under microgravity conditions onboard International Space Station (ISS) with an accuracy of ±1 g. By the performance analysis on the space scale, it was verified that an instrument with a compact size could be implemented and be quickly measured with a reasonable accuracy under microgravity conditions.
This study reviewed sulfuric acid resistance of high acid resistance of inorganic binder based on industrial by-products. As the results of test, the mix of high acid resistance of inorganic binder showed the excellent chemical resistance against aqueous solution of 10% H2SO4 comparing to the mix of OPC, however, the mass of inorganic binder rather increased while approximately 3.4% of mass loss ratio appeared during 7 days of material age of soaking in case of using portland cement usually.
Marine mass concrete mixture for floating structures is derived that can minimize heat of hydration and several construction methods are investigated to reduce thermal cracks. Analysis variables are type and amount of mineral admixtures, number of lifts and placing interval. Probability of thermal crack occurrence is evaluated.
이 글은 바흐의 세속칸타타를 담론의 중심으로 끌어들이려는 노력의 일환으로 기획된 것 이다. 이를 위해 이 글은 1733년을 주목한다. 바흐담론에서 1733년은 바흐의 《1733년 미 사》가 작곡되고 이것이 드레스덴 궁정에 헌정된 해로 기억되고 있다. 그러나 바흐담론은 이 시기 바흐가 모두 5곡의 세속칸타타를 작곡하였고, 이들 역시 드레스덴 궁정에 헌정되었다 는 사실을 과소평가하고 있다. 이 글이 시도하는 것이 이러한 기존의 시각에서 종교와 세속 의 날선 구분을 잠시 내려놓은 채 이것을 넘어선 바흐의 일상을 재구성하는 일이다. 이는 바 흐의 세속칸타타(또는 그의 《1733년 미사》)를 작곡가의 ‘특별한 과외 활동’으로 간주하지 않고, 그의 음악활동의 일상으로 이해하려는 노력이며 또한, 이것은 드레스덴을 향한 바흐의 동경, 또는 야심이 그의 대표작인 《1733년 미사》뿐 아니라 이 시기 작곡된 그의 세속칸타 타들을 통해서도 일관되게 구현되었다는 것을 말하려는 시도이기도 하다.
Spontaneous rupture of the carotid artery is rare, however, it is a fatal injury and early diagnosis is very important. We expe-rienced a 54-year-old male patient who presented to the emergency department with an expanding neck mass after cough. Rupture of the common carotid artery 2 cm before bifurcation with a pseudoaneurysm was diagnosed on neck computed tomography angiography. Focal tear of the artery was repaired surgically with suture. Herein, we report on a rare occurrence of a spontaneous carotid artery rupture and review other reports.
This study investigates weekday/weekend characteristics of PM10 and PM2.5 concentration and metallic elements in Busan in the springtime of 2013. PM10 concentration on weekday/weekend were 77.54 and 67.28 ㎍/㎥, respectively. And PM2.5 concentration on weekday/weekend were 57.81 and 43.83 ㎍/㎥, respectively. Also, PM2.5/PM10 concentration ratio on weekdays/weekend was 0.75 and 0.65, respectively. The contribution rates of Na to total metallic elements in PM10 on weekday/weekend were 38.3% and 38.9%, respectively. It would be useful in control effectively with management of urban fine particle to understand characteristics of fine particle concentration on weekday/weekend.
We present a by-product of our long term photometric monitoring of cataclysmic variables. 2MASS J18024395 +4003309 = VSX J180243.9 +400331 was discovered in the field of the intermediate polar V1323 Her observed using the Korean 1-m telescope located at Mt. Lemmon, USA. An analysis of the two-color VR CCD observations of this variable covers all the phase intervals for the first time. The light curves show this object can be classified as an Algol-type variable with tidally distorted components, and an asymmetry of the maxima (the O’Connell effect). The periodogram analysis confirms the cycle numbering of Andronov et al. (2012) and for the initial approximation, the ephemeris is used as follows: Min I. BJD = 2456074.4904+0.3348837E . For phenomenological modeling, we used the trigonometric polynomial approximation of statistically optimal degree, and a recent method “NAV” (“New Algol Variable”) using local specific shapes for the eclipse. Methodological aspects and estimates of the physical parameters based on analysis of phenomenological parameters are presented. As results of our phenomenological model, we obtained for the inclination i=90°, M1=0.745M◉, M2=0.854M◉, M=M1+M2=1.599M◉, the orbital separation a=1.65·109m=2.37R◉ and relative radii r1=R1/a=0.314 and r2=R2/a=0.360. These estimates may be used as preliminary starting values for further modeling using extended physical models based on the Wilson & Devinney (1971) code and it's extensions
Atmospheric aerosol particles were investigated at GNTECH university in Jinju city. Samples were collected using the Nanosampler period from January to December 2014. The Nanosampler is a 6 stage cascade impactor(1 stage : > 10 μm, 2 stage : 2.5~10 μm, 3 stage : 1.0~2.5 μm, 4 stage : 0.5~1.0 μm, 5 stage : 0.1~0.5 μm, back-up : < 0.1 μm) with the stages having 50% cut-off ranging from 0.1 to 10 μm in aerodynamic diameter.
The mass size distribution of Atmospheric aerosol particles was unimodal with peak at 1.0~2.5 μm or 0.5~1.0 μm. The annual average concentrations of TSP, PM10, PM2.5, PM1, PM0.5 and PM0.1 were 44.0 μg/m3, 40.3 μg/m3, 31.4 μg/m3, 18.0 μ g/m3, 8.2 μg/m3, 3.0 μg/m3, respectively. On average PM10, PM2.5, PM1, PM0.5 and PM0.1 make up 0.91, 0.70, 0.41, 0.19 and 0.07 of TSP, respectively. The annual average of PM2.5/PM10 ratio was 0.77.
This study presents the concept of a multi-functional Tuned Mass Damper (TMD) using piezocomposite element as damping component. This new type of TMD intends to exploit the unused energy produced by the traffic-induced vibrations of the bridge structure for the generation of electric power while fulfilling its natural role of reducing undesirable vibrations in the structure. Since the proposed TMD is still in a development stage, this paper summarizes the concept underlying the mechanism of the TMD.
산악지형이 많은 우리나라의 지형적 특성상 터널은 장대화, 대단면화 되어 가고 있으며 다양한 암반을 관통하여 시공된다. 특히 도로, 철도 터널의 시종점부는 암반 구성 조건이 상부로부터 붕적토, 풍화암, 연암 등으로 구성되며 아칭 효과(Arching Effect)를 많이 기대할 수 없어 보조, 보강 공법을 적용한다. 따라서 안정한 시공을 위해 터널 시공 전에 수치 해석을 실시하여 보강 여부, 범위를 검토한 후 실제 시공 중에 발생한 변형, 응력 등 계측 결과와 수치 해석 결과를 서로 비교 검토(Feed Back) 하는 과정이 필요하다. 본 연구에서는 비교적 얕은 토피고를 갖는 풍화암 지반의 터널 시종점부에 대한 유한요소해석(Finite Element Analysis, FEA)과 실제 시공 중에 계측한 결과를 비교하여 터널의 안정성 여부를 최종 확인하였다.
The uneven mass distribution of the Moon highly perturbs the lunar spacecrafts. This uneven mass distribution leads to peculiar dynamical features of the lunar orbiters. The critical inclination is the value of inclination which keeps the deviation of the argument of pericentre from the initial values to be zero. Considerable investigations have been performed for critical inclination when the gravity field is assumed to be symmetric around the equator, namely for oblate gravity field to which Earth’s satellites are most likely to be subjected. But in the case of a lunar orbiter, the gravity field of mass distribution is rather asymmetric, that is, sectorial, and tesseral, harmonic coefficients are big enough so they can’t be neglected. In the present work, the effects of the first sectorial and tesseral harmonic coefficients in addition to the first zonal harmonic coefficients on the critical inclination of a lunar artificial satellite are investigated. The study is carried out using the Hamiltonian framework. The Hamiltonian of the problem is cconstructed and the short periodic terms are eliminated using Delaunay canonical variables. Considering the above perturbations, numerical simulations for a hypothetical lunar orbiter are presented. Finally, this study reveals that the critical inclination is quite different from the critical inclination of traditional sense and/or even has multiple solutions. Consequently, different families of critical inclination are obtained and analyzed.
Ambient particulate matters(PM10 and PM2.5) were investigated at GNTECH university in Jinju city. Samples were collected using a dichotomous sampler(series 240, Andersen Corp.) and a TEOM(Tapered Element Oscillating Microbalance) monitor period from November 2012 to October 2013. For the dichotomous sampler measurements, daily 24-h integrated PM2.5 and PM10–2.5 ambient air samples were collected at a total flow rate of 16.7 L /min. For the TEOM monitor measurements, daily 1-h integrated PM10 ambient air samples were collected at a flow rate of 16.7 L /min. The annual average concentrations of PM10-2.5 and PM2.5 by a dichotomous sampler were 10.0±6.1 μg/m3 and 22.6±9.3 μg/m3, respectively. And PM10 concentration by dichotomous sampler were similar to TEOM monitor by 32.7±12.9 μg/m3 and 31.7±11.3 μg/m3, respectively. And good correlation (R2=0.964) between the two methods was observed. The annual average of PM2.5/PM10 ratio was 0.70±0.12.
Vertical pipe cooling method was developed for the thermal cracking control of vertically long and slender mass concrete member. This method was applied to mass concrete wall, and the performance of this method was investigated.
본 연구에서는 건물의 질량중심과 면진층의 강성중심 사이의 차이에 따른 면진효과에 대하여 살펴보았다. 면진기술은 면진층에 설치되는 면진장치의 성능에 크게 의존하는 기술이므로 면진장치 제작 후 전수검사를 통하여 면진장치의 수평강성을 검토하게 되어 있다. 하지만면진장치 성능실험 시 각각의 면진장치의 품질기준은 건축기준에는 정해져 있지 않으며, 이로 인해 설계 시 적용된 강성과 실제 강성의 차이가 발생하여 면진층 상부 부재에 큰 문제를 야기할 수 있다. 연구결과, 최대응답변위의 차이는 크게 나타나지 않았으나 편심이 증가할수록 최대응답가속도, 층전단력 및 상부구조의 부재력은 크게 증가하여 일부 부재에서는 과도한 손상이 예상된다. 따라서 면진층은 실제 장치제작 후 전수검사를 실시하여 반드시 설계된 의도대로 편심이 발생하지 않도록 장치를 재배치할 필요가 있으며, 가능하다면 건물의 질량중심과 강성중심의 차이는 동일하게 설계할 것을 추천한다.
This experiment was carried out to establish the optimum cutting time, plant growth regulator, and bed-soilfor rooting by greenwood cutting of Schisandra chinensis. Approximately 7㎝ long-shoots of greenwood cuttings weretransplanted by various cutting times, plant growth regulators, and bed-soils in the plastic-film house. The rooting rate ofgreenwood cutting was 12.5% in the April 5th, 73.5% in the May 8th, and 75.5% in the August 5th. The number and lengthof primary root in greenwood cutting were more in the early May than those in the early August. For mass propagation ofSchisandra chinensis. using greenwood cutting, shoots were treated with plant growth regulators on May to increase rootingrate. Rooting rate was 100% with IAA 50㎎/ℓ,92.9% with NAA 100㎎/ℓ,and NAA 1,000㎎/ℓ,for 60 min. To selecteffective media for rooting, various medias for bed-soil were treated by single and mixture form for 100 days after cutting.Rooting rate was 91.8% in the single treatment of peat moss or decomposition of granite soil, and this result was better thanthose in other treatment. The treatment by 1:1 mixture of peat moss and horticulture bed soil was rooting with 94.0% bestrooting rate.
상용의 GoldSim과 GoldSim 이동 모듈 (GoldSim Transport Module; GTM)을 이용하여 방사성폐기물 처분시스템과 같이 복 잡한 질량 이동 시스템을 신뢰성 있고 효율적으로 모사할 수 있다. 그러나 GTM의 특성을 보다 정확하게 이해하여야 이를 사용하여 실제 처분시스템의 안전성 평가 프로그램을 개발할 때 발생할 수 있는 오류를 피할 수 있다는 것을 인지하는 것이 중요하다. 이를 위하여 GTM에서 다양하게 제공되는 요소 (element) 중, 질량 이동 모사에 유용한 Transport pathway의 특 징에 대하여 소개하고, 방사성폐기물 처분시스템 안전성 평가를 위해 시스템 내 핵종의 거동과 같은 질량 이동 모사에서 이 에 대한 올바른 활용 방안을 제시하였다.
The number concentrations, the mass concentrations and the elemental concentrations of PM10 have measured at Gosan site in Jeju, Korea, from March 2010 to December 2010. And the correlation and the factor analysis for the number, the mass and the elemental concentrations of PM10 are performed to identify their relationships and sources. The average PM10 number concentration is observed 246 particles/㎝3(35.7∼1,017 particles/㎝3) and the average PM10 mass concentration is shown 50.1 ㎍/㎥(16.7∼441.4 ㎍/㎥) during this experimental period. The number concentrations are significantly decreased with increasing particle size, hence the concentrations for the smaller particles less than 2.5 ㎛(PM2.5) are contributed 99.6% to the total PM10 number concentrations. The highest concentration of the 20 elements in PM10 determined in this study is shown by S with a mean value of 1,497 ng/㎥ and the lowest concentration of them is found by Cd with a mean value of 0.57 ng/㎥. The elements in PM10 are evidently classified into two group based on their concentrations: In group 1, including S>Na> Al>Fe>Ca>Mg>K, the elemental mean concentrations are higher than several hundred ng/㎥, on the other hand, the concentrations are lower than several ten ng/㎥ in group 2, including Zn>Mn>Ni>Ti>Cr>Co>Cu>Mo>Sr>Ba>V >Cd. The size-separated number concentrations are shown positively correlated with the mass concentrations in overall size ranges, although their correlation coefficients, which are monotonously increased or decreased with size range, are not high. The concentrations of the elements in group 1 are shown highly correlated with the mass concentrations, but the concentrations in group 2 are shown hardly correlated with the mass concentrations. The elements originated from natural sources have been predominantly related to the mass concentrations while the elements from anthropogenic sources have mainly affected on the number concentrations of PM10.
Adsorption of phenol on activated carbon in a fixed bed was studied. The effects of fixed-bed length, superficial velocity (flow rate) and particle size of adsorbent on fixed-bed performance were investigated. Some characteristic parameters such as the breakthrough time (t0.05), saturation time (t0.95), length of mass transfer zone (LMTZ), adsorptive capacity (W), and adsorption rate constant (Ka) were derived from the breakthrough curves. Adsorbent particle sizes significantly affected the shape of the breakthrough curve. Larger particle sizes resulted in an earlier breakthrough, a longer LMTZ and a lower adsorption rate. Superficial velocity was a critical factor for the external mass transfer during fixed-bed adsorption process. The external mass transfer resistance was dominant as increasing superficial velocity.