The characteristics of abrasive wear on sliding speed of glass fiber reinforcement (GF/PUR) composites were investigated at ambient temperature by pin-on-disc friction test. The cumulative wear volume, friction coefficient and surface roughness of these materials on sliding speed were determined experimentally. The major failure mechanisms were lapping layers, deformation of resin, ploughing, delamination, and cracking by scanning electric microscopy (SEM) photograph of the tested surface. As increasing the sliding speed the GF/PUR composites indicated higher friction coefficient. The surface roughness of the GF/PUR composites was increased as the sliding speed was higher in wear test.

Glasses were prepared with compositions of (13-x)BaO-80B2O3-7Li2O·xSm2O3, BBLSx(x=0.5, 0.4, 0.3) by melting the starting materials of boron oxide(99.9%), lithium oxide(99.9%), barium carbon oxide(99.9%), and samarium oxide(99.9%) and then quenching the melt at 1350˚C. This led to good-quality BBLSx(x=0.4, 0.3) and poor-quality BBLSx(x=0.5) glasses. The physical and structural properties of the BBLSx glasses were studied by means x-ray diffraction, scanning electron microscopy(SEM), differential scanning calorimetry(DSC), and dielectric spectroscopy. From the x-ray diffraction and SEM results, the quality of the BBLSx glasses significantly depends on the Sm2O3 concentration. The x-ray diffraction pattern showed that the crystallites in the BBLSx glasses after heat treatment at 700˚C may be LiBaB9O15. From the DSC results, the glass transition temperatures(Tg), crystallization temperatures(Tc), and the maximum temperatures of the crystallized(Tp) BBLSx glasses all changed with the Sm2O3 concentration. According to the dielectric spectroscopy results, the values of the real dielectric constant and Tan δ of the BBLSx glasses depended on the Sm2O3 concentration. The values of the real dielectric constant and Tan δ were also shown to depend on the measuring temperature, possibly due to the ion migration in the bulk of the BBLSx glasses.

본 연구에서는 유리단섬유로 보강된 분사식 섬유보강 복합재료의 인장거동 평가를 위한 실험 및 해석연구를 수행하였다. 이를 위해 다양한 변형율속도(strain rate)에 따른 에폭시수지 및 분사식 섬유보강 복합재료의 인장강도 실험을 수행하였다. 본 연구에 사용된 분사식 섬유보강 복합재료는 15mm 길이로 절단된 유리단섬유가 25% 부피비율로 혼입된 보수·보강용 재 료이다. 에폭시수지의 점탄성 특성을 고려하기 위해 역산모델링(inverse simulation)을 수행하여 변형율속도에 따른 점성변화 를 함수식으로 제안하였다. 역산모델링을 통해 제안된 함수식을 미세역학 기반의 점탄성 손상모델(micromechanics-based viscoelastic damage model; Yang et al., 2012)에 적용하여 분사식 섬유보강 복합재료의 인장거동을 수치적으로 해석하였다. 분사식 섬유보강 복합재료의 인장거동 해석결과와 실험결과를 비교하여 미세역학 기반의 점탄성 손상모델의 정확성을 검증 하였다.

The objective of this study was to investigate the effectiveness of cryopreservation methods for the effect of various vitrification containers, such as EM-grid, OPS, or cryo-loop on the survival and developmental rate of vitrified mouse pronuclear embryos, and mouse cleavage embryo, at 21, 24, 27 and 30 hr after hCG injection. Post-thaw cleavage was similar among treatments, while the developmental rates of mouse blastocyst and hatched blastocyst were higher ( <0.05) in 27 hr and 30 hr than 21 hr. The developmental rate of hatched blastocyst at vitrified cleavage mouse embryos in cryo-loop was significantly higher than vitrified pronuclear embryos of control group as well as EM-grid and OPS ( <0.05). The developmental rate using cryo-loop was higher than EM-grid, but in case of OPS at vitrified cleavage and mouse pronuclear embryos, no significant difference was noticed. These results of our study show that the developmental rates of mouse embryos were unaffected by various vitrification containers, but in case of mouse embryos and hatched blastocysts at late vitrified pronuclear embryos the developmental rates were higher than early vitrified pronuclear embryos. Moreover, the developmental rate of hatched blastocyst at vitrified cleavage mouse embryos was significantly higher than vitrified pronuclear embryos. For better execution of this study, it will be mandatory to include improvement of vitrification containers, cryopreservation methods and conditions, higher survival rate, safe preservation, contamination and embryo loss.

A Li2O-2SiO2 (LS2) glass was investigated as a lithium-ion conducting oxide glass, which is applicable to a fast ionic conductor even at low temperature due to its high mechanical strength and chemical stability. The Li2O-2SiO2 glass is likely to be broken into small pieces when quenched; thus, it is difficult to fabricate a specifically sized sample. The production of properly sized glass samples is necessary for device applications. In this study, we applied spark plasma sintering (SPS) to fabricate LS2 glass samples which have a particular size as well as high transparency. The sintered samples, 15mmφ×2mmT in size, (LS2-s) were produced by SPS between 480˚C and 500˚C at 45MPa for 3~5mim, after which the thermal and dielectric properties of the LS2-s samples were compared with those of quenched glass (LS2-q) samples. Thermal behavior, crystalline structure, and electrical conductivity of both samples were analyzed by differential scanning calorimetry (DSC), X-ray diffraction (XRD) and an impedance/gain-phase analyzer, respectively. The results showed that the LS2-s had an amorphous structure, like the LS2-q sample, and that both samples took on the lithium disilicate structure after the heat treatment at 800˚C. We observed similar dielectric peaks in both of the samples between room temperature and 700˚C. The DC activation energies of the LS2-q and LS2-s samples were 0.48±0.05eV and 0.66±0.04eV, while the AC activation energies were 0.48±0.05eV and 0.68±0.04eV, respectively.

본 연구는 19세기에 그려진 추사(秋史) 김정희(金正喜)의 <세한도(歲寒圖)>가 당대와 현대를 가로지르면서 시대적, 문화적 차이를 통해 수용된 다층성을 밝히고자 한다. 김정희는 조선후기의 뛰어나 서화가(書畵家)이자 금석학자(金石學者)이자 실학자(實學者)이다. 그는 1844년, 그의 나이 58세 때에 제주도로 귀양을 가게 되었다. 그때 김정희를 기억해준 유일한 제자, 역관 ‘李尙迪’을 기리는 마음으로 <세한도>를 그렸다. 이 <세한도>는 네 종류의 글로 오늘날까지 기억되고 있다. 그 첫 번째는 김정희가 이상적을 기리기 위한 발문이다. 두 번째는 이상적이 김정희의 의사와 무관하게 정치적인 이유로 청나라 명사 16인에게 보여주고 받은 찬문찬시이다. 세 번째는 광복 후 김석준, 오세창, 이시영이 더한 찬문찬시이다. 네 번째는 황지우를 비롯한 여러 시인이 남긴 현대시이다. 롤랑 바르트가 제기한 것처럼, 하나의 기호는 2차 의미체계에 의해 새로운 의미를 생성해낸다. 그런 측면에서 바라볼 때, 추사 김정희의 <세한도>는 오늘날 황지우의 <유리끼운 세한도>에 영향을 미쳤다. 추사 김정희가 <세한도>를 통해 자신에게 의리를 지킨 이상적을 기억하며 19세기의 ‘의’를 밝혔다면, 황지우는 추사 <세한도>를 20세기에 불러내어 현 시대의 문제와 해결방안을 제시하였다. 즉 거대담론이 사라진 것처럼 인식된 현실세계에서 추사 김정희의 <세한도>를 다시금 불러 세워, 아직은 사회적 문제, 거대담론의 문제로 행동해야할 때임을 드러냈던 것이다. 추사 김정희의 <세한도>는 당대 개별적 작품성뿐만 아니라 시대를 넘나드는 시대사적 의의를 지닌다. 이를 드러낸 현대 시인이 바로 황지우이다.

Squid ink was added to the low salt fermented squid by 4% of concentration and ripened at 10℃ for 6 weeks and at 20℃ for 28 days. The effect of the squid ink on the titrable acidity and free amino acids of low salt fermented squid were investigated. The results are as follows; The titrable acidity in the salt fermented squid without addition of the squid ink was continuously decreased except for the salt fermented squid with 9% salt content till the latter stage of the ripening, had larger decreasing range than treatment groups. Seeing the composition of free amino acid, the major amino acids are proline, arginine, glutamic acid. leucine and glycine.

This study was carried out to investigate the effect of muscle part and aging period on free amino acids and aroma compounds of Hanwoo (Korean cattle) cow beef. The M. longissimus (ML) and M. semitendinosus (MS) from 101 mon-old-cows were aged at 2℃ for 14 d. The free amino acids concentration increased in both ML and MS on 14 d of aging. In ML, asparagine, glutamine, histidine, glycine, threonine, arginine, tyrosine, phenylalanine, isoleucine, leucine and lysine were significantly (p<0.05) higher than those in MS. Varieties of aldehydes, ketones, alcohols, hydrocarbons, nitrogen and sulfur compounds were detected in both ML and MS and majority of these compounds showed increasing trend on aging. The ML had higher 14 aldehydes (acetaldehyde, 2-methylpropanal, 3-methylbutanal, 2- methylbutanal, pentanal, hexanal, heptanal, E-2-heptanal, octanal, 2-octenal, 2-nonenal, E-2-decenal, E,E-2,4-decadienal and 2-undecenal), 5 ketones (2-propanone, 2,3-butanedione, 2-butanone, 2-heptanone and 2,3-octanedione), 4 alcohols (ethanol, 1-pentanol, 1-hexanol and 1-octanol), 3 hydrocarbons (3-ethyl-2-methyl-1,3-hexadiene, 3- methyldecane and 2,2-dimethyloctane) significantly (p<0.05) compared with MS. However, the MS had higher 5 nitrogen and sulfur compounds (methanethiol, dimethyldisulfide, fufural, 2,5-dimethylpyrazine and 2-octylfuran) significantly (p<0.05) compared with ML.

유리강회플라스틱(GRP)은 재료의 자중에 비해 아주 높은 강도를 가지고 있다. 또한 부재의 두께에 따라서 투명 혹은 반투명의 효과를 거둘 수 있다. 하지만 Hand laminating의 특성상 일률적인 재료의 강도를 선뢰하기 어렵기 때문에 구조 계산 혹은 설계 시 반드시 재료 실험을 수행하여야한다. 본 논문은 두께 4mm, 높이 30m의 의장적 기둥을 구조적으로 설계하기 위한 재료 실험을 수행하였다. 또한 실험 결과에 대한 평가를 통해 DIN에서 규정하는 재료적인 강도와 비교 분석하였다. 이를 통해 규준에서 제시하는 값과의 차이를 확인했으며 실제 설계에 반영하기 위해 반드시 재료실험이 수행되어야함을 알 수 있다.

 ,  , Synanthedon velox (Fixsen) is redescribed and the genus Bembecia is reported for the first time from Korea with B. pavicevia Tosevski, Description, images of the adult, genitalia, and the Korean common names of two species are provided. Their host plants are listed and their biology is briefly summarized.

The present study was performed to investigate the survival and subsequent embryonic developmental rate of immature and mature oocytes after vitrification and pronuclear stage embryos after slow-freezing and vitrification. We have also tried to examine the dependency of concentrations (7.5, 15%) and exposure time (5, 10, 20 min) of ED cryoprotectant on developmental rate of pronuclear stage embryos. The developmental rates of 2-ce1l and blastocyst embryos at mature oocytes were significantly (p<0.05) higher than immature oocytes. After slow freezing, vitrification and thawing of pronuclear stage embryo, the survival and developmental rates of blastocysts and hatched blastocysts were significantly (p<0.05) higher after vitrification than after slow-freezing. On contrary, the developmental rates of 2-cell embryos were significantly (p<0.05) higher after slow freezing than after vitrification. The cryopreservation methods of pronuclear stage embryos vitrified by exposed to 7.5% ED solution for 5 minutes was significantly (p<0.05) higher than other experimental group. The results of our study suggest 1hat the developmental rates of mature oocytes have been more successful than immature oocytes during vitrification. Vitrification was more efficient than slow freezing in case of pronuclear stage embryos. The effective cryopreservation method of pronuclear stage embryos was vitrified by exposed to 7.5% ED solution for 5 minutes.