Environmental pollution has led to global warming, which threatens human life. In response, hydrogen is gaining attention as a next-generation energy source that does not emit carbon. Due to its explosive nature, special care must be taken in the safe storage and transportation of hydrogen. Among various storage methods, liquefied storage, which can reduce its volume to 1/800, is considered efficient. However, since its boiling point reaches -253°C, the design of an insulation system is essential. For the design of insulation systems applied to large containers, a membrane-type design is required, which necessitates the use of cryogenic adhesives. To evaluate whether the cryogenic adhesive is properly implemented, assessments such as tensile and shear tests are necessary. This study presents a methodology for shear evaluation. Conventional methods for shear evaluation of adhesives result in slippage, preventing proper assessment. Therefore, a method involving drilling holes in the gripper and pulling from the holes must be applied. Optimal design concerning the size and location of the holes is required, and this study derives optimal values based on finite element analysis. By conducting experiments based on the results of this study, it is expected that the risk of gripper damage will be minimized, allowing for accurate evaluation of the adhesive’s performance.
PURPOSES : Pavement surface friction depends significantly on pavement surface texture characteristics. The mean texture depth (MTD), which is an index representing pavement surface texture characteristics, is typically used to predict pavement surface friction. However, the MTD may not be sufficient to represent the texture characteristics to predict friction. To enhance the prediction of pavement surface friction, one must select additional variables that can explain complex pavement surface textures. METHODS : In this study, pavement surface texture characteristics that affect pavement surface friction were analyzed based on the friction mechanism. The wavelength, pavement surface texture shape, and pavement texture depth were hypothesized to significantly affect the surface friction of pavement. To verify this, the effects of the three abovementioned pavement surface texture characteristics on pavement surface friction must be investigated. However, because the surface texture of actual pavements is irregular, examining the individual effects of these characteristics is difficult. To achieve this goal, the selected pavement surface texture characteristics were formed quantitatively, and the irregularities of the actual pavement surface texture were improved by artificially forming the pavement surface texture using threedimensionally printed specimens. To reflect the pavement surface texture characteristics in the specimen, the MTD was set as the pavement surface texture depth, and the exposed aggregate number (EAN) was set as a variable. Additionally, the aggregate shape was controlled to reflect the characteristics of the pavement surface texture of the specimen. Subsequently, a shape index was proposed and implemented in a statistical analysis to investigate its effect on pavement friction. The pavement surface friction was measured via the British pendulum test, which enables measurement to be performed in narrow areas, considering the limited size of the three-dimensionally printed specimens. On wet pavement surfaces, the pavement surface friction reduced significantly because of the water film, which intensified the effect of the pavement surface texture. Therefore, the pavement surface friction was measured under wet conditions. Accordingly, a BPN (wet) prediction model was proposed by statistically analyzing the relationship among the MTD, EAN, aggregate shape, and BPN (wet). RESULTS : Pavement surface friction is affected by adhesion and hysteresis, with hysteresis being the predominant factor under wet conditions. Because hysteresis is caused by the deformation of rubber, pavement surface friction can be secured through the formation of a pavement surface texture that causes rubber deformation. Hysteresis occurs through the function of macro-textures among pavement surface textures, and the effects of macro-texture factors such as the EAN, MTD, and aggregate shape on the BPN (wet) are as follows: 1) The MTD ranges set in this study are 0.8, 1.0, and 1.2, and under the experimental conditions, the BPN (wet) increases linearly with the MTD. 2) An optimum EAN is indicated when the BPN (wet) is the maximum, and the BPN decreases after its maximum value is attained. This may be because when the EAN increases excessively, the space for the rubber to penetrate decreases, thereby reducing the hysteresis. 3) The shape of the aggregate is closely related to the EAN; meanwhile, the maximum value of the pavement surface friction and the optimum EAN change depending on the aggregate shape. This is believed to be due to changes in the rubber penetration volume based on the aggregate shape. Based on the results above, a statistical prediction model for the BPN (wet) is proposed using the MTD, EAN, and shape index as variables. CONCLUSIONS : The EAN, MTD, and aggregate shape are crucial factors in predicting skid resistance. Notably, the EAN and aggregate shape, which are not incorporated into existing pavement surface friction prediction models, affect the pavement surface friction. However, the texture of the specimen created via three-dimensional printing differs significantly from the actual pavement surface texture. Therefore, the pavement surface friction prediction model proposed in this study should be supplemented with comparisons with actual pavement surface data in the future.
The influence of specimen geometry and notch on the hydrogen embrittlement of an SA372 steel for pressure vessels was investigated in this study. A slow strain-rate tensile (SSRT) test after the electrochemical hydrogen charging method was conducted on four types of tensile specimens with different directions, shapes (plate, round), and notches. The plate-type specimen showed a significant decrease in hydrogen embrittlement resistance owing to its large surface-to-volume ratio, compared to the round-type specimen. It is well established that most of the hydrogen distributes over the specimen surface when it is electrochemically charged. For the round-type specimens, the notched specimen showed increased hydrogen susceptibility compared with the unnotched one. A notch causes stress concentration and thus generates lots of dislocations in the locally deformed regions during the SSRT test. The solute hydrogen weakens the interactions between these dislocations by promoting the shielding effect of stress fields, which is called hydrogen-enhanced localized plasticity mechanisms. These results provide crucial insights into the relationship between specimen geometry and hydrogen embrittlement resistance.
This study aims to examine the correlation between microstructures and the mechanical properties of two highstrength API X70 linepipe steels with different specimen directions and Moaddition. The microstructure of the Mo-added steel has an irregularly shaped AF, GB matrix with pearlite because of the relatively large deformation in the non-recrystallization temperature region, while that of the Mo-free steel shows a PF matrix with bainitic microstructure. In the Mo-added steel, the M/A (martensite-austenite) in granular bainite (GB) and pearlite act as crack initiation sites with decreased upper shelf energy and an increased ductile to brittle transition temperature (DBTT). Regardless of Mo addition, all of the steels demonstrate higher strength and lower elongation in the T direction than in the L direction because of the short dislocation glide path and ease of pile-up at grain boundaries. In addition, the impact test specimens with T-L direction had a lower impact absorbed energy and higher DBTT than those with the L-T direction because the former exhibit shorter unit crack path compared to the latter.
Several tests should be performed to estimate the structural and chemical stability of the radioactive waste. Among the tests in Gyeongju LILW repository, the leaching test which follows ANS 16.1 standard test method should be conducted for Cs, Sr, and Co radionuclides and must satisfy leachability index larger than 6 which applies deionized water as a leachant. However, the expected leachant inside the silo is groundwater that contains various ions and a high pH condition is predicted due to the concrete structures inside the silo. According to the chemical environment of the leachant, the chemical form of the radionuclides varies from precipitate to ion. Cobalt precipitates when the leachant has high pH environment which is similar condition to the cement-saturated leachant. Unlike the cobalt, cesium is preferred to exist as ion in the high pH condition. Therefore, the significant effect of the chemical environment of the leachant on the leachability of the radionuclides should be considered for the waste acceptance criteria of the radioactive waste repository. From the ‘NRC, Technical position on the waste form, rev1’, the leaching test method should follow the ANS 16.1 methods by using deionized water as leachant, however, a new leachant showing more aggressive leachability can be applied instead of deionized water. In the other hand, ASTM C1308 leaching test method recommends applying actual groundwater of the repository as a leachant. FT-04-020, the leaching test method of France, suggests the ion composition of the groundwater including the pH value. Therefore, the adequacy of using deionized water as leachant for the leaching test method of Cs, Sr, and Co should be re-examined. In this study, the leaching behavior of Cs, Sr, and Co under the several leachant types is estimated. The cement solidified specimen containing single Cs, Sr, and Co were manufactured. The leaching test following ANS 16.1 was performed by applying deionized water, simulated groundater, and cement-saturated groundwater. As a result, a leachability index difference according to the leachant type was discussed. The result of this study is expected to be a background data that helps understanding the actual leaching behavior of the Cs, Sr, and Co in the Gyeongju LILW repository.
In this study, measurement errors of the X and Y axes were verified by using an 80-100 mm gauge block, an NPL type angle measuring device, and a spelling on a contact-type 3D measuring device surface plate. In addition, the measurement specimen was repeatedly measured 10 times at 10° intervals from 0° to 40° to confirm the average value and standard deviation. After confirming the statistical test value (P) through ANOVA analysis of the statistical program, the correlation between angle change and error was confirmed.
Recently 3d printer industry has two demands. first is color 3d printing. second is mass production using 3d printer that has large bed. According to previous studies, 3D printed objects have different weights depending on filament colors. 3D printed tensile specimens with filaments of various colors were checked to see they had the same weight. If so, we wanted to see it was statistically significant. As a result, we found that the weight of 3D printed objects was statistically significantly different depending on the filament color. The average weight of 3d printed objects is: Black(8.63g), Blue(8.58g), Yellow(8.53g), White(8.48g), Natural(8.46g), Green (8.45g), Red(8.42g).
In this study, using a 100mm gauge block in a contact-type three-dimensional measuring machine surface plate, an NPL-type angle measurement, and a steel ruler, the specimen was measured at 0°, 5°, 10°, 20°, 30°, and 40° along the X and Y axes. After setting the measurement conditions, the average value and standard deviation were confirmed by repeating measurements for each yield 10 times. After checking the statistical test value (P) through ANOVA, the correlation between the angle change and the error was checked.
Low and intermediate radioactive wastes in South Korea have been disposed in Wolsong Low and Intermediate Level Radioactive Waste Disposal Center (WLDC), Gyeongju. This repository structure is planned to be operated few hundred years while toxicity of the waste is sufficiently decayed. The structural integrity of the repository is required to protect the waste in safe. The integrity of the structure is commonly estimated using acoustic emission (AE) method. The integrity of the structure using AE is obtained by following process: 1) Estimation of maximum acoustic crack energy of the structure, 2) Acoustic signal measurement and filtering, and 3) Measurement of simultaneous acoustic cracking energy. The damage of the structure can be obtained from cumulative cracking energy from the structure divided by the predicted maximum cracking energy of the structure. Estimation of maximum cracking energy is gained by the specimens whose components are identical to the repository structure. The cracking energy of the different specimens are obtained during uniaxial compressive test and volume of the specimen is calculated. Then, the fractal coefficient for the structure is obtained and the maximum crack energy of the target structure can be calculated. The specimens whose diameters vary from 50 mm to 150 mm and heights are twice of the diameter are made with same recipe of WLDC silo concrete. The uniaxial compression test is conducted with loading rate of 0.1 mm·min−1. The fractal coefficient is obtained by least square method from the volume-cumulative energy relationship.
In this introduction, test devices for radwaste characterization specimen was developed and utilized. In order to permanently dispose of solidified radwastes, not only radioactive characterization but also physical & chemical characterization shall be performed to assess compliance with the waste acceptance criteria. Waste acceptance criteria can be made up measurement of free standing water, compressive strength test, thermal cycling test, radiation resistance test, leaching test, immersion test. Approximately, the equipment for each test is sorted out five types. equipment for making characterization specimen, equipment for compressive strength test, equipment for thermal cycling test, equipment for radiation resistance test, equipment for Immersion test and leaching test. Equipment for making characterization specimen is operated the dry process. The equipment of two types: one (sampling device) that cores solidified radioactive waste in a drum, and the other (cutting machine) that properly cuts the coring samples. Sampling device is not used in industry, so it is specially manufactured, cutting machine is using ready-made products. In addition, devices for compressive strength test and thermal cycling test are using ready- made products. Facility for Radiation resistance test is located in Jeong-eup. For the efficient test, a table was manufactured in the columnar form like the specimen. Finally, devices for immersion test and leaching test are so transformed that contact all surfaces of the specimen with the liquid.
Numerous low-and intermediate level radioactive wastes were generated from the decommissioning processes of nuclear power plants. Radionuclides such as Co and Cs contained in decommissioning wastes should be immobilized to prevent the release of radionuclides from the wastes due to its harmful impacts on ecosystem by high radioactivity and long half-life. Ethylenediaminetetraacetic acid (EDTA) used as decontamination agent can be contained in cement waste during decommissioning process of nuclear power plants. In addition, EDTA can be stably and strongly bound with radionuclides, resulting in the acceleration of the nuclide release from solidified cement matrix. Here, we investigated the effects of EDTA on leaching behaviors of Co and Cs immobilized in the cement specimen. The leaching tests were performed according to the ANS 16.1 “Measurement of the leachability of solidified low-level radioactive wastes by a short-term test procedure”. From the results, an increase in the EDTA content in the cement specimen led to an increase in Co leaching, whereas a decrease in Cs leaching. Leaching of Cs was dominantly controlled by diffusion from the pore space of the cement specimen to the solution. The effective diffusion coefficient and leachability index of nuclide were determined using the diffusion-release models of ANS 16.1. The results of present study can be used in the safety assessment for disposal of the radioactive waste generated by decommissioning of nuclear power plants.
During normal and off-normal conditions, the concrete structures of dry storage system for spent nuclear fuel must maintain structural integrity. A stress-strain curve is the most important key factor for structural integrity evaluation. The ASTM C39 specifies the concrete specimen geometry for the static compression test. However, there is no standard specimen size for intermediate stain rate, and it is not easy to maintain consistency among all test results because the failure tendency is different from each other. In order to account for the strain rate effects on concrete, the dynamic increase factor (DIF) is conventionally addressed by dividing dynamic strength by static strength. However, the DIF value considers only the strength of concrete and does not describe the overall behavior of concrete, such as a stress-strain relation. The objective of this study is to propose proper specimen geometry for the concrete dynamic compression test by several parametric study. The static compression simulation results with the specimen specified in ASTM C39 showed the constant strain distribution in a cylindrical specimen. However, as the strain rate increases, the strain state in specimen showed a nonuniform with the same geometry of ASTM C39. The non-uniform strain state in the specimen deteriorates the consistency and accuracy of the compression test. Therefore, we presented the specimen shape and size to form a uniform strain state through radial direction by drilling a hole in the axial direction. We analyzed two specimens using ABAQUS with the concrete damaged plasticity model, one with a hole at the center and the other without the hole. As a result, the strain distribution became more uniform than the specimen without the hole. Based on the results, we proposed the specimen shape and size for the intermediate strain rate compression test.
소변검사 전 냉/해동 반복과 해동 과정에 따라 대표적인 임상 화학검사 측정값의 변화를 확인 함으로써 소변검사의 안정성과 품질 개선방안을 모색하고자 하였다. 조사 대상자는 모두 건강한 남성 10명이었으며 이들의 소변 검체를 이용하여 냉/해동 안정성(freeze and thaw stability) 실험을 진행하였다. Micro-albumin과 Amylase의 경우 시간이 경과 됨에 따라 37℃에서 는 통계적 유의성은 없었으나, 42℃와 60℃에서는 시간의 경과에 따른 결과가 통계적으로 유의한 변동 이 있었고, BUN, Creatinine, Uric acid와 Glucose에서는 통계적으로 유의한 변동이 있었다. Long term의 안정성 결과, 7일이 지난 후에는 Glucose의 변이는 증가하였고, 60℃에서는 Amylase가 감 소하는 양상을 보였다. Glucose와 Amylase의 경우 시간의 경과에 따른 결과가 통계적으로 유의한 변동 이 있었다. 신뢰성 있는 검사결과를 얻기 위해서는 소변 시료의 채취, 보관 및 저장 등을 비롯한 요검사 의 정확한 표준화가 필요하며 생체 물질별 안정성 확보를 위한 조건들의 체계적 연구가 필요하다.
PURPOSES : In this paper, the measurement criteria was determined by assessing the factors influencing the measurement of bending resonance frequency which is not specified in KS F 2437. METHODS : The durability evaluation analysis of concrete beam specimens was performed immediately after freezing and thawing processes. It is primarily aiming at improving the repeatability and reproducibility of measurement results by providing measurement criteria for various measurement factors that can occur during the collection of resonance frequency data. An independent concrete durability test (KS F 2456) was executed with the proposed measurement protocol for evaluation.
RESULTS : A measurement protocol was proposed to determine the transverse resonance frequency of concrete beam specimens.
CONCLUSIONS : It was concluded that the proposed measurement protocol may be used for the concrete durability test; where the resonance frequency could be stably collected.
본 연구는 벨크로를 이용하여 콘크리트 공시체의 압축거동시 구속합축효과를 검토하였다. 벨크로(Velcro)는 갈고리 모양의 후크(Hook)와 고리모양의 루프(Loop)가 물리적으로 결합하여 접착력을 가지는 제품으로 다양한 형태를 가지고 있다. 벨크로 보강 공법은 접착제를 사용하지 않아 쉽고 빠른 시공이 가능하여 공사비가 낮고 시공 시 편리한 장점이 있다. 본 연구에서는 벨크로로 횡 구속된 콘크리트 압축부재에 대하여 보강면적변화에 따른 벨크로 횡구속 콘크리트 부재의 압축거동에 대하여 연구하였다. 벨크로로 보강된 시편의 압축거동을 조사하기 위하여 횡구속 콘크리트 시편을 제작, 보강면적변화에 따른 횡 구속 성능을 평가하였다. 보강면적은 50%, 75%, 100%로 설계하였다. 실험 결과 벨크로 보강에 의한 압축 강도 증가는 크게 증가하지 않았다. 또한 보강 전과 비교하여 구속 효과의 강도 증가도 미미했습니다. 그러나 항복점 이후의 거동에서는 연성 거동이 나타 났다. 본 연구를 통해 Velcro를 이용한 콘크리트 보강재 개발에 필요한 기본 정보로 활용할 수 있습니다.