In this study, Sparassis crispa(cauliflower mushroom), which is rich in beta-glucan, was pulverized using ultrafine grinding technology for its potential utilization as a diverse food ingredient. The physical and antioxidant properties of cauliflower mushroom powder were evaluated at various grinding times. The results showed that as the grinding time of cauliflower mushroom increased, the average particle size significantly decreased (p<0.05). Additionally, the water-holding capacity, swelling capacity, and water solubility index of cauliflower mushroom increased significantly(p<0.05). Based on the analysis mentioned above, cauliflower mushroom prepared as a superfine powder for 5 minutes exhibited superior physical and chemical properties as well as antioxidant characteristics and is expected to be widely used in various foods.

The antioxidant, physicochemical, and sensory properties of muffins using fermented Curcuma longa L. were investigated. Sensory properties of the samples were examined, and the correlation between the physicochemical, antioxidant, and sensory properties was studied. The pH of the samples was pH 7.26-7.42, which was the optimal pH range for the air formation of the dough, color, or volume. The antioxidant activities of the sample group were significantly higher than the control (p<0.05). In the sensory intensities, the 1.0 and 1.5%-added sample groups showed a similar savory aroma, sweet aroma, savory taste, sweet taste, and texture to those of the control. Samples containing 1.0 and 1.5% showed similar overall acceptance values to the control. The muffin containing 1.0 or 1.5% fermented Curcuma longa L. powder was developed successfully, and it was concluded that the developed muffin with the fermented turmeric powder could be a highly valued product in the increasingly competitive muffin food industry.

Thermal barrier coatings(TBCs) are being applied in many industrial fields such as thermal power generation, aviation and seasonal fields. ZrO2-Y2O3(8%) thermal spray coating powders are commercially used as thermal-barrier coating materials to protect against oxidation and corrosion of heat-resistant alloys at elevated temperatures. Currently, ZrO2-Y2O3(8%) thermal-spray powder is made using the industrial co-precipitation process, which is very complex and requires a lot of time. In this study, orthorhombic ZrO2 and Y2O3 powders were fabricated by mechanical mixing, which is more economical than the co-precipitation process. A tetragonal, yttria-stabilized zirconia(YSZ) coating-layer was produced by plasma spraying, using orthorhombic ZrO2-Y2O3(8%) powder. Our experimental results indicate that ZrO2-Y2O3(8%) mixed powder can be used economically in industry because it is no longer necessary to make this powder by liquid and gas-phase methods.

본 연구는 다양한 생리적 효능이 우수한 솔잎 분말을 첨가 (0, 3, 6, 9, 12%)한 매작과를 제조하여 매작과의 항산화 활성 을 입증하고 품질특성을 측정하였다. 솔잎 분말의 총 페놀화 합물 함량은 9.93±0.2 ㎎ GAE/g이며, 이를 매작과에 첨가한 경우 시료의 첨가량에 비례하여 증가하였다. 제조된 매작과 의 DPPH 라디칼 소거능을 측정한 결과, 솔잎 분말의 첨가량 에 따라 항산화 활성도 유의적으로 증가하는 결과를 나타내 었다. 솔잎 분말 첨가 매작과의 품질평가를 실시한 결과, 반죽의 밀도는 솔잎 분말 첨가량이 증가할수록 높게 나타났고, pH는 감소하였다. 매작과의 부피는 매작과의 첨가량에 따라 감소하는 경향이었으며, 매작과의 색도는 솔잎 분말의 첨가 량이 증가할수록 L값과 b값이 낮아지고, a값이 높아졌으며, 수분 함량과 경도는 증가하는 경향을 나타내었다. 매작과의 기호도 검사(전반적인 기호도, 향, 맛, 바삭함, 색)에서는 6% 솔잎 매작과의 기호도가 가장 높게 나타났다. 또한 저장기간 에 따른 매작과의 산가와 과산화물가를 살펴본 결과, 솔잎 분 말 첨가량이 증가할수록 산패가 지연되는 경향을 나타냈다. 이러한 결과로 보아 매작과에 솔잎 분말을 첨가하는 것은 매 작과의 기호도를 증가시키고 총 페놀 함량과 DPPH 라디칼 소거능을 높여 매작과의 가치를 높이는 것으로 사료되며, 솔 잎 분말을 첨가하여 매작과를 제조할 경우, 6% 로 솔잎 분말 을 첨가할 경우 매작과의 관능적인 품질을 증진시킬 수 있는 가장 최적 조건으로 생각되며, 상품 개발 가능성이 가장 높은 것으로 사료된다.

Dependence of the freeze-drying process condition on microstructure of porous W and pore formation mechanism were studied. Camphene slurries with contents of 10 vol% were prepared by milling at with a small amount of dispersant. Freezing of a slurry was done in Teflon cylinder attached to a copper bottom plate cooled at . Pores were generated subsequently by sublimation of the camphene during drying in air for 48 h. The green body was hydrogen-reduced at for 30 min, and sintered in the furnace at for 1 h. After heat treatment in hydrogen atmosphere, powders were completely converted to metallic W without any reaction phases. The sintered samples showed large pores with the size of about which were aligned parallel to the camphene growth direction. Also, the internal wall of large pores and near bottom part of specimen had relatively small pores with dendritic structure due to the growth of camphene dendrite depending on the degree of nucleation and powder rearrangement in the slurry.

Niobium powder was made from potassium heptafluoroniobite () as the raw material using sodium (Na) as a reducing agent based on the hunter process. The apparatus for the experiment was designed and built specifically for the present study. The niobium particle size greatly increased as the reduction temperature increased from to . The particle size was fairly uniform, varying from to depending on the reduction temperatures. The niobium powder morphology and particle size are very sensitive to a reaction temperature in the metallothermic reduction process. The yield of niobium powder increased from 55% to 80% with a increasing a reaction temperature.

The amorphous (at%) alloy strip was pulverized using a jet mill and an attrition mill to get flake-shaped powder. The flake powder was mixed with dielectric powder and its dispersant to increase the permittivity. The powders covered with dielectric powders and its dispersant were mixed with a binder and a solvent and then tape-cast to form sheets. The absorbing properties of the sheets were measured to investigate the roles of the dielectric powder and its dispersant. The results showed that the addition of powders and its dispersant improved the absorbing properties of the sheets noticeably. The powder sheet mixed with 5 wt% of powder and 1 wt% of dispersant showed the best electromagnetic wave absorption rate because of the increase of the permittivity and the electrical resistance

Pure tantalum powder has been produced by combining Na as a reducing agent, as feed material, KCl and KF as a diluent in a stainless steel(SUS) bomb, using the method of metallothermic reduction. The present study investigated the effect of the amount of the diluent and reaction temperature on the characteristics of tantalum powder in the production process. The temperature applied in this study and the amount of the additional reductant from +5% of the theoretical amount used for the reduction of the entire . The results showed that as the amount of the diluent increased, the reaction temperature became lower because the diluent prevented a temperature rise. Also, according to the mixture ratio of the feed materials and the diluent changed from 1 : 0.25 to 1 : 2, the particle size decreased from to and a particle size distribution which is below 325 mesh in fined powder increases from 71% to 83%. The average size of Tantalum powder, , was close to that of the commercial powders(). Also under this condition, impurities contained in the powder were within the range allowed for the commercial Ta powders.

본 연구에서는 용사용WC-17%Co 복합분말을 분무건조법으로 제조하고 열처리 온도(850˚C, 1000˚C, 1150˚C, 1300˚C)에 따른 조립분말의 미세구조, 입도분포, 유동도, 및 결정상변화를 고찰하였다. 분무건조상태의 입형은 구형이었으며, 입도분포, 평균입자크기, 유동성은 각각 20.6-51.7μm, 27.2μm, 0.26 sec/g 이었다. 열처리에 의하여 조립분말은 치밀화되어 1300˚C 열처리 후에는 입도분포와 평균입자크기가 각 각 6.9-37.9μm과 17.8μm로 감소하였으며, 유동성은 0.12 sec/g로 향상되었다. 열처리중에 WC와 Co의 상화확산에 의하여 Co6W6C및 Co3W3C이 생성되었으며, 두 상이 나타나는 임계온도는 1150˚C이었다.

In this study the calcined condition and characteristic of Cu-Ni-Zn ferrite powder were investigated. The Cu-Ni-Zn ferrite powder has been synthesized by the thermal decomposition of the organic acid salt. This process did not require a strict pH control and provided the uniform composition and fine powder with about 0.3 . The XRD diffraction pattern of this powder showed about 50% spinel phase. The optimum calcination was found to be done at for one hour. After the calcination, the amount of spinel increased to 90%. The distribution of the particle size showed bimodal peaks, one was about 0.5 and the other was about 20 . The large particles of 20 were the agglomeration of fine Particles. The mean Particle size of the powder was about 0.4 . The powder was compacted under 100 MPa pressure and sintered at 1100~ for one hour in air. The density of ferrites specimen was a function of the sintering temperature. The higher the temperature, the denser the ferrite. The maximum relative density of the sintered ferrite was about 93% at . The grain size of sintered specimen at was 5 and homogeneous.

폐-광석으로부터 금속구리분말을 회수하기 위하여 더미 미생물용출, Fe 제거와 전기분해실험을 수행하였다. Cu가 0.034% 함유된 폐-광석시료에 대하여 더미 용출실험을 수행한 결과, Cu 용출률은 박테리아 용출-용액에서 61%, 황산 용출-용액에서 62%로 나타났다. Fe를 효과적으로 제거하기 위하여 더미 용출-용액에 NaOH, H2O2 및 Ca(OH)2를 각각 적용한 결과 H2O2가 가장 효과적인 Fe 제거제로 선정되었다. 전해질 용액을 준비하기 위하여 H2O2를 더미 용출-용액에 처리한 결과 박테리아 용출-용액에서 Fe가 99%, 황산 용출-용액에서 60%로 제거된 반면에 Cu 제거율은 각각 5%와 7%로 나타났다. 이 용액에 대하여 전기분해 실험을 수행한 결과 Cu 회수율이 박테리아 용출-용액에서 98%, 황산 용출-용액에서 76%로 나타났다. 모수석 형태의 금속구리분말이 양쪽 용출-용액에서 회수되었다.

Waste stone sludge generated during the collection of crushed aggregate is difficult to use due to high moisture content. Production of 1 ton aggregate generates approximately 0.25 tons of waste stone sludge. Considering the total crushed aggregate collection in 2012 of about 100 million tons, it can be estimated that 25 million tons of waste stone sludge is generated annually. Recycling of waste stone sludge is made difficult by the high moisture content of 30%. Therefore, to make recycling this process must be a drying process, which makes a fine powder of even better quality that can use as an additive. The purpose of this study is to analyze the changes in physical properties caused by the use of dried waste stone sludge as an additive in the extrusion of cement. A test specimen was made, substituting 50% of the silica with waste stone sludge, and physical performance evaluation was performed. Results showed that 50% substitution of silica resulted in no difference in moldability, but a slight increase in the water content required for the same workability was found. Flexural strength and drying shrinkage were found to be 97% of normal levels, but satisfied the specified performance in the KS F 4735 standard.

파우더 파운데이션은 사용이 간편하고 수정화장이 용이하여 고객들이 많이 사용하고 있으며, 파우더 파운데이션을 만드는 방법은 건식방식, 소성방식, 그리고 습식방법으로 크게 분류할 수가 있다. 이중 습식방법은 이미 잘 알려진 바와 같이 back injection 방법과 front injection 방법이 있으며, 본 논문에서는 front injection 방법을 사용해 실험을 진행하였다. 실험결과 용매의 종류에 따른 경도 변화를 살펴보면 휘발성 실리콘이나 탄화수소계 휘발성 물질을 이용할 때 보다 정제수를 이용할 때 경도가 높게 나타났으며, 사용감 측면에서는 물보다는 탄화수소계 휘발성 물질과 휘발성 실리콘 등을 사용했을 때, 고객 선호도가 높게 나타났다. 또한 코팅물질 변화에 따른 경도 변화로는 아미노산계 코팅물질을 사용하였을 대 경도가 상승하는 효과를 나타냈으며, 실리콘 코팅 물질을 사용했을 때 경도 상승효과가 미비한 것으로 나타났다. 이러한 결과를 토대로 각 대상 고객에 맞는 처방을 개발하고자 할 때 사용감과 경도의 상관관계를 알고, 처방설계에 이용한다면 고객이 원하는 사용감에 한발 더 접근할 수 있으리라 생각된다.

Drink and tea-bag were processed with safflower seed powder. Drinks were processed with 90C hot water extraction. Yield, soluble solid, pH and centrifugation residue of drinks were ranged in 79.2~89.3%, 0.6~0.99%, 5.98~6.40 and 1.00~1.18, respectively. Sensory score of overall acceptance in drinks were highest at that of enzyme treated drink. Tea-bag was processed with roasted safflower seed powder, alone(1.2g) and the mixtured tea-bags were consisted of persimmon leaves, pine needle and angelica gigas powder in same amount, respectively. Teas were prepared with extraction at 80C water for 2 min. Soluble solid and sensory evaluation score of teas were the highest when the tea was processed with safflower seed alone.