In this investigation, Bi2MoO6 deposited graphene nanocomposite (BMG) was synthesized using a simple microwave assisted hydrothermal synthesis method. The synthesized BMG nanocomposite was characterized by X-ray diffraction, transmission electron microscopy, scanning electron microscopy with energy dispersive X-ray analysis, and photocurrent analysis. The study revealed that the catalysts prepared have high crystalline nature, enhanced light responsive property, high catalytic activity, and good stability. XRD results of BMG composite exhibit a koechlinite phase of Bi2MoO6. The surface property is shown by SEM and TEM, which confirmed a homogenous composition in the bulk particles of Bi2MoO6 and nanosheets of graphene. The catalytic behavior was investigated by the decomposition of Rhodamine B as a standard dye. The results exhibit excellent yields of product derivatives at mild conditions under ultrasonic/visible light-medium. Approximately 1.6-times-enhanced sono-photocatalytic activity was observed by introduction of Bi2MoO6 on graphene nanosheet compared with control sample P25 during 50 min test.

Biomass of agricultural waste is getting increasing attention all over the world as it is a kind of renewable, abundantly available, low cost, and environmentally friendly resource. Preparation of activated carbon from agricultural waste via microwave-assisted chemical agent activation. The porosity, surface area, and functional and surface chemistry were featured by means of low-temperature nitrogen adsorption, Scanning Electron Microscopy, (SEM) and Fourier Transform Infrared Spectroscopy (FTIR). The best conditions resulted in activated carbon with adsorption capacity of 517.5 mg/g and carbon yield of 80.99%. The activated carbons from carbonized tobacco stem with K2CO3 activation by microwave radiation is highest of surface area, and total pore volume corresponded to 2557 m2/g, and 1.647 cm3/g, respectively, with a high contribution of mesopores, microwave power of 700 W, and irradiation time of 30 min. The results of the review showed that chemical activation could develop both microporosity and mesoporosity. The findings support the potential to prepare high surface area and micropore-activated carbon from agricultural waste by microwave-induced chemical activation.

This research aims to study the simultaneous extraction and transesterification of Chlorella vulgaris (C. vulgaris) using microwave irradiation with methanol as solvent and potassium hydroxide (KOH) as catalyst. The microwave-assisted insitu transesterification of C. vulgaris is assessed at various ratios of biomass-to-methanol, reaction times, and catalyst concentrations during the centrifugation and evaporation process. Gas chromatography-mass spectrometry (GC-MS) analysis is performed to confirm fatty acid methyl ester (FAME) composition. Biodiesel preparation is carried out by simultaneous extraction and transesterification of microalgae from C. vulgaris. The product is then characterized using Fourier transform infrared spectroscopy (FTIR) and proton nuclear magnetic resonance (1H-NMR); microalgae are observed using scanning electron microscopy (SEM). The highest amount of FAME is obtained at a biomass-to-methanol ratio of 1:12, reaction time of 40 min, and catalyst concentration of 2 wt%. Biodiesel shows conversion to about 77.64% of methyl ester (methyl myristate, methyl palmitoleate, methyl linoleate, methyl oleate, methyl arachidonate, and methyl 5,8,11,14,17-eicosapentanoate).

A facile microwave assisted solvothermal process is designed for fabricating SnS nanoparticles decorated on graphene nanosheet, which used as visible light driven photocatalyst. Some typical characterization techniques such as XRD, FT-IR, SEM with EDX analysis, and TEM and BET analysis are used to analyse the physical characteristics of as-prepared samples. Spherical SnS nanoparticles are uniformly dispersed on the surface of graphene nanosheet due to ammonia, which can prevent the aggregation of graphene oxide. Meanwhile, microwave radiation provides fast energy that promotes the formation of spherical SnS nanoparticles within a short time. The visible light photocatalytic activity of as-prepared SnS-GR nanocomposites is analysed through photodegradation efficiency of methylene blue with high concentration. According to the higher photocatalytic property, the as-prepared SnS-GR nanocomposites can be expected to be an efficient visible light driven photocatalyst. After five cycles for decolorization, the rate decreases from 87 % to 78 % (about 9 %). It is obvious that the photocatalytic activity of SnS-GR nanocomposite has good repeatability.

Oxide semiconductor, represented by a-IGZO, has been commercialized in the market as active layer of TFTs of display backplanes due to its various advantages over a-Si. a-IGZO can be deposited at room temperature by RF magnetron sputtering process; however, additional thermal annealing above 300oC is required to obtain good semiconducting properties and stability. These temperature are too high for common flexible substrates like PET, PEN, and PI. In this work, effects of microwave annealing time on IGZO thin film and associated thin-film transistors are demonstrated. As the microwave annealing time increases, the electrical properties of a-IGZO TFT improve to a degree similar to that during thermal annealing. Optimal microwave annealed IGZO TFT exhibits mobility, SS, Vth, and VH of 6.45 cm2/Vs, 0.17 V/dec, 1.53 V, and 0.47 V, respectively. PBS and NBS stability tests confirm that microwave annealing can effectively improve the interface between the dielectric and the active layer.

The purpose of this study was to derive the conditions for manufacturing rice porridge with optimum properties after reheating. The characteristics of rice porridge according to the soaking time, water addition rate, heating temperature, heating time, and cooling conditions were compared using the ‘Samkwang’ cultivar. In Step Ⅰ, as the heating temperature increased, the weight change decreased and the viscosity increased, and the temperature known as the main factor of the gelatinization also appeared to affect the viscosity increase. In Step Ⅱ, the viscosity and the texture properties was not significantly different as the soaking time was reduced, and 10 minutes was suitable because of due to the shortening effect of the total process time. In Step Ⅲ, the residual heat was lowered by cooling after the rice porridge production, so the viscosity could be greatly reduced. Also, it was confirmed that the water addition rate of 900% and the heating temperature of 15 minutes were optimal manufacturing conditions. The next study will investigate the porridge processability of rice cultivars using these results.

The composite PAN fibers which incorporated with CNTs and Titania were prepared by mean of wet spinning. These fibers were then pre-oxidized with microwave heating in an air atmosphere. A combination of characterizations was carried out to study the impact of nanoparticles fillers on the properties of as-spun fibers and their performance during the microwave pre-oxidation. The addition of an equal amount of fillers made obvious changes in the chemical and crystalline structure, consequently improves the strength, and this could lower the capability to creep over a wide range of temperatures in the subsequent processes. FTIR and NMR analyses results of the pre-oxidized fibers exhibited clear changes in the PAN structure, where the dehydrogenation reaction and the degree of cyclization were investigated. Additional confirmation of the occurrence of cyclization reaction was achieved by XRD and thermal analysis. According to the TGA results, the pre-oxidized CNT1/ Ti-PAN fibers exhibit greater thermal stability suggesting high carbon content and good quality could result in the dependent carbon fibers.

The study presented in the article is focused on use of graphene obtained by novel microwave-enhanced chemical vapor deposition (MECVD) method as a construction material for 3D porous structures—aerogels and sponges. MECVD graphene nanoplatelets-based aerogels were obtained by mixing MECVD graphene nanoplatelets and chitosan, dissolved in 3% acetic acid followed by its freeze drying and carbonization at 800° in inert medium. Surface morphology of aerogels was characterized by SEM. MECVD graphene nanoplatelets-based aerogels are characterized by a porous structure; they are superhydrophobic and possess high sorption capacity with regard to organic liquids of different densities. Polyurethane sponges coated with MECVD graphene can serve as an alternative to aerogels. The process of their obtaining is cheaper and less complicated. They were obtained by facile “dip-coating” method, modifying its surface to increase its hydrophobicity. The resulting sponges are superhydrophobic and superoleophilic, and demonstrate high rate of sorption of organic liquids and can be easily regenerated by squeezing. In addition, they can be used as a separating material in conjunction with vacuum system for continuous and selective collection of organic liquids from the surface of water.

Graphene and Fe3O4 were bound by electrostatic attraction and prepared by effective reduction through microwave treatments. As a result of fabricating graphene with Fe3O4 as a composite material, it has been confirmed that it contributes to the structural improvement in graphene stabilization and at the same time, it shows improved electrochemical performance through improved charge transfer. It was also confirmed that the crystalline Fe3O4 was uniformly dispersed in the rGO sheet, effectively blocking the reaggregation due to the van der Waals interaction between the neighboring rGO sheets. The structural analysis of prepared composites was confirmed by transmission electron microscopy, and X-ray diffractometer. Electrochemical properties of composites were studied by cyclic voltammetry, galvanostatic charge–discharge curves, and electrochemical impedance spectroscopy. The Fe3O4 (0.4 M)/rGO composite showed a high specific capacitance of 972 F g−1 at the current density of 1 A g−1 in 6 M KOH electrolyte, which is higher than that of the pristine materials rGO (251 F g−1) and Fe3O4 (183 F g−1). Also, the prepared composites showed a very stable cyclic behavior at high current density, as well as an improvement in comparison with pristine materials in terms of resistance.

Phosphorus is a vital resource for sustaining agriculture and nutrition, but a limited non-renewable resource. Thus, the recovery of phosphorus from waste activated sludge(WAS) was attempted by microwave heating and magnesium ammonium phosphorus(MAP) crystallization. Polyphosphate-accumulating organisms(PAOs) in WAS release phosphate from the cell when they are exposed to high temperature environments. Microwave heating caused phosphorus and ammonia to release from WAS. The amount was increased with increasing temperature, showing that 88.5% of polyphosphate present in the cells were released in the form of phosphate at 80oC. A similar result was also observed in the release of ammonia. On the other hand, both phosphorus and ammonia were crystallized with magnesium, and then was harvested as MAP. Phosphorus recovery rate reached almost 97.8%, but the ammonia was about 13.4%. These results cleary indicate that phosphorus could be recovered from WAS using a physiological trait of PAOs. Heavy metal analyses also show that the MAP crystal is useful and safe as a phosphorus fertilizer.

본 연구에서는 서해 연안에서의 실측-위성 해수면온도 차이를 규명하고 그 특성을 분석하기 위해 GCOM-W1/ AMSR2 마이크로파 해수면온도 자료와 서해 연안에 위치한 덕적도, 칠발도, 외연도 해양기상 부이의 실측 수온 자료를 활용하여 2012년 7월부터 2017년 12월까지 총 6,457개의 일치점 자료를 생산하였다. 5년 이상의 덕적도, 칠발도, 외연도 해양 부이 수온 자료와 AMSR2 해수면온도를 비교하여 정확도를 제시하였다. 마이크로파 위성 해수면온도와 현장 관측 부이 해수면온도 간의 차이는 풍속과 수온 등 환경 요인에 대한 의존성을 가지는 것으로 나타났다. 낮시간 풍속이 약할 때 (<6 ms−1 ) AMSR2 해수면온도는 실측 해수면온도보다 높게 산출되며, 밤시간에 대해서는 풍속이 커질수록 양의 편차가 증가함을 밝혔다. 또한 AMSR2 해수면온도와 실측 해양부이 수온 간의 차이가 증가하는 경향은 낮은 온도에서 마이크로파 센서의 민감도의 저하와 육지에 의한 자료오염과 관련이 있는 것으로 나타났다. 실측-위성 해수면온도 차이를 월별로 도시해본 결과, 마이크로파 위성 해수면온도의 편차는 강한 바람이 부는 겨울철에 가장 커진다고 알려져 있던 기존의 경향성과는 달리 덕적도, 칠발도 부이에서는 여름철 가장 큰 해수면온도 편차값이 나타났다. 이러한 차이는 부이의 위치에 따른 조석 혼합의 공간적 차등에 기인한 것으로 사료된다. 본 연구는 인공위성 합성장에 기여도가 높은 마이크로파 위성 해수면온도를 사용할 때 한반도 서해안에서 발생할 수 있는 문제점과 제한점을 제시하였다.