본 연구는 혈압 강하, 비타민 B1의 활성화, 항암 효과, 노화방지 등에 탁월한 효과가 있다고 알려진 마늘의 활용도를 더욱 높이기 위하여 중력분에 수준별(1%, 3%, 5%) 마늘 분말을 첨가하여 물성 변화 및 마늘가루 첨가가 제면 적성에 미치는 영향을 실험하였다. 마늘 분말 첨가량을 달리하였을 때 호화도 변화를 측정한 결과, 마늘 분말 양이 증가하면 호화 개시온도가 높아졌으며, 최고 점도는 낮아졌다. 최고 점도와 최저 점도의 차이를 나타내는 breakdown 값도 낮아졌다. 또한 최종 점도도 약간 낮아지는 경향을 보였으며, 마늘 분말 첨가량이 증가하면 set back값은 감소하는 경향이었지만 노화를 억제할 정도는 아니었다. Farinogram의 consistency는 마늘 분말 첨가량이 많아질수록 높아졌고, 수분흡수율 또한 높아지는 경향을 보였다. 반죽형성시간은 길어졌으며 안정도는 낮아졌으며, 마늘 분말 첨가량이 많아질수록 time to breakdown 값이 급격하게 떨어졌다. Mechanical tolerance index 값이 마늘 분말 첨가 시료들의 경우 낮게 나타나, 마늘 분말을 첨가하면 반죽의 기계적 적성이 떨어진다는 것을 알 수 있었다. Farinogram quality number는 중력분 대조구에 비하여 마늘 분말 첨가구들은 첨가량이 많아질수록 그 수치가 떨어졌다. 그러나 1% 첨가구와 3% 첨가구 사이에서는 서로 간에 유의적인 차이를 보이지 않았다. Alveogram을 이용하여 글루텐 강도를 측정한 Pmax 값은 마늘분말 첨가량이 많아질수록 Pmax 값이 감소되었을 뿐만 아니라, 서로 간에 유의적인 차이를 보이지도 않았다. 팽창된 반죽이 터질 때까지의 신장성을 나타내는 L값은 마늘 분말 첨가량이 증가하면 감소하였다. 그러나 3% 첨가구와 5% 첨가구 사이에서 유의적인 차이는 나타나지 않았다. 팽창지표를 나타내는 G값 역시 마늘 분말 함량이 많아지면 G값은 낮아졌다. 하지만 3% 첨가구와 5% 첨가구 사이에서는 L값과 마찬가지로 유의적인 차이를 보이지 않았다. 변형 에너지 값인 W값도 마늘 분말 첨가량이 증가하면 W값은 감소하였으며, 특히 대조구에 비하여 마늘 분말 1% 첨가구는 급격하게 수치가 낮아졌다. 3% 첨가구와 5% 첨가구 사이에서는 유의적인 차이를 보이지 않았다.

2012년 2월부터 11월까지 인천 지역에서 유통된 건고추 및 고춧가루 193건을 대상으로 아플라톡신 B1과 오크라톡 신 A의 오염도를 조사하였다. Immunoaffinity column 및 HPLC를 이용한 시험법은 모두 80% 이상의 회수율을 보였고, 아플라톡신 B1 및 오크라톡신 A의 검출한계는 각각 0.13 μg/kg, 0.30 μg/kg였다. 오염도 조사를 한 결과 아플라 톡신 B1은 17.1%의 검출율을 보였고 오크라톡신 A는 20.7% 의 검출율을 보였으며, 아플라톡신 B1의 검출농도는 0.14~ 9.67 μg/kg였고, 오크라톡신 A의 검출 농도는 0.31~3.31 μg/ kg였다. 이는 우리나라 식품공전 상의 기준인 10 μg/kg(아 플라톡신 B1), 7 μg/kg(오크라톡신 A)보다는 낮은 수치로 비교적 안전한 수준이었다.

Stress-strain curves are fundamental properties to study characteristics of materials. Flow stress curves of the powder materials are obtained by indirect testing methods, such as tensile test with the bulk materials and powder compaction test, because it is hard to measure the stress-strain curves of the powder materials using conventional uniax- ial tensile test due to the limitation of the size and shape of the specimen. Instrumented nanoindentation can measure mechanical properties of very small region from several nanometers to several micrometers, so nanoindentation tech- nique is suitable to obtain the stress-strain curve of the powder materials. In this study, a novel technique to obtain the stress-strain curves using the combination of instrumented nanoindentation and finite element method was introduced and the flow stress curves of Fe powder were measured. Then obtained stress-strain curves were verified by the com- parison of the experimental results and the FEA results for powder compaction test.

TiB2-reinforced iron matrix composite (Fe-TiB2) powder was in-situ fabricated from titanium hydride (TiH2) and iron boride (FeB) powders by the mechanical activation and a subsequent reaction. Phase formation of the composite powder was identified by X-ray diffraction (XRD). The morphology and phase composition were observed and measured by field emission-scanning electron microscopy (FE-SEM) and energy-dispersive X-ray spectroscopy (EDS), respectively. The results showed that TiB2 particles formed in nanoscale were uniformly distributed in Fe matrix. Fe2B phase existed due to an incomplete reaction of Ti and FeB. Effect of milling process and synthesis temperature on the formation of composite were discussed.

High-coercive (Nd,Dy)-Fe-B magnets were fabricated via dysprosium coating on Nd-Fe-B powder. The sputtering coating process of Nd–Fe–B powder yielded samples with densities greater than 98%. (Nd,Dy)2Fe14B phases may have effectively penetrated into the boundaries between neighboring Nd2Fe14B grains during the sputtering coating process, thereby forming a (Nd,Dy)2Fe14B phase at the grain boundary. The maximum thickness of the Dy shell was approximately 70 nm. The maximum coercivity of the Dy sputter coated samples(sintered samples) increased from 1162.42 to 2020.70 kA/m. The microstructures of the (Nd,Dy)2Fe14B phases were effectively controlled, resulting in mproved magnetic properties. The increase in coercivity of the Nd-Fe-B sintered magnet is discussed from a micro- structural point of view.

Effects of the amount of nickel powder (Ni) in Ni-carbon fiber (CF) hybrid filler systems on the conductivity(or resistivity) and thermal coefficient of resistance (TCR) of filled high density polyethylene were studied. Increases of the resistivity and TCR with increasing Ni concentration at a given hybrid filler content were observed. Using the fiber contact model, we showed that the main role of Ni in the hybrid filler system is to decrease the interfiber contact resistance when Ni concentration is less than the threshold point. The formation of structural defects leading to reduced reinforcing effect resulted in both a reduction of strength and an increase of the coefficient of thermal expansion in the composite film; these changes are responsible for the increases of both resistivity and TCR with increasing Ni concentration in the hybrid filler system.

This study investigated the quality of noodles containing different amounts of Lagocephalus lunaris powder (LLP). Noodles were prepared at ratios of 0, 1, 3, 5 and 7% LLP based on flour weight, after which cooking quality, mechanical texture properties, and viscosity were measured, and a sensory evaluation was performed. The gelatinization points of the composite LLP-wheat flours were shown to increase. Additionally, measurement of the viscosity at 95, viscosity at 95 after 15 minutes, and the maximum viscosity values decreased, as the LLP content increased. As increasing amounts of LLP were added, the L and a values decreased, whereas the b value increased and the color values, weight, and volume of cooked noodle increased, as did the turbidity of the soup. Finally the LLP additive increased hardness and decreased adhesiveness, cohesiveness and springiness. Sensory evaluation showed that high quality cooked noodle could be produced by inclusion of 5% LLP.

GdBa2Cu3O7-y(Gd123) powders were synthesized by the solid-state reaction method using Gd2O3 (99.9% purity), BaCO3 (99.75%) and CuO (99.9%) powders. The synthesized Gd123 powder and the Gd123 powder with Gd2O3 addition (Gd1.5Ba2Cu3O7-y(Gd1.5)) were used as raw powders for the fabrication of Gd123 bulk superconductors. The Gd123 and Gd1.5 bulk superconductors were fabricated by sintering or a top-seeded melt growth (TSMG) process. The superconducting transition temperature (Tc,onset) of the sintered Gd123 was 93 K and the transition width was as large as 20 K. The Tc,onset of the TSMG processed Gd123 was 82 K and the transition width was also as large as 12 K. The critical current density (Jc) at 77 K and 0 T of the sintered Gd123 and TSMG processed Gd123 were as low as a few hundreds A/cm2. The addition of 0.25 mole Gd2O3 and 1 wt.% CeO2 to Gd123 enhanced the Tc, Jc and magnetic flux density (H) of the TSMG processed Gd123 sample owing to the formation of the superconducting phase with high flux pinning capability. The Tc of the TSMG processed Gd1.5 was 92 K and the transition width was 1 K. The Jcs at 77 K (0 T and 2 T) were 3.2×104 A/cm2 and 2.5×104 A/cm2, respectively. The H at 77 K of the TSMG-processed Gd1.5 was 1.96 kG, which is 54% of the applied magnetic field (3.45 kG).

In the present work, 6061 Al-B4C sintered composites containing different B4C contents were fabricated and their characteristic were investigated as a function of sintering temperature. For this, composite powders and their compacts with B4C various contents from 0 to 40 wt.% were fabricated using a planetary ball milling equipment and cold isostatic pressing, respectively, and then they were sintered in the temperature ranges of 580 to 660o C. Above sin- tering temperature of 640o C, real density was decreased due to the occurrence of sweat phenomena. In addition, it was realized that sinterability of 6061Al-B4C composite material was lowered with increasing B4C content, resulting in the decrease in its real density and at the same time in the increment of porosity.

Nano-sized cobalt powder was fabricated by wet chemical reduction method at room temperature. The effects of various experimental variables on the overall properties of fabricated nano-sized cobalt powders have been investigated in detail, and amount of NaOH and reducing agent and dropping speed of reducing agent have been prop- erly selected as experimental variables in the present research. Minitab program which could find optimized conditions was adopted as a statistic analysis. 3D Scatter-Plot and DOE (Design of Experiments) conditions for synthesis of nano- sized cobalt powder were well developed using Box-Behnken DOE method. Based on the results of the DOE process, reproducibility test were performed for nano-sized cobalt powder. Spherical nano-sized cobalt powders with an average size of 70-100 nm were successfully developed and crystalline peaks for the HCP and FCC structure were observed without second phase such as Co(OH).

We investigated the quality characteristics of cookies prepared following the addition of various concentrations of used Hongkuk powder (0%, 1%, 3%, 5%, all w/w) as a substitute for flour. In this study, the moisture content of dough decreased and pH increased by adding Hongkuk powder. The L and b value were decreased significantly, but the a value of cookies increased by addition of Hongkuk powder. The spread factor of cookies was slightly decreased by the addition of Hongkuk powder. The hardness of the control group was higher than that of the cookies prepared with different levels of Hongkuk powder. The result of the sensory score showed that cookies added with 1% Hongkuk powder had higher taste, flavor, and overall acceptability scores than other samples. As a result of this study, the quality of cookies with the addition of 1% Hongkuk powder were the most suitable in terms of its taste, flavor, texture, and sensory properties.

본 연구에서는 약리작용과 기능성이 함유된 국내산 산수유를 설기떡에 활용하여 건강식품으로 보급 발전시키기 위하여 산수유를 설기떡 재료의 최적 배합 비율을 얻고자 하였다. 멥쌀가루에 0, 5, 10, 15, 20%의 동결건조한 산수유 분말을 첨가하여 설기떡을 제조하고 20oC에서 저장하여 시료로 사용하였으며, 수분함량, 색도, 당도, pH, 기계적 품질특성, 관능적 품질특성을 측정한 결과는 다음과 같다. 산수유 분말 첨가량이 증가할수록, 수분 함량이 증가하는 경향을 보였고 색도에서 L값은 감소하였으며, a값과 b값은 증가하는 경향을 나타냈다. 당도는 첨가량이 증가할수록 증가하는 경향을 보였지만 pH 측정값은 낮아졌다. 경도(hardness), 부착성(adhesiveness)은 대조군이 가장 높았고, 첨가량이 증가할수록 낮아지는 경향을 보였다. 응집성(cohesiveness)과 탄력성(springiness)은 산수유 분말 15% 첨가군이 가장 높은 값을 나타냈다. 씹힘성(chewiness)은 대조군과 산수유 첨가량의 유의적 차이는 나타나지 않았지만 산수유 15%일 때 가장 높은 값으로 측정되었다. 관능평가의 전체적인 기호도(overall-acceptability)는 산수유 첨가군 15% > 10% > 20% > 5% > 0% 순으로 나타났다. 따라서, 동결건조한 산수유 분말 첨가량이 15% 수준에서 설기떡에 첨가하여 제조하는 것이 적정한 수준으로 여겨진다.

(Y123) powders for the fabrication of bulk superconductors were synthesized by the powder reaction method using (99.9% purity), (99.75%) and CuO (99.9%) powders. The raw powders were weighed to the cation ratio of Y:Ba:Cu=1:2:3, mixed and calcined at in air with intermediate repeated crushing steps. It was found that the formation of Y123 powder was more sensitive to reaction temperature than reaction time. The calcined Y123 powder and a mixture of (Y123 + 0.25 mole + 1 wt.% , (Y1.5)) were used as raw powders for the fabrication of poly-grain or single grain superconductors. The superconducting transition temperature () of the sintered Y123 sample was 91 K and the transition width was as large as 11 K, whereas the of the melt-grown Y1.5 sample was 90.5 K and the transition width was 3.5 K. The critical current density () at 77 K and 0 T of the sintered Y123 was 700 , whereas the of the top-seeded melt growth (TSMG) processed Y1.5 sample was . The magnetic flux density (H) at 77 K of the TSMG-processed Y123 and Y1.5 sample showed the 0.53 kG and 2.45 kG, respectively, which are 15% and 71% of the applied magnetic field of 3.5 kG. The high H value of the TSMG-processed Y1.5 sample is attributed to the formation of the larger superconducting grain with fine Y211 dispersion.

Ultra-fine zirconium carbide (ZrC) powder with nano-sized primary particles was synthesized by the carbothermal reduction method by using nano-sized and nano-sized graphite powders mixture. The synthesized ZrC powder was well dispersed after simple milling process. After heat-treatment at for 2 h under vacuum, ultra-fine ZrC powder agglomerates (average size, ) were facilely obtained with rounded particle shape and particle size of ~200 nm. Ultra-fine ZrC powder with an average particle size of 316 nm was obtained after ball milling process in a planetary mill for 30 minutes from the agglomerated ZrC powder.

This study investigated the functional nutrition of red yeast rice to added beurre mani? in the production of brown sauce. We added X to Y at levels of 0%, 5%, 10%, 15% and 20% and investigated the effects on the viscosity, water content, turbidity, pH, sugar level, reducing sugar, color, and sensory quality characteristics of the resultant brown sauce. The viscosity of Brown sauce was increased with increasing red yeast rice beurre mani? while water content and turbidity were decreased. pH was between 4.57～4.91. Sugar level and reducing sugar were increased with increasing red yeast rice powder content. L and a were increased with increasing red yeast rice powder content, and b was decreased. In sensory testing, visual appearance and flavor were highest for brown sauce preparations containing 15% and 20% X. Aftertaste and taste scored the highest for additions of 10% and 15%. For general preference, a 15% addition of X resulted in the highest score. Based on the results, it seems that red yeast rice powder, 15% red yeast rice powder added brown sauce has the highest the general preference.

알루미늄 테르밋 반응의 환원제로서 알루미늄 분말은 200 메쉬 이하의 미분이 필요하나, 알루미늄의 높은 인성과 분말 제조비 때문에 경제적으로 용이하지 않다. 그러므로 Mn3O4 분진 환원용 알루미늄 미분의 제조 코스트를 낮추기 위해, 알루미늄 합금분말의 제특성이 검토되었다. 망간을 다량 함유한 알루미늄 합금괴는 취성이 큰 금속간 화합물을 함유하고 있기 때문에 쉽게 파쇄할 수 있다. 또 망간은 망간 합금철의 주성분이다. Al-15%Mn 합금분말을 기계적 파쇄법으로 저렴하게 제조할 수 있다. Al 분말 대신에 Al-15%Mn 합금분말을 사용한 테르밋 반응 결과는 환원제로 순 알루미늄 분말을 사용한 경우와 같이 고순도 망간 합금철을 얻을 수 있었다. Al-15%Mn 합금분말를 이용한 Mn3O4 분진의 망간 회수율은 알루미늄 분말을 이용한 경우의 약 65% 보다 높은 약 70%의 높은 수준을 보였으며, 이는 비산이 적은 것에 기인한다.