YSZ (Y2O3-stabilized zirconia)-based ceramics have excellent mechanical properties, such as high strength and wear resistance. In the application, YSZ is utilized in the bead mill, a fine-grinding process. YSZ-based parts, such as the rotor and pin, can be easily damaged by continuous application with high rpm in the bead mill process. In that case, adding WC particles improves the tribological and mechanical properties. YSZ-30 vol.% WC composite ceramics are manufactured via hot pressing under different pressures (10/30/60 MPa). The hot-pressed composite ceramics measure the physical properties, such as porosity and bulk density values. In addition, the phase formation of these composite ceramics is analyzed and discussed with those of physical properties. For the increased applied pressure of hot pressing, the tetragonality of YSZ and the crystallinity of WC are enhanced. The mechanical properties indicate an improved tendency with the increase in the applied pressure of hot pressing.
This study focused on improving the phase stability and mechanical properties of yttria-stabilized zirconia (YSZ), commonly utilized in gas turbine engine thermal barrier coatings, by incorporating Gd2O3, Er2O3, and TiO2. The addition of 3-valent rare earth elements to YSZ can reduce thermal conductivity and enhance phase stability while adding the 4-valent element TiO2 can improve phase stability and mechanical properties. Sintered specimens were prepared with hot-press equipment. Phase analysis was conducted with X-ray diffraction (XRD), and mechanical properties were assessed with Vickers hardness equipment. The research results revealed that, except for Z10YGE10T, most compositions predominantly exhibited the t-phase. Increasing the content of 3-valent rare earth oxides resulted in a decrease in the monoclinic phase and an increase in the tetragonal phase. In addition, the t(400) angle decreased while the t(004) angle increased. The addition of 10 mol% of 3-valent rare-earth oxides discarded the t-phase and led to the complete development of the c-phase. Adding 10 mol% TiO2 increased hardness than YSZ.
According to the classification of World Health Organization, primary adenocarcinomas of the sinonasal tract can be initially classified as salivary and non-salivary types. The latter are further divided into intestinal and non-intestinal types. Sinonasal intestinal-type adenocarcinoma(ITAC) is rare adenocarcinoma subtype, which is closely occupational exposure to hardwood dusts, leather. In this study, we present a case of ITAC in a 68-year-old man. We successfully treated with wide excision and soft tissue reconstruction with free anterolateral thigh flap.
Thermal protection systems (TPS) are a group of materials that are indispensable for protecting spacecraft from the aerodynamic heating occurring during entry into an atmosphere. Among candidate materials for TPS, ceramic insulation materials are usually considered for reusable TPS. In this study, ceramic insulation materials, such as alumina enhanced thermal barrier (AETB), are fabricated via typical ceramic processing from ceramic fiber and additives. Mixtures of silica and alumina fibers are used as raw materials, with the addition of B4C to bind fibers together. Reaction-cured glass is also added on top of AETB to induce water-proof functionality or high emissivity. Some issues, such as the elimination of clumps in the AETB, and processing difficulties in the production of reusable surface insulation are reported as well.
3Y-TZP ceramics obtained by doping 3 mol.% of Y2O3 to ZrO2 to stabilize the phase transition are widely used in the engineering ceramic industry due to their excellent mechanical properties such as high strength, fracture toughness, and wear resistance. An additional increase in mechanical properties is possible by manufacturing a composite in which a high-hardness material such as oxide or carbide is added to the 3Y-TZP matrix. In this study, composite powder was prepared by dispersing a designated percentage of WC in the 3Y-TZP matrix, and the results were compared after manufacturing the composite using the different processes of spark plasma sintering and HP. The difference between the densification behavior and porosity with the process mechanism was investigated. The correlation between the process conditions and phase formation was examined based on the crystalline phase formation behavior. Changes to the microstructure according to the process conditions were compared using field-emission scanning electron microscopy. The toughness-strengthening mechanism of the composite with densification and phase formation was also investigated.
EBV-positive mucocutaneous ulcer (EBVMCU) is an indolent, superficial lymphoproliferative disorder that occurs in either iatrogenic or age-associated immunocompromised patients with latent Epstein-Barr virus (EBV) infection. Although EBVMCU is histologically similar with other lymphoproliferative disorders, such as EBV-positive diffuse large B cell lymphoma, the diseases are classified as distinct entities by the World Health Organization with different clinical manifestations, prognosis, and genetic profiles. EBVMCU commonly shows spontaneous regression by conservative management, reduction or cessation of immunosuppressive treatment, but local progression is possible. Complete remission of disease can be achieved with combination of surgical resection, chemotherapy and local radiation therapy. Herein, we report 2 cases of oral superficial lymphoproliferative disorders arising adjacent to the gnathic bone with striking differences in prognosis and bone involvement. One of the cases induced extensive osteomyelitis in the underlying bone. Furthermore, we discussed the differential diagnosis of EBVMCU and reviewed the former literature.
Plunging ranula is a mucous retention cyst with extension below to the mylohyoid muscle. It can occur by an extravasation of saliva from the salivary gland due to trauma or obstruction of the duct. Fluid from the obstructed gland penetrate through the defect of mylohyoid muscle or through the posterior edge of mylohyoid muscle, and spreading to the cervical area. The “tail sign” has been widely reported as pathognomonic for their diagnosis. It indicates the communication between the collapsed sublingual and submandibular space over the posterior edge of the mylohyoid muscle. In this case, in addition to simple ranula in the right floor of mouth, MRI findings showed homogeneous contrast enhancement in front of the right cervical carotid artery and in the deep part of sternocleidomastoid muscle, but tail sign was not observed. Therefore it was clinically diagnosed as a branchial cleft cyst and was removed through surgical procedure. As a result of the final pathologic biopsy, the lesion, which has been suggested to be simple ranula in the floor of mouth, was diagnosed as reactive pyogenic granuloma, and the cervical lesion was diagnosed as a plunging ranula. This is a case report in which these two lesions are decided to have been separated from one before surgery. This report indicate that plunging ranula can be observed without tail sign and how to make an accurate diagnosis of plunging ranula by reporting misdiagnosis case.
SiC is a material with excellent strength, heat resistance, and corrosion resistance. It is generally used as a material for SiC invertors, semiconductor susceptors, edge rings, MOCVD susceptors, and mechanical bearings. Recently, SiC single crystals for LED are expected to be a new market application. In addition, SiC is also used as a heating element applied directly to electrical energy. Research in this study has focused on the manufacture of heating elements that can raise the temperature in a short time by irradiating SiC-I2 with microwaves with polarization difference, instead of applying electric energy directly to increase the convenience and efficiency. In this experiment, Polydimethylsilane (PDMS) with 1,2 wt% of iodine is synthesized under high temperature and pressure using an autoclave. The synthesized Polycarbosilane (PCS) is heat treated in an argon gas atmosphere after curing process. The experimental results obtain resonance peaks using FT-IR and UV-Visible, and the crystal structure is measured by XRD. Also, the heat-generating characteristics are determined in the frequency band of 2.45 GHz after heat treatment in an air atmosphere furnace.
본 논문은 CFRP 쉬트로 휨 보강된 철근콘크리트 보에서 보강재의 탈락이 구조물에 미치는 영향을 파악하기 위한 실험적 그리고 해석적 연구결과를 보고한다. 실험적 연구로 CFRP 시트의 비부착 수준 및 위치를 실험변수로 고려한 실험체들에 대한 휨파괴 실험이 수행되었다. 중앙부에 비부착구간을 갖는 실험체의 경우 비부착구간의 증가에도 불구하고 최대하중 및 강성의 변화는 크게 감소하지 않았다. 단부에 비부착 구간을 갖는 실험체의 경우 비부착 구간이 증가할수록 최대하중 및 강성이 크게 감소하였다. 이것은 보강재의 작은 보강길이로 인한 정착력의 부족으로 인해 철근의 항복 이후 보강재가 조기 박리되었기 때문으로 판단된다. 본 연구의 결과와 기존 제안된 부착강도 모델을 이용한 예측 결과의 비교를 통해 기존 부착강도 모델들은 단부 비부착 실험체들보다 중앙 비부착 실험체들의 내하력을 더 정확하게 예측하는 것으로 나타났다.
As automation systems become more common, there is growing interest in functional labeling systems using organic and inorganic hybrid materials. Especially, the demand for thermally and chemically stable labeling paper that can be used in a high temperature environment above 300 oC and a strong acid and base atmosphere is increasing. In this study, a composite coating solution for the development of labeling paper with excellent thermal and chemical stability is prepared by mixing a silica inorganic binder and titanium dioxide. The silica inorganic binder is synthesized using a sol-gel process and mixed with titanium dioxide to improve whiteness at high-temperature. Adhesion between the polyimide substrate and the coating layer is secured and the surface properties of the coating layer, including the thermal and chemical stability, are investigated in detail. The effects of the coating solution dispersion on the surface properties of the coating layer are also analyzed. Finally, it is confirmed that the developed functional labeling paper showed excellent printability.
SiAlON ceramics are used as ceramic cutting tools for heat-resistant super alloys (HRSAs) due to their excellent fracture toughness and thermal properties. They are manufactured from nitride and oxide raw materials. Mixtures of nitrides and oxides are densified via liquid phase sintering by using gas pressure sintering. Rare earth oxides, when used as sintering additives, affect the color and mechanical properties of SiAlON. Moreover, these sintering additives influence the cutting performance. In this study, we have prepared Ybm/3Si12-(m+n)Alm+nOnN16-n (m = 0.5; n = 0.5, 1.0) ceramics and manufactured SiAlON ceramics, which resulted in different colors. In addition, the characteristics of the sintered SiAlON ceramics such as fracture toughness and microstructure have been investigated and results of the cutting test have been analyzed.
Piezoelectric ceramic specimens with the Pb(Mg1/3Nb2/3)0.65Ti0.35O3 (PMN-PT) composition are prepared by the solid state reaction method known as the “columbite precursor” method. Moreover, the effects of the Li2O-Bi2O3 additive on the microstructure, crystal structure, and piezoelectric properties of sintered PMN-PT ceramic samples are investigated. The addition of Li2O-Bi2O3 lowers the sintering temperature from 1,200oC to 950oC. Moreover, with the addition of >5 wt.% additive, the crystal structure changes from tetragonal to rhombohedral. Notably, the sample with 3 wt.% additive exhibits excellent piezoelectric properties (d33 = 596 pC/N and Kp = 57%) and a sintered density of 7.92 g/cm3 after sintering at 950oC. In addition, the sample exhibits a curie temperature of 138.6oC at 1 kHz. Finally, the compatibility of the sample with a Cu electrode is examined, because the energy-dispersive X-ray spectroscopy data indicate the absence of interdiffusion between Cu and the ceramic material.
남부지역에서 고구마 바이러스 무병묘의 정식시기 및 재배 기간에 따른 괴근 수량 및 씨고구마 생산량을 조사한 결과는 다음과 같다. 1. 바이러스 무병묘 정식시기에 따라 씨고구마로 사용하기에 알맞은 100~300 g 크기의 괴근 생산량은 6월 중순 정식 재배에서 ‘신율미’ 2,364 kg/10a, ‘풍원미’ 2,625 kg/10a 수준이었다. 2. 바이러스 무병묘를 7월 상순에 정식하여 재배하여도 씨고구마로 사용하기에 알맞은 100~300 g 크기의 괴근 수량은 ‘신율미’ 2,043, ‘진홍미’ 1,799, ‘다호미’ 1,390, ‘풍원미’ 1,985 kg/10a 정도가 생산되었다. 3. 고구마 바이러스 무병묘 정식 후 110일, 120일, 그리고 130 일 재배 시 씨고구마 수량은 ‘풍원미’ 1,605, 1,907, 1,834 kg/ 10a, ‘호감미’ 1,816, 1,771, 2,137 kg/10a 수준으로 생산되었다. 4. 수확 전 채취한 고구마 잎에서 SPLCV, SPFMV, SPVG, SPLV 등 4종 바이러스 이병 정도를 검정한 결과 정식시기, 재배기간 등 품종에 따라 약간 차이는 있으나 낮게 검출되어 다음해 씨고구마 종자로 문제가 없다고 판단하였다. 5. 바이러스 무병묘 대량 증식에는 시설과 노력이 많이 소요되고 증식량이 적어 면적 확대에 어려움이 있기 때문에 무병씨고구마를 생산하면 면적 확대에 유리하다. 무병묘가 소량 일 경우는 계속 증식하면서 7월 상순까지 본밭에 정식하여도 씨고구마 생산이 가능하였다. 금후에는 무병묘로 생산한 연차 간 씨고구마에 대해 품종별 수량과 품질 평가 후 씨고구마의 적정 갱신 주기를 설정하고자 한다.
Three-dimensional(3D) printing is a process for producing complex-shaped 3D objects by repeatedly stacking thin layers according to digital information designed in 3D structures. 3D printing can be classified based on the method and material of additive manufacturing process. Among the various 3D printing methods, digital light processing is an additive manufacturing technique which can fabricate complex 3D structures with high accuracy. Recently, there have been many efforts to use ceramic material for an additive manufacturing process. Generally, ceramic material shows low processability due to its high hardness and strength. The introduction of additive manufacturing techniques into the fabrication of ceramics will improve the low processability and enable the fabrication of complex shapes and parts. In this study, we synthesize silica composite material that can be applied to digital light processing. The rheological and photopolymeric properties of the synthesized silica composite are investigated in detail. 3D objects are also successfully produced using the silica composite and digital light processing.
Cervical neck dissection is a frequent technique during treatment for oral squamous cell carcinoma (SCC). Occasionally, specimens harvested as cervical lymph nodes reveal thyroid tissue and need differentiation with metastatic thyroid cancer and ectopic thyroid tissue. Here, we report a case of an ectopic thyroid tissue with lymphocytic thyroiditis mimicking thyroid cancer metastasis at the cervical lymph node.
1. 본 연구는 고구마의 큐어링 처리 및 저장기간에 따른 품종별 저장성 차이를 조사하여 품종별 적정 저장 조건을 설정하고자 수행하였다. 수확된 고구마는 온도 32±1℃, 상대습도 92±3% 조건에서 3일간 큐어링 처리를 실시하였고 대조구와 함께 13±℃의 저장고에 30주간 저장하였다. 2. 저장 기간에 따른 부패율 및 감모율은 품종별로 큐어링 처리 여부에 따라 다른 양상을 보였으며 대부분 품종에서 큐어링 처리구의 부패율과 감모율이 낮게 나타났다. 품종별로는 ‘호감미’, ‘풍원미’, ‘신건미’, ‘주황미’가 장기저장을 위해서 큐어링 처리가 필요한 품종으로 나타났으며, ‘다호미’, ‘연자미’ 품종은 큐어링 처리 여부에 따른 유의한 차이가 없었다. 3. 큐어링 처리 여부에 따른 부패율 차이가 없었던 ‘다호미’, ‘연자미’를 제외한 나머지 품종은 감모율 조사에서도 큐어링 처리가 장기 저장에 더 유리한 것으로 조사되었다. 4. ‘호감미’ 품종의 경우 저장기간별 부패율 및 감모율을 예측하고 조수입을 계산하였을 때 큐어링 처리 시에는 조수입이 증가하였으나 큐어링 무처리 시에는 저장기간이 길어질수록 조수입이 감소하였다. 5. 따라서 이러한 품종별 저장성 차이를 고려하여 각 품종에 맞는 수확 후 관리 및 적정 출하시기를 예측하는 것이 고구마 저장성 증대 및 농가 소득 향상에 유용하게 적용될 수 있을 것으로 판단된다.
This study was carried out to obtain the basic quality characteristics, like moisture contents, hunter color value, total polyphenol, starch, amylose, and ash contents and pasting characteristics of sweet potato cultivars according to storage periods. Moisture contents of all the varieties decreased with long storage period, and were lower in dry type than tender and moist type sweet potato. Lightness(L value) of sweet potato flesh was decreased in Shinyulmi, Daeyumi, Shinhwangmi but other seven cultivars showed increasing trend. Redness(a value) was increased in Sinyulmi, Sinhwangmi, Sinjami and yellowness (b value) increased in Yeonjami only. The total polyphenol contents increased in Dahomi, Sinjami up to 4 months of storage and all other varieties showed decrease during storage period. The starch contents also decreased with storage period. The amylose contents showed different by the cultivars. The ash contents in all varieties ranged from 1.1 to 1.7%, and there was no difference among varieties and storage periods. There was no change in pasting temperature during storage periods. Peak viscosity, through viscosity, breakdown and final viscosity were different according to storage periods and cultivars. But setback tended to increase in all cultivars.