In this study, nano-sized tin oxide powder with an average particle size of below 50 nm is prepared by the spray pyrolysis process. The influence of air pressure on the properties of the generated powder is examined. Along with the rise of air pressure from 0.1kg/cm2 to 3kg/cm2, the average size of the droplet-shaped particles decreases, while the particle size distribution becomes more regular. When the air pressure increases from 0.1kg/cm2 to 1kg/cm2, the average size of the dropletshaped particles, which is around 30-50 nm, shows hardly any change. When the air pressure increases up to 3kg/cm2, the average size of the droplet-shaped particles decreases to 30 nm. For the independent generated particles, when the air pressure is at 0.1kg/cm2, the average particle size is approximately 100 nm; when the air pressure increases up to 0.5kg/m2, the average particle size becomes more than 100 nm, and the surface structure becomes more compact; when the air pressure increases up to 1kg/cm2, the surface structure is almost the same as in the case of 0.5kg/cm2, and the average particle size is around 80- 100 nm; when the air pressure increases up to 3kg/cm2, the surface structure becomes incompact compared to the cases of other air pressures, and the average particle size is around 80-100 nm. Along with the rise of air pressure from 0.1kg/cm2 to 0.5kg/cm2, the XRD peak intensity slightly decreases, and the specific surface area increases. When the air pressure increases up to 1kg/cm2 and 3kg/cm2, the XRD peak intensity increases, while the specific surface area also increases.

본 연구는 백년초 분말 첨가가 아질산염의 대체를 통한 소시지의 품질 특성에 미치는 영향을 조사하기 위하여 C(아질산염 및 백년초 분말 무 첨가구), T1(0.014% 아질산염 첨가구), T2(0.014% 아질산염 + 0.5% 백년초 분말 첨가구), T3(0.014% 아질산염 + 1.0% 백년초 분말 첨가구), T4(0.5% 백년초 분말 첨 가구) 및 T5(1.0% 백년초 분말 첨가구)로 처리하며 소시지를 제조하였으며 4℃에서 15일간의 저장을 통하여 실험을 실시하였다. 명도를 나타내는 CIE L*값은 대조구가 다른 모든 처리구들에 비해 높게 나타났 으며, 적색도를 나타내는 CIE a*값은 T5 처리구가 T1과 T3 처리구의 중간 값인 10.84-11.30 범위를 나 타내었다(p<0.05). 황색도를 나타내는 CIE b*값과 보수력 및 조직감을 나타내는 응집성, 탄력성 그리고 씹힘성은 T5 처리구에서 다른 처리구들에 비해 유의적으로 높게 조사되었다(p<0.05). 이에 반하여, 수분 함량, pH 및 백색도를 나타내는 W값은 T1 처리구에서 가장 높게 나타났다. 관능적 특성에서는 T1과 T5 처리구 간 유의적인 차이가 나타나지 않았다(p>0.05). 따라서 본 실험 결과에 의하면 0.014% 아질산염의 소시지내 첨가는 1.0%의 백년초 분말로 대체시 조직감에 부정적인 영향을 주지 않으면서도 적색도를 높일 수 있는 소시지 제조가 가능할 것으로 판단되며 이를 실용화하기 위해서는 제품의 유통기한 설정에 관한 추가 연구가 필요할 것으로 사료된다.

The principal objective of this study was to evaluate the quality characteristics of dried noodles when different concentrations of Loquat (Eriobotyya japonica Lindley) leaf powder (LLP) were added to the wheat flour. The cooking quality, mechanical texture properties, and viscosity were measured, and a sensory evaluation was conducted with the prepared noodles. The gelatinization points of the composite LLP-wheat flours were shown to increase. As measured via amylograph, viscosity at 95℃, viscosity at 95℃ after 15 minutes, and maximum viscosity values of those samples decreased as the LLP content increased. As increasing amounts of LLP were added, the L and a values were reduced, whereas the b value was increased and the color values, weight, and volume of the cooked noodle increased, as did the turbidity of the soup. With regard to the textural characteristics, the LLP additive increased hardness and cohesiveness, and reduced adhesiveness and springiness. Overall, the noodles prepared with 5% LLP were preferred more than the others, according to the results of our sensory evaluation.

1. 원료 형태별 청국장의 발효시간에 따른 건물중은 콩, 환, 분말의 모든 원료형태에서 발효시간이 경과할수록 건물의 중량이 감소하는 경향을 보였다. 2. 원료 형태별 청국장의 발효시간에 따른 진의 길이 변화를 측정한 결과, 모든 원료 형태에서 발효시간이 경과할수록 진의 길이가 증가하는 경향을 보였으며, 48시간 이후에는 그 증가치가 완만함을 보였다. 태광콩을 콩의 형태로 발효하였을 때 진의 생성이 가장 많았고, 분말을 1cm의 두께로 발효하였을때 진이 거의 생성되지 않았다. 3. 원료 형태별 청국장의 발효시간에 따른 생균수의 변화를 측정한 결과, 콩 형태로 발효시켰을 경우 모든 품종에서 비슷한 수준의 생균수가 측정되었다. 환 형태로 발효시켰을 경우 12시간 이후에 생균수가 급격히 증가하다가 24시간 이후 증가치가 완만해졌다. 분말형태로 발효시켰을 경우 시간에 따라 경시적으로 증가하였다. 4. 원료 형태별 청국장의 발효시간에 따른 색도의 변화를 측정한 결과, 모든 원료 형태에서 발효시간이 경과할수록 명도는 흑색에 가까워졌고, 색상과 채도의 경우는 각각 적색과 황색을 띠는 쪽으로 변화하였다. 5. 원료 형태별 청국장의 발효시간에 따른 pH의 변화를 측정한 결과, 모든 원료 형태에서 발효시간이 경과할수록 알칼리성으로 변화하였다. 6. 원료 형태별 청국장의 발효시간에 따른 isoflavone 함량의 변화를 측정한 결과, 발효 후 48시간까지 isoflavone의 함량이 증가하다 감소하는 경향을 보였다. 7. 청국장을 건조온도를 달리하여 균의 재생능력을 실험해본 결과 동결건조를 하였을 때 가장 많은 수의 균이 존재하였다. 8. 분말 또는 분말 (환)의 형태로 청국장을 만들 경우 종자 이용 시 보다 청국장의 품질이 떨어졌으며 분말 (환)을 이용하여 경제적인 청국장 제조를 위해서는 더 많은 연구가 필요한 것으로 고려되어 진다.

In this study, the effect of milling time on the microstructure and phase transformation behaviors of Ni-12 wt.%B powders was investigated using vibratory ball milling process. X-ray diffraction patterns showed that the phase transformation of mixed Ni-B elemental powder occurred after 50 hours of milling, with a formation of nickel boride phases. Through the study of microstructures in mechanical alloying process, it was considered that ball milling strongly accelerates solid-state diffusions of the Ni and B atoms during mechanical alloying process. The results of X-ray photoelectron spectroscopy showed that most of B atoms in the powder were linked to Ni with a formation of nickel boride phases after 200 hours of milling. It was finally concluded that mechanical alloying using ball milling process is feasible to synthesize fine and uniform nickel boride powders.

꾸지뽕잎 분말의 첨가량을 0-20%로 달리하여 스펀지 케이크를 제조한 후 물리화학적 품질특성 및 소비자 기호도를 비교하였다. 꾸지뽕잎 분말의 첨가비율이 증가함에 따라 케이크의 비체적, 높이 및 수분함량은 단계적으로 감소하는 경향을 나타내었고, 케이크의 외관상 특성인 부피지수 및 대칭지수 또한 유의적으로 감소하였다(p < 0.05). 밝기를 나타내는 L*값과 황색도를 나타내는 b*값은 꾸지뽕잎 분말 첨가량이 증가할수록 단계별로 유의적으로 감소하였으며(p < 0.05), 반면 적색도를 나타내는 a*값은 5% 대체군에서 최소값을 나타내고 이 후 증가하는 경향을 나타내었다(p < 0.05). 케이크의 경도는 꾸지뽕잎 분말 첨가량에 따라 0.11-0.66 kgf로 단계별로 유의적으로 증가하였다(p < 0.05). 총 페놀화합물 함량은 0-15% 첨가군 사이에 단계별로 유의적인 차이없이 증가하는 경향을 나타내었고(p > 0.05) 이후 유의적인 증가를 보였다. 소비자 기호도 검사 결과 대조군, 5% 및 10% 첨가군 간 맛과 향미의 유의적인 차이는 발견되지 않았고(p > 0.05), 전체적인 기호도 또한 대조군과 5% 첨가군 사이에 유의적인 차이는 발견되지 않아(p > 0.05), 관능품질을 저해하지 않고 꾸지뽕잎 분말의 건강 기능성 효과 등을 고려할 때 5% 첨가군이 가장 적절한 것으로 판단된다.

본 연구는 식품소재로서의 활용가능성이 높고 생리활성 효과가 우수한 황기분말을 농도별로 첨가(0.5%, 1.0%, 1.5%, 2.0%)하여 어묵을 제조하고 품질특성을 측정하였다. 수분함량은 황기분말의 첨가여부에 관계없이 유의적인 차이는 나타나지 않았으며 pH는 전체적으로 6.75-6.86의 범위를 나타내었다. L값은 황기분말의 첨가량 증가에 따라 유의적인 차이는 나타나지 않았으나 a값은 높아지고 b값은 낮아지는 경향을 나타내었다. 황기분말 첨가 어묵의 절곡검사 결과는 모든 시료에서 AA로 측정되어 황기분말의 첨가가 어묵의 유연성에 영향을 미치지 않았으며 기계적 조직감 중 강도(strength)는 황기분말의 첨가량이 증가할수록 높아지는 경향을 나타내었고 검성(gumminess), 응집성(cohesiveness), 파쇄성(brittleness)은 황기분말 2.0% 첨가구가 가장 높게 측정되었다. 황기분말 첨가 어묵의 관능적특성 중 생선 비린내 정도(fishy smell)는 황기분말의 첨가량 증가에 따라 강도의 정도가 약해졌으며 구수한 냄새의 정도(savory smell)는 황기분말 1.0% 첨가구가 가장 높은 점수를 보였다. 구수한 맛의 정도(savory taste)는 황기분말 1.0% 첨가구가 6.27로 가장 높은 점수를 나타내었으며 느끼한 맛의 정도(oily taste)는 황기분말 첨가량의 증가에 따라 약해지는 것으로 평가되었다. 황기맛의 정도(Astragalus membranaceus taste)는 황기냄새의 정도와 마찬가지로 황기분말의 첨가량이 증가할수록 강하게 평가되었으며 관능적 조직감의 정도는 각 시료간 유의적인 차이가 나타나지 않았다. 관능적 선호도 평가결과, 황기분말 1% 첨가구가 냄새, 맛, 조직감, 전반적인 선호도 항목에서 가장 우수함을 나타내었다.

단립종 100%, 장립종 100%, 단립종 50%와 팽화미분 50% 그리고 장립종 50%와 팽화미분 50%로 제조한 탁주의 pH, 산도, 단백질, 색도, 환원당, 총당, 알코올 그리고 관능성질을 조사하였다. 모든 시료의 pH는 발효 초기에 급격히 감소한 후 장립종 100%를 제외하고 서서히 상승하였다. 발효 2일 후 단립종은 장립종보다 그리고 팽화미분은 순 쌀보다 같거나 높았다(p < 0.05). 산도는 발효 시간 지낼수록 모든 시료에서 증가하였다. 장립종 100%는 단립종 100%보다 3일부터 그리고 장립종 50%는 단립종 50%보다 4일부터 높았다(p < 0.05). 모든 시료의 단백질은 1일에 증가한 후 감소하였고 팽화미분은 순 쌀과 같거나 높았다(p < 0.05). L값은 모든 시료에서 발효 초기에 증가한 후 감소하였다. 발효 4일부터 단립종은 장립종보다 그리고 3일부터 팽화미분은 순 쌀보다 L값이 낮았다. 담금 직후부터 순 쌀의 a값은 점점 감소하였고 팽화미분은 3일 때까지 증가하다가 감소하였다. 모든 시료의 b값은 발효 2와 3일에 최고값을 보인 후(p < 0.05) 감소하는 경향을 보였다. 담금 직후 팽화미분은 순 쌀보다 환원당이 훨씬 높았다. 순 쌀은 발효 1일에 증가한 후 감소하였고 팽화미분은 급격히 감소하였다. 총당은 환원당과 유사하였다. 알코올은 발효 2일까지 모든 시료에서 급격히 증가하였고 단립종은 장립종보다 그리고 팽화미분은 순 쌀보다 항상 높았다(p < 0.05). 단립종 100%와 장립종 100%는 1% 수준에서 유의적인 차이가 있었지만 선호도는 차이가 없었다. 단립종 50%와 장립종 50%는 유의적으로 차이가 없었다.

Soybean powder is a readily-available food ingredient. Furthermore, saltwort powder is an herb with various physiological effects. Therefore, in this study we examined the physiochemical characteristics of soybean dasik prepared with 0, 4, 8, and 12% saltwort powder. We measured Hunter's color values, mechanical characteristics, and sensory qualities. The result of each analysis is as follows. There were not significant differences between the moisture content of the control group and the groups with saltwort powder. The ash content increased while the fat and protein content decreased as the ratio of saltwort powder increased (p<0.001). In the analysis of color differences, the L, a, and b values decreased as the ratio of saltwort powder increased (p<0.001). The hardness (p<0.001) of the groups increased as the ratio of saltwort powder increased, but adhesiveness decreased. Sensory evaluation data showed that softness, hardness, and chewiness decreased while color increased as the ratio of saltwort powder increased. Finally, aroma, sweet taste, nutty taste, and overall acceptability was shown to be best for the 4% addition group.

In this study, p-type : TAGS-85 compound powders were prepared by gas atomization process, and then their microstructures and mechanical properties were investigated. The fabricated powders were of spherical shape, had clean surface, and illustrated fine microstructure and homogeneous + GeTe solid solution. Powder X-ray diffraction results revealed that the crystal structure of the TAGS-85 sample was single rhombohedral GeTe phase, which with a space group . The grain size of the powder particles increased while the micro Vickers hardness decreased with increasing annealing temperature within the range of 573 K and 723 K due to grain growth and loss of Te. In addition, the crystal structure of the powder went through a phase transformation from rhombohedral () at low-temperature to cubic () at high-temperature with increasing annealing temperature. The micro Vickers hardness of the as-atomized powder was around 165 Hv, while it decreased gradually to 130 Hv after annealing at 673K, which is still higher than most other fabrication processes.

The present study focused on the synthesis of Bi-Te-Se-based powder by an oxide-reduction process, and analysis of the thermoelectric properties of the synthesized powder. The phase structure, chemical composition, and morphology of the synthesized powder were analyzed by XRD, EPMA and SEM. The synthesized powder was sintered by spark plasma sintering. The thermoelectric properties of the sintered body were evaluated by measuring its Seebeck coefficient, electrical resistivity, and thermal conductivity. powder was synthesized from a mixture of , , and powders by mechanical milling, calcination, and reduction. The sintered body of the synthesized powder exhibited n-type thermoelectric characteristics. The thermoelectric properties of the sintered bodies depend on the reduction temperature. The Seebeck coefficient and electrical resistivity of the sintered body were increased with increasing reduction temperature. The sintered body of the powder synthesized at showed about 0.5 of the figure of merit (ZT) at room temperature.

In this study, powder metallurgy and severe plastic deformation by high-pressure torsion (HPT) approaches were combined to achieve both full density and grain refinement at the same time. Water-atomized pure iron powders were consolidated to disc-shaped samples at room temperature using HPT of 10 GPa up to 3 turns. The resulting microstructural size decreases with increasing strain and reaches a steady-state with nanocrystalline (down to ~250 nm in average grain size) structure. The water-atomized iron powders were deformed plastically as well as fully densified, as high as 99% of relative density by high pressure, resulting in effective grain size refinements and enhanced microhardness values.

Green strength is an important property of powders since high green strength guarantees easy and safe handling before sintering. The green strength of a powder compact is related to mainly mechanical and surface characters, governed by interlocking of the particles. In this study, the effect of powder surface roughness on the green strength of iron powders was investigated using a transverse rupture test. Three-dimensional laser profiler was employed for quantitative analyses of the surface roughness. Two different surface conditions, i.e. surface roughness, of powders were compared. The powders having rough surfaces show higher green strength than the round surface powders since higher roughness leads increasing interlocked area between the contacting powders.

It was researched to be alternative of TGIC type hardener with human hazard element as PT 910 mix powder paint with hardener. Generally PT 910 was compared with TGIC & Epoxy resin of hardener to be used at thermosetting powder paint. We inquired a property of matter for paint through Gel time, glass transition temperature, melting point and a property of matter for film through a property of adhesion, a property of tolerance, softness, gloss, acid-resistant, alkali-resistant, salt water spray-resistant, facilitation climatic. When PT 910 is used of hardener, it was shown the excellent results in gel time, softness, salt water spray-resistant, fracilitation climatic and the similar results in melting point, a property of tolerance, a property of adhesion, gloss, acid-resistant, alkali-resistant, as compared with the powder paint used by TGIC hardener. The glass transition temperature was little low. But there was slightly different results. After the study results, we reached the conclusion that thermosetting powder used by PT 910 is alterative to by TGIC hardener.

Antioxidant agent, 1,1,3-tris(2-methyl-4-hydroxy-5-tert-butylphenyl)butane were prepared and investigated the antioxidant activity on recycled rubber mat manufactured with waste tire powder. Mechanical properties of rubber mat are influenced by many factor such as compounding ingredients and state of cure, process of rubber, and fillers. Our study aim is to investigate influence of antioxidant activities on ozone cracking and the thermal aging time. In this work, the degradation of recycled rubber mat was studied and suggested mechanism to involve two-type of degradation, thermal aging and cracking both of which can be contained antioxidant or non-antioxidant agent.

Nano-sized Y2O3 powders were prepared via a sol-gel method starting with Y(NO3)3·6H2O (Yttrium(III) nitrate hexahydrate) and water with ethanol as a cosolvent. Y2O3 is an important rare earth oxide and has been considered for use in nuclear applications, such as ceramic materials, due to its excellent optical and refractory characteristics. It has been used as a chemically stable substrate, a crucible material for melting reactive metals, and a nozzle material for jet casting molten rare earth-iron magnetic alloys. Oxalic acid (C2H2O4) has been adopted as a chelating agent in order to control the rate of hydrolysis and polycondensation, and ammonia was added in order to adjust the base condition. The synthesized Y2O3 powder was characterized using TG/DTA, XRD, FE-SEM, BET and Impedance Analyzer analyses. The powder changed its properties in accordance with the pH conditions of the catalyst. As the pH increases according to the FE-SEM, the grain grew and it showed that the pore size decreased while confirming the effect of the grain size. The nano-material Y2O3 powders demonstrated that the surface area was improved with the addition of oxalic acid with ammonium hydroxide.

This study was performed to analyze the retarded degree of Garaetteok retrogradation added with different ratios 0-15% (w/w) of apple pomace dietary fiber powder (DFP). SEM (×500) showed that air cell size on the Garaetteok surface increased as DFP content increased, whereas control had a compact structure without air cells. The degrees of Garaetteok retrogradation after 3 days at 4 and 25℃ by α-amylase iodine method were 57.44 and 41.55% for control, respectively. On the other hand, those of 15% DFP Garaetteok were 28.38 and 15.05%, respectively. Enthalpy changes (δE) by DSC of control, 10 and 20% DFP Garaetteok after 3 days of storage at 4℃ were 4.41, 4.17, and 3.80 J/g, respectively, whereas those at 25℃ were 2.14, 1.04, and 0.72 J/g. Hardness of 15% DFP Garaetteok was around 48% compared to that of control after 3 days of storage at 25℃. Increasing DFP content from 0 to 15% decreased L color value from 86.2 to 55.1, whereas a and b values increased from -1.9 to 8.9 and from 5.3 to 20.8, respectively. In a sensory intensity test, hardnesses of 15% DEP Garaetteok were significantly different at 1 and 0.1% compared to those of control after production and followed by storage for 3 days at 4℃, respectively.