The effect of chemical composition of the sintering atmosphere on density, microstructure and mechanical properties of Fe-3%Mn-(Cr)-(Mo)-0.3%C steels is described. Pre-alloyed Astaloy CrM and CrL, ferromanganese and graphite were used as the starting powders. Following pressing in a rigid die, compacts were sintered at 1120 and in atmospheres having different ratio and furnace cooled to room temperature. It has been found that the atmosphere composition has negligible effect on the as-sintered properties of the investigated materials.
The effect of different cooling rate on the structure and mechanical properties of Fe-3%Mn-(Cr)-(Mo)-0.3%C steels is described. Pre-alloyed Astaloy CrM and CrL, ferromanganese and graphite were used as the starting powders. Following pressing in a rigid die, compacts were sintered at and in atmospheres and cooled with cooling rates and . Convective cooled specimens were subsequently tempered at for 60 and 240 minutes.
The characteristics of residual stresses occurring in PM steel based nickel (FLN2-4405) was investigated. The measurements of residual stresses were carried out by electrochemical layer removal technique. The values and distributions of residual stresses occurring in PM steel processed under various densities and heat treatment conditions were determined. In most of the experiments, tensile residual stresses were recorded in surface of samples. The residual stress distribution on the surface of the PM steels is affected by the heat treatment conditions and density. Maximum values of residual stresses on the surface were observed sinter hardened condition and density. Minimum level of recorded tensile residual stresses are150 MPa and its maximum level is 370 MPa.
The use of the nickel free, high nitrogen stainless steel powder and nitriding during sintering of iron based materials have been shown as an alternative way to the conventional PM stainless steels containing nickel. Nitrogen as an alloying element for iron improves in an effective way the properties of sintered alloyed steels. The powder metallurgy route is a suitable way to introduce nitrogen into these alloys and, in particular, to produce high nitrogen (close to the solubility limit) stainless steels. The paper presents and discusses the nitriding behavior of nickel-free stainless steels produced by powder metallurgy method. Alloyed melt was atomized by nitrogen and in this way nitrogen was introduced into the powder. Further nitriding occurred during sintering in a nitrogen atmosphere. For comparison, compacts having the same composition as an alloyed powder were produced from elemental powders mixture. Sintering-nitriding behaviour of investigated materials has been controlled by dilatometry, chemical and X-Ray phase analysis and metallography. Mechanical properties of sintered compacts were also measured.
The mixed atomized iron powders with 0.3% graphite and 1% Ni powders were cold pressed and sintered at for 30 min under pure Ar gas atmosphere. Some of the sintered specimens were intercritically annealed at and quenched in water (single quenching). The other sintered specimens were first fully austenized at and water quenched. These specimens were then intercritically annealed at and re-quenched in water. The experimental results showed that the wear coefficient effectively decreased in the double quenched specimen.
Due to the increasing use that the stainless steel is getting recently in the nuclear industry, this document proposes the study of the stainless steel 316L with boron addition. With the final product, the properties of the stainless steel 316L (good mechanical properties and high corrosion resistance) with the boron neutron absorption properties are claimed to unify. The P/M technologies allow adding higher boron quantities than with the solidification conventional technologies, where segregation is produced.
This study was conducted to improve the durability and decrease the friction of the sintered bushing used in the joints of construction equipment. Research was carried out to examine the effects of the groove pattern on the inner surface. The following results were obtained: (1) The bushing (EK Bush) with grooves on the inner diameter showed increased durability as compared to a non-grooved bushing. (2) The helical-grooved bushing showed the least amount of wear; it was 1/10 of the wear of the non-grooved bushing. (3) If the distance between grooves was decreased, then the coefficient of friction also decreased.
We investigated that the effect of based compound on machinability of two types of PM steels. One is a copper steel which is selected as a general PM steel, and the other is a diffusion alloyed steel selected as a high strength PM steel. It is found that based compound addition improves machinability in drilling of both of the PM steels. Although the compound addition degrades the mechanical properties of PM steels, it is considered that decrease of the properties can be compensated by increasing density.
The present paper investigates the possibilities of niobium using for the mechanical properties of the common low alloyed Cu-Ni-Mo-C sintered structural steels enhancing. On both thermodynamic and experimental bases there were demonstrated the Nb nitrides/carbides/carbonitrides preferential formation in these steels during sintering in dissociated ammonia at both common and elevated temperatures. The obtained results for fine Nb powder and 0.3% graphite additions to Distaloy AB iron base powder cold compacted and sintered in dissociated ammonia proved the expected strengthening effect, leading to higher mechanical properties of the processed steels than of the common Cu-Ni-Mo-C ones.
This work presents mechanical properties and corrosion resistance of duplex stainless steels obtained through powder metallurgy starting from austenitic, martensitic powders by controlled addition of alloying elements in the right quantity to obtain the chemical composition of the structure similar to biphasic one. In the mixes preparations the Schaffler's diagram was taken into consideration. Prepared mixes of powders have been sintered in a vacuum furnace with argon backfilling. After sintering rapid cooling was applied using nitrogen. Corrosion properties have been studied through electrochemical methods in 1M NaCl.
Several chemicals were studied to suppress the damage due to stress corrosion cracking (SCC) of steam generator (SG) tubes in nuclear power plants. The effects on the SCC of the compounds, , TyzorLA and , were tested for several types of SG tubing materials. The test with the addition of and showed an effect in decreasing the SCC for the SG tubing material. However, caused some more SCC for Alloy 800. The penetration property into a crevice of the inhibitors was investigated by using Alloy 600 specimens with different gap.
The stress corrosion cracking (SCC) susceptibility of Alloy 600 MA, Alloy 600 TT, Alloy 800, and Alloy 690 TT were investigated in a deaerated 0.01 M solution of sodium tetrathionate using reverse u-bend test samples at . The results showed that SCC occurred in all alloys, excluding Alloy 690 TT. The SCC susceptibility decreased with an increase in the chromium content of the alloys. The results of the deposits and spectra taken from an energy dispersive X-ray system confirmed the existence of a reduced sulfur causing SCC.
Based on the comparison of structures and properties of the HS6-5-2 high speed steels made with the powder injection moulding method, pressureless forming, compacting and sintering, and commercial steels made with the ASEA-STORA method, fine carbides spread evenly in the steel matrix were found in the structure of all tested high-speed steels in the sintered state. The steels made with the pressureless forming method are characteristic of the lowest sintering temperature and the highest density, resulting from the high carbon concentration coming from the binding agent degradation.