Mg-Zn-RE alloys had a novel lond period stacking ordered (LPO) structure. Their rapidly solidified powder metallurgy (RS P/M) alloys exhibited a combination of high strength and god ductility (tensile yield strength above 550 MPa and elongation above 5%). The LPO Mg-Zn-RE RS P/M alloys had high elevated temperature strength (tensile yield strength above 380 MPa at 473 K) and exhibited a high-strain-rate superplasticity at higher temperatures. In Japan, a national project for developing high strength LPO Mg-Zn-RE RS P/M alloys has started at 2003 for 5 years, which is founded by the Ministry of Economy, Trade and Industry (METI) of Japan. In the national project, project targets in materials performances have been achieved. The developed LPO Mg-Zn-RE RS P/M alloys exhibited higher tensile yield strength, fatigue strength and corrosion resistance than high strength aluminum alloys of extra-super-duralumin (7075-T6).
The vacuum infiltration method is one of the composite producing methods. There are several parameters in composite production by vacuum infiltration. One of them is particle size of reinforcement in particulate reinforced composites. In this study, MgO powder and Al were used as reinforcement and matrix respectively. MgO powders with different size and amount to give same height were filled in quartz tubes and liquid metal was vacuum infiltrated into the MgO powder under same vacuum condition and for same time. Infiltration height was measured and microstructure and fracture behavior of composite were investigated. It has been found that infiltration height and fracture strength were increased with particulate reinforcement sizes. It has also been determined that molten metal temperature facilitates infiltration.
Chemically pure, hydride/dehydride titanium powders were cold pre-compacted then extruded at and under argon. The extrusions were 100% dense with a narrow band of surface porosity and equiaxed microstructure of similar magnitude to the starting material. The tensile properties of the bars were better than conventionally extruded CP titanium bar product. Outcomes from this study have assisted in the identification of a number of key characteristics important to the extrusion of titanium from pre-compacted CP titanium powders, allowing the elimination of canning and hot isostatic pressing (HIPping) of billets prior to extrusion as per conventional PM processes.
The ever increasing requirements on today's compacts with regard to their geometry and precision call for flexible high-precision and most capable production systems. DORST Technologies has coped with these requirements by developing the new HP series for pressing forces between 1600 kN and 16000 kN and the new HS series for pressing forces between 150 kN and 1200 kN. These fully hydraulic presses featuring upper ram, lower ram, core rod, filler, up to 4 lower tool levels and up to 4 upper tool levels with closed-loop controlled movements. Thanks to latest servo technology and an electronic bus system it is possible to have all movements closed-loop controlled in the desired relation to each other. Thus, today's hydraulic presses provide high stroke rates, low energy consumption and a user-friendly interface. The input of data is carried out via clearly arranged screen masks on a touch-screen. The innovative DORST (Intelligent Program Generator) has been designed to support the set-up staff in preparing and optimizing the toolprogram. The combination of the machine type with the hydraulic unit determines the productivity in consideration of the specific application and the part to be pressed. Thanks to the closed-loop control circuits, DORST hydraulic automatic presses of the latest generation ensure unmatched precision and repeatability - and consequently process reliability - often without necessitating subsequent machining steps.
New product line with additional secondary operation of oil pump rotor was built in necessity of increasing capacity. This new line includes steam treatment process after sizing. The new line achieved 1.6 times higher performance compared with a conventional line.
The well-established Universal Powder Press UPP, designed by the Swiss press manufacturer Osterwalder AG in Lyss, went through a major improvement process. The result is a high efficient production machine with state-of-the-art technology. It will be shown the technical design, some process engineering as well as the influence of PRP - =Part-Related-Programming, first published in 1994 - on the set-up time. This development has enabled Osterwalder to round off their range of presses, the mechanical-hydraulic KPP as well as the hydraulic CA-NC II and UPP, to an attractive offer ranging from 120 kN up to 10'000 kN.
We reported a P/M soft magnetic material with core loss value of , which is lower than that of 0.35mm-thick laminated material, by using high purity gas-atomized iron powder. Lack of mechanical strength and high cost of powder production are significant issues for industrial use. In order to achieve both low core loss and high strength by using inexpencive powder, the improvement of powder shape and surface morphology and binder strength was conducted. As the result, the material based on water-atomized powder with 80 MPa of TRS and 108 W/kg of core loss (W10/1k) was achieved.
[ ] nanocomposite powders with a nominal composition of were prepared by HDDR combined with mechanical milling. The microstructure was studied by Mossbauer spectrometry and TEM. The magnetic properties were investigated by VSM using bonded magnet samples. The results showed that the annealing temperature had significant influence on both the recombination kinetics and the grain size of the and phases, and the bonded magnets presented the best magnetic properties when the nanocomposite powders were prepared by annealing at for 30 min.
Innovative SMC with low iron loss was made from iron powders with evaporated MgO insulation coating. The coating had greater heat-resistance than conventional phosphatic insulation coating, which enabled stress relieving annealing at higher temperature. Magnetic properties of toroidal samples (OD35mm,ID25mm, t5) were examined. The iron loss at 50Hz for Bm = 1.5T was lower 50% of conventional SMC and was almost the same with silicon iron laminations(t0.35). It became clear that MgO insulation coating has enough heat resistance and adhesiveness to powdersurface to obtain innovative SMC with low iron loss.
Fabrication of matrix in-situ composite, reinforced by a FeAl phase, was studied by using the powder metallurgical processing route. Especially, in order to disperse the second phase more finely, we chose the mechanical alloying process. We investigated the microstructural and mechanical properties of the consolidated material. After consolidation by vacuum hot pressing, the compact showed almost full density and consisted of a matrix and FeAl second phase (average particle size was less than 1m). The compact showed HV746, which was higher than that of the arc melted monolithic material, HV603.
A non-equilibrium powder metallurgy processing such as an MA/SPS (Mechanical Alloying / Spark Plasma Sintering) process is examined in a Ti-48moll%Al. TiAl intermetallic compound is a potential light-weight/high-temperature structural material. One of the major problems, however, limiting the practical use of the material is its poor workability. From this point, the powder metallurgy (PM) processing route has been attractive alternative of the conventional processing for such material The MA/SPS process is able to apply to a LIGA process. Optimization of the pseudo-superplasticity enables to fabricate micro-parts made of fine grained ceramics composites of TiAl by the LIGA process.
Various reactions and the in-situ formation of new phases can occur during the mechanical alloying process. In the present study, Al powders were strengthened by AlN, using the in-situ processing technique during mechanical alloying. Differential thermal analysis and X-ray diffraction studies were carried out in order to examine the formation behavior of AlN. It was found that the precursors of AlN were formed in the Al powders and transformed to AlN at temperatures above . The hot extrusion process was utilized to consolidate the composite powders. The microstructure of the extrusions was examined by SEM and TEM. In order to investigate the mechanical properties of the extrusions, compression tests and hardness measurements were carried out. It was found that the mechanical properties and the thermal stability of the Al/AlN composites were significantly greater than those of conventional Al matrix composites.
Both plastic and elastic properties change dramatically from the beginning to the end of the compaction phase. Previous investigations have shown that powder transfer and high powder flow during initial compaction at low density affects the strength of the final component significantly. Investigated here are shear failure and elastic shear modulus in the low density range for hard metal powder and for pre-alloyed water atomized iron powder. Direct shear test equipment for sand and clay has been modified to measure the shearing properties of powder for an axial loading between 1 kPa and 500 kPa.
In the present work, the influence of the ball-milling time, milling atmosphere and weight ratio of ball to powder on characteristics of was studied. Results show that, the grain sizes of the and CuO in the ball-milled powder mixture were significantly decreased with increasing the milling time. Those of each oxide ball-milled in Argon and Hexane atmosphere for 30 and 20 hour were about 98 and 84 nm, respectively. After milling of 20 hour in Hexane as PCA, the powder had a homogeneously mixed structure and the average size of powders was determined to about 230nm.
Sintered composites of Al-8wt%Cu-10vol%SiCp were deformed by repressing or equal channel angular pressing(ECAP) at room temperature, and . Repressing produced more densification than ECAP but resulted in much lower transverse rupture strengths. In both cases, deformation at room temperature and , resulted in much lower strengths than deformation at , and also caused the fracturing of some SiC particles. The higher bend strengths and less SiC fracturing at are attributable to the presence of an Al-Cu liquid phase during deformation. The employment of copper coated SiC instead of bare SiC particles for preparing the composites was found not improving the properties.