간행물

한국분말야금학회 학술대회논문집

권호리스트/논문검색
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권호

한국분말야금학회 2006년도 추계학술대회논문집 (2006년 9월) 358

221.
2006.09 구독 인증기관·개인회원 무료
Magnetic characteristics observed in BiSrCaCuO superconductor were studied. In the measurement of differential conductance, it was cleared that the mechanism of magnetic memory effect couldn't be explained by using conventional flux flow model. By changing the density of external magnetic flux, changes in inductance of a coil in which a superconducting bar inserted were also measured. The results showed that the filament model was valid to explain the mechanism of the occurrence of a voltage in superconducting sample. It was concluded that the electromagnetic characteristics arose from the interaction between the trapped magnetic flux and weak link of the filament formed in the superconducting bulk.
222.
2006.09 구독 인증기관·개인회원 무료
When was added to Ti-excess ((Ba+Y)/Ti =1), the area occupied by ion was confirmed by its microstructure development, electrical conductivity behavior and lattice constant. Grain growth inhibition was observed when the content of donor dopant exceeded a critical value () in system. A donor-doped behavior was observed at various Y contents ( mol% Y) when was added to -excess . As Y content was increased, (002) and (200) peaks shifted to higher angles and the lattice constant (a and c axis) decreased gradually.
223.
2006.09 구독 인증기관·개인회원 무료
The Powder characteristics and sintering behavior of coated were studied. Silica coated powders were prepared by sol-gel method. The particle size of the powders were nm and the thickness of the coating layer was nm. As the content increased, the layers improved the powder dispersion. The Zeta potential of coated was getting close to that of pure silica with a more negative charge, compared with that of the uncoated . The onset temperature of shrinkage curves shifted to higher temperatures with increasing contents
224.
2006.09 구독 인증기관·개인회원 무료
The mechanical properties of ceramics materials can be tailored by designing their microstructures. We have reported that development of texture can be controlled by slip casting in a strong magnetic field followed by heating even for diamagnetic ceramics such as alumina. A strong magnetic field of 12T was applied to the suspension indcuding alumina powder to rotate each particle during slip casting. The sintering was conducted at the desired temperature in air without a magnetic field. C-axis of alumina was parallel to the magnetic field. Bending strength of textured alumina depended on the direction of oriented microstructure.
227.
2006.09 구독 인증기관·개인회원 무료
The pretreatment for substrate was carried out in change of gun pressure of bar using wet blasting. The size of powder was about . As the results, the surface roughness of cemented carbide substrate was improved with increment of gun pressure of wet blasting. A new surface layer was formed and Co particles were uniformly distributed over the entire surface after pretreatment. The adhesion of the pretreated substrate in same PVD-TiAlN film was improved and in approximately shown the best adhesion value.
228.
2006.09 구독 인증기관·개인회원 무료
Several boride sintered bodies such as , , and were previously reported. In the present study, the sinterability and physical properties of chromium boride containing chromium carbide sintered bodies were investigated in order to determine its new advanced material. The samples were sintered at desired temperature for 1 hour in vacuum under a pressure by hot pressing. The relative density of sintered bodies was measured by Archimedes' method. The relative densities of addition of 0, 5, 10, 15 and 20 mass% composites were 92 to 95%. The Vickers hardness of the with 10 and 15 mass% composites were about 14 and 15 GPa at room temperature, respectively. The Vickers hardness at high temperature of the addition of 10 mass% composite decreased with increasing measurement temperature. The Vickers hardness at 1273 K of the sample was 6 GPa. The Vickers hardness of addition of composites was higher than monolithic sintered body. The powder X-ray diffraction analysis detected CrB and phases in containing composites.
230.
2006.09 구독 인증기관·개인회원 무료
The coating of conductive polypyrrole (Ppy) on nonconductive ceramic substrates was performed by polymerization of pyrrole (Py) in an aqueous solution. The Ppy film was characterized by scanning electron microscopy and conductivity measurements. Electrophoretic deposition of bimodal alumina suspension prepared with a phosphate ester was performed using Ppy film as a cathode. Fabrication of alumina ceramics with irregular shapes or complicated patterns were also attempted by sintering the deposits together with the Ppy coated substrates in air.
233.
2006.09 구독 인증기관·개인회원 무료
[ ] was coated with , MgO and respectively by sol-gel method and cured at 900 and . The coated oxides did not react with at but reacted with it to form at . The specimen coated with at formed a dense protecting layer and showed the best oxidation resistance at in air. However, the dense protecting layers did not form in and MgO coated specimens cured even at . MgO coated specimen showed the worst improvement in the oxidation resistance because the reactivity of MgO with was highest. On the other hand, the electrical conductivities were measured in MgO and coated specimens to have TiCx but could not be measured in the coated ones because of the nonconductive dense protected layers.
234.
2006.09 구독 인증기관·개인회원 무료
The perovskite- type oxide containing transition metals on the B-site show mixed (electronic/ionic) conductivity. These mixed-conductivity oxides are promising materials for oxygen permeating membranes. The main objective of this research work is to synthesize and characterization ceramic powders of the Sr-Co-Fe-O system for methane conversion using membrane reactor. SCFO powders were synthesized from the route was based on the complex method of combination of acid EDTA and citrate and shown be available by control efficient of synthesis to performed , moreover, it presented easy implementation, reproducibility and operation. Powder ceramic was characterized by XRD, microscopic optic, SEM and TG-DTA.
235.
2006.09 구독 인증기관·개인회원 무료
The preparation of single-phase with delafossite-type structure by means of the solid-state reaction method was investigated using X-ray diffraction. The results showed that notwhistanding the fact that there was a trace of metallic copper, nearly single-phase was obtained by using as a lanthanum source and by firing the mixed powder with nonstoichiometric composition ratio of in a vacuum at 1273 K for 10 h. The measurement of electrical conductivity and Seebeck coefficient showed that thus obtained was a p-type semiconductor and had a Seebeck coefficient of approximately .
236.
2006.09 구독 인증기관·개인회원 무료
Lanthanide tantalite (Ln= La, Nd, Sm, Dy, Er and Tm) was synthesized by a solid state reaction between mixed powders of and . The single-phase was prepared by sintering at temperatures of 1423-1673 K in air. The SEM observation showed that the particles were provided with the growth steps and the depeloped facets. The photocatalytic activity for water splitting of prepared was measured under UV light irradiation. The activity obtained was higher than that previously reported. These results suggested the crystallinity of photocatalysts correlates closely with the efficiency of water splitting.
238.
2006.09 구독 인증기관·개인회원 무료
High Energy Milling (HEM) is applied for the grinding of cement and this can lead to substantial refinement (<2μm) and mechanically activation of the powder particles. The present paper reviews the preliminary studies, explains the novel technique and suggests the route into commercial application. Particular attention is paid to wear results with an applied unit where no substantial wear was found after 4000 h of operation.
240.
2006.09 구독 인증기관·개인회원 무료
Mn-Fe oxide and Mn-Fe oxide/(50wt%/50wt%) were prepared by ball milling method. XRD data of the prepared samples revealed that hematite and ferrite phase coexisted. Water splitting at 1273K, after thermal reduction at 1573K, was performed 4 times for the samples. Hydrogen production amount was analyzed by GC with TCD detector. Water splitting capacity of Mn-Fe oxide was improved by ball milling with .