The influence of red lead(Pb3O4) to curing and formation reaction properties when it was added in positive material of lead acid battery for vehicle use has been investigated. At the results, it was confirmed that the addition of red lead led 4BS crystal size to be smaller and increased the rates of 4BS formation and Pb consumption. Consequently the curing time was shortened to half compared with that of red lead-free one. In addition to this, the lead acid battery prepared by adding red lead showed 14% higher efficiency at the life cycle test than that without red lead.

This study investigates the paste mixing of positive active materials which, affect the life cycle of batteries in Pb-Ca-Sn grids, and generation of 4BS in a curing process and considers the effects of these things on the initial charge characteristics and life cycle. In the results of the experiments applied in this study, it was possible to reduce the curing time in which the fine 4BS was formed by the mixing of the positive active materials of lead acid battery applied at high temperature compared to that of the existing coarse 4BS and that represented some improvements in the life cycle performance.

This article shows various factors that influence the thermal-cycling reliability of semiconductor devices utilizing the lead-on-chip (LOC) die attach technique. This work details how the modification of LOC package design as well as the back-grinding and dicing process of semiconductor wafers affect passivation reliability. This work shows that the design of an adhesion tape rather than a plastic package body can play a more important role in determining the passivation reliability. This is due to the fact that the thermal-expansion coefficient of the tape is larger than that of the plastic package body. Present tests also indicate that the ceramic fillers embedded in the plastic package body for mechanical strengthening are not helpful for the improvement of the passivation reliability. Even though the fillers can reduce the thermal-expansion of the plastic package body, microscopic examinations show that they can cause direct damage to the passivation layer. Furthermore, experimental results also illustrate that sawing-induced chipping resulting from the separation of a semiconductor wafer into individual devices might develop into passivation cracks during thermal-cycling. Thus, the proper design of the adhesion tape and the prevention of the sawing-induced chipping should be considered to enhance the passivation reliability in the semiconductor devices using the LOC die attach technique.

In this study, positive plates of lead acid battery of Pb-Ca alloy and Pb-Ca-Sn alloy were fabricated and the mechanical characteristics of positive plates were measured. This study observed how the changes of content of Ca & Sn affect interface corrosion which is located in between grid & active materials and lead acid batteries as well. The mechanical characteristics of grid alloy is better when Ca is 0.05 wt.% then 0.1 wt.%. This study said that the corrosion rate between the active material based on the charge/discharge cycle of lead acid battery and grid interface is much faster than a grid which contains Sn. And furthermore, according to the study the rate 30 of Sn/Ca which is added to grid shows the best performance.

Trace analysis of Cd and Pb at surface modified thick film graphite electrode with Bi nanopowder has been carried out using square-wave anodic stripping voltammetry (SWASV) technique. Bi nanopowder synthesized by gas condensation (GC) method showed the size of nm with BET surface area, . For a strong adhesion of the Bi nanopowder onto the screen printed carbon paste electrode, nafion solution was added into Bi-containing suspension. From the SWASV, it was found that the Bi nanopowder electrode exhibited a well-defined responses relating to the oxidations of Cd and Pb. The current peak intensity increased with increasing concentration of Cd and Pb. From the linear relationship between Cd/Pb concentrations and peak current, the sensitivity of the Bi nanopowder electrode was quantitatively estimated. The detection limit of the electrode was estimated to be and for Cd and Pb, respectively, on the basis of the signal-to-noise characteristics (S/N=3) of the response for the solution under a 10 min accumulation.

Positive temperature coefficient of resistivity (PTCR) characteristics of (1-x)BaTiO3-x(Bi0.5K0.5)TiO3ceramics doped with Nb2O5 were investigated in order to develop the Pb-free PTC thermistor available at hightemperatures of >120oC. The PTCR characteristics appearing in the (Bi0.5Ki0.5)TiO3 (<5mol%) incorporatedBaTiO3 ceramics, which might be mainly due to Bi+3 ions substituting for Ba+2 sites. The 0.99BaTiO3-0.01(Bi0.5K0.5)TiO3 ceramics showed good PTCR characteristics of a low resistivity at room temperature (ρr) of31 Ω·cm, a high ρmax/ρmin ratio of 5.38×103, and a high resistivity temperature factor (α) of 17.8%/oC. Theaddition of Nb2O5 to 0.99BaTiO3-0.01(Bi0.5K0.5)TiO3 ceramics further improved the PTCR characteristics.Especially, 0.025mol% Nb2O5 doped 0.99BaTiO3-0.01(Bi0.5K0.5)TiO3 ceramics exhibited a significantly increasedρmax/ρmin ratio of 8.7×103 and a high α of 18.6%/oC, along with a high Tc of 148oC despite a slightly increasedρr of 39 Ω·cm.

The performance of positive plates depends on the structure of the lead dioxide active mass. The positive active materials (PAM) consists of a skeleton, built up of agglomerates and macropores. Agglomerates, in their turn, comprise particles and micropores. This paper described a study conducted to determine the effects of different soaking times between the acid fill and formation stages of the tubular plate production. For the positive plates a lead oxide were filled into tubular bag with a red lead. After filling the positive plates were soaked in H2SO4 solution. X-ray diffraction(XRD), scanning electron microscopy(SEM) and electrical testing had been used to study the compositional and morphological aspects of the positive active material(PAM) just prior and after formation. Results indicate that PAM compositions were effected by the soaking time and acid density of H2SO4 solution. It can be seen that as the soaking time duration increases, α-PbO, Pb3O4, and Pb were all gradually sulphating. Composition of 3BS reached a maximum at around 3 h duration and H2SO4 of sp. gr. 1.10 on soaking. This results would suggest that the most beneficial conditions for soaking were the H2SO4 of sp. gr. 1.10 and 2 to 6 h of soaking.

This study was conducted to made a grid alloy (Pb-Ca-Sn-Al) which has a temporary composition ratio in order to improve the efficiency of lead acid batteries. The positive activity material made a 3BS(tri-basic lead sulfate; 3PbO·PbSO4·H2O) by a low temperature curing and it evaluates the plate efficiency through the life cycle testing. The initial current capacity of low temperature curing plate was excellent but the life cycle was not good (S1). As for the S2 plate, however, the initial current capacity and the life cycle were superior.

본 연구는 2000~2002년 사이에 우리나라에서 사망한 야생조류의 간, 신장 그리고 뼈에서의 납과 카드뮴 농도를 분석하였다. 연구에 이용된 시료는 황새목(n=10), 기러기목 (n=3), 매목 (n=7), 도요목 (n=8), 비둘기목 (n=2) 그리고 참새목 (n=6)이었다. 간에서 납 농도는 도요목<기러기목<황새목<매목<참새목<황새목<기러기목<매목<참새목

목적：본 연구의 목적은 지역사회중심 뇌졸중작업치료프로그램이 클라이언트의 기능향상과 삶의 질 향상에 효과가 있었는지 분석하고, 실습교육으로서 학생들의 프로그램 운영에 따른 만족도를 분석하여 지역사회중심 임상실습교육프로그램의 기초 자료를 제공하고자 한다. 연구방법：연구대상은 뇌졸중작업치료프로그램에 참여한 클라이언트와 프로그램의 운영에 참여한 작업치료과 재학생을 대상으로 하였다. 1) 클라이언트는 2006년 4월-11월 동안 2차로 나누어 초기평가-10주 중재-재평가를 실시하였으며, 26명을 분석 대상으로 하였다. 2) 작업치료과 학생들은 평가, 중재프로그램 계획, 프로그램 실행, 재평가에 참여하였으며, 그중 설문에 응답한 50명의 학생을 대상으로 교과목과 연결된 임상실습교육으로서의 만족도를 분석하였다. 분석은 클라이언트의 전·후 변인의 차이를 검증하기 위해 윌콕슨 쌍대비교(Wilcoxon matched-paired sign-ranks test), 학생들의 만족도분석은 기술통계를 이용하였다. 결과： 1) 클라이언트의 기능향상에서는 전반적으로 호전되었으며, 특히 균형능력과 감각 중 통증과 심부압박이 유의한 결과를 보였다(p<.05). 삶의 질은 전반적으로 좋아졌으며, 특히 일반적 건강은 통계학적으로 유의한 차이를 보였다(p<.05). 2) 학생들의 실습교육 프로그램 운영에 따른 만족도는 전체 평균이 4.32/5점 척도로 높게 나타났으며, 작업치료사의 역할에 대한 이해 향상의 만족도가 4.46±0.61(M±SD)로 가장 높았다. 결론：지역사회중심 뇌졸중작업치료프로그램에 참여한 클라이언트의 기능향상과 삶의 질 향상에 효과가 있었으며, 학생들의 실습교육 프로그램 운영에 따른 만족도도 매우 높게 나타났다. 그러므로 다양한 지역사회중심 임상실습교육프로그램의 개발·운영을 통해 지역사회에 공헌하고, 학생들에게는 학교 졸업 후 임상에서 초임 작업치료사로서 역할을 다할 수 있도록 다양한 경험과 자신감을 제공할 수 있는 질적인 임상실습교육이 필요하다.

본 연구는 국내 유통 중인 프라이팬, 냄비, 주전자, 불판 등 금속제 주방기구 총 71품목을 대상으로 안전성 및 오염 정도에 대한 기초 자료를 제공하고자 실시되었다. 현행 식품공전 금속제의 재질 규격은 Pb 10 %, Sb 5 % 이하이며 용출 규격은 Pb 1.0 mg/L 이하이다. 알루미늄, 스테인리스 및 주철 총 71품목의 금속제 주방기구에 대한 재질시험 결과 Pb은 0.06 % 이하로 검출되었으나 기준이하였으며 Sb은 모든 제품에서 검출되지 않았다. 또한 이들 주방기구의 용출시험 결과에서도 기준치이하인 0.41 mg/L 의 Pb이 검출되어 국내 유통 중인 금속제 주방기구는 기준규격에 적합한 것으로 나타났다.

Generally, it has been known that positive plate efficiency is the most influential effect on the initial current capacity of lead acid battery. Thus, in this study, we have investigated the curing effect of the positive plate, which is one of the important lead acid battery processes. The curing process of the positive plate is performed either with the separation of each plate with 1mm gap or with no gap of plate. As a result, when there is no interval between each plate, the higher temperature current happened than expected, resulting in the changes in the initial current efficiency of the lead acid battery. The chemical composition and crystal structure of a material coated on the positive plate were identified with XRD and SEM. It was resulted that were only there not a lot of 4BS (tetrabasic-lead sulfate, 4PbO·PbSO4) on the plate in case of curing of plates without interval, but a large quantity of Pb3O4 also formed on the surface. On the other hand, it was observed that 3BS (tribasic-lead sulface, 3PbO·PbSO4·H2O) was the main product on the plate in case of typical curing process with some interval. From the initial current capacity test, the positive plate having 3BS was approximately 40% higher in initial current capacity than that having 4BS. It was concluded that 4BS and Pb3O4 on the plate surface were harmful to the initial current capacity of lead acid battery.

제조업체의 성공은 고객의 요구를 파악하는 능력과 이들 요구를 만족시키면서, 얼마나 최소비용을 투자하여 제품화를 신속히 개발하는가에 달려있다. 기업의 목표를 달성하기 위해서 제조 판매 및 마케팅 그리고 제품 디자인 및 개발기간과 같은 여러 요소들이 복합적으로 적절히 조화를 이루어야만 한다. 이 논문에서는 여러 요소 중 신제품 개발기간에 초점을 맞추어 현재 각 기업에서 많이 사용되고 있는 6시그마 기법을 적용하여 새로운 제품의 개발기간을 단축시키기 위한 방법론을 제시한다.

Some distributions have been used for diagnosing the lead time demand distribution in inventory system. In this paper, we describe the negative binomial distribution as a suitable demand distribution for a specific retail inventory management application.

기업은 고객이 원하는 시기에 원하는 제품을 구매할 수 있도록 항상 준비가 되어 있어야 한다. 고객의 수요를 만족시키기 위하여 기업은 다양한 수요예측방법을 통하여 적절한 재고 수준과 수요예측을 하고 있다. 제조 기업의 경우에는 다른 산업에 비하여 정확한 수요예측과 낮은 재고 수준의 유지가 비용과 직접적인 연관이 있기 때문에 제조 기업은 경제적인 주문량 결정(Economic Order Quantity: EOQ)이 매우 중요한 문제이다. 주문량을 결정하는 방법에는 여러 가지가 있지만, 본 논문에서는 고객 지연을 방지하기 위하여 경제적 주문량 결정에 고객 지연과 관련된 비용을 포함시키는 것은 물론 고객 지연이라는 상황을 방지하는 노력의 한 방법으로 가격 할인(discount system)을 이용하고자 한다. 가격 할인을 이용하여 고객으로 하여금 빠른 주문을 유도하고 그로 인하여 고객 지연 상황의 발생을 줄여보려고 한다.